IV/ Result :

Part A: Preparation of KMnO4 solution.

Experiment I:
Calculated weight of solid KMnO4:
Cm x V
 n(KMnO4) = 0.0025 (mol)  m(KMnO4) = 0.395 (g)
Actual weight of solid KMnO4: 0.395(g)
Volume of distilled water: 250mL
Final result: 250mL of 0.01M KMnO4 solution.

Experiment II:
Volume of 0.01 M KMnO4:
C1 x V1 = C2 x V2
 50 x 2x10-3 = V x 0.01  V = 10 (mL)
Volume of distilled water: 40mL
Final result: 50mL of 2mM KMnO solution.
4
Experiment III:
 Final concentration Volume of 0.01M Volume of distilled
No
(mM) KMnO4 (mL) water (mL)

1 1.0 1 10

2 0.6 0.6 6

3 0.4 0.4 4

4 0.2 0.2 2

5 0.1 0.1 1

Final result: 10mL of each following solutions: 1.0 mM KMnO4, 0.6 mM KMnO4, 0.4
mM KMnO4, 0.2 mM KMnO4, 0.1mM KMnO4.

Experiment 4:
Volume of 2mM KMnO4: 𝑪𝟏 𝑽𝟏 = 𝑪𝟐 𝑽𝟐 => 2 𝑥 𝑽𝟏 = 𝟏 𝒙 𝟔 => 𝑽𝟏 = 𝟑 (𝒎𝑳)
Dilution factor:
df = V2 / V1 = 6/3 = 2
With V2 = 6 (mL), V1 = 3 (mL)
Final result:
6 mL of each following solutions:
 Test Volume
tubes
1 2.0 mM KMnO4
2 1.0 mM KMnO4
3 0.5 mM KMnO4
4 250 µM KMnO4
5 125 µM KMnO4
6 62.5 µM KMnO4

Part B: Preparation/Testing 1of 0.10 M Copper sulfate pentahydrate.

Absorbance of CuSO .5H O at 700 nm wavelength

4 2
 Sample Absorbance (A)

1 0.755

2 0.755

3 0.755

Absorbance at 700 nm, 0.10 M CuSO .5H O, known: 0.77

4 2

Absorbance at 700 nm, 0.10 M CuSO .5H O, measured:

4 2

0.755 + 0.755 + 0.755

𝐴= = 0.755
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𝑨𝒎𝒆𝒂𝒔𝒖𝒓𝒆𝒅 − 𝑨𝒌𝒏𝒐𝒘𝒏
% 𝑬𝒓𝒓𝒐𝒓 = 𝒙 𝟏𝟎𝟎%
𝑨𝒌𝒏𝒐𝒘𝒏

0.755 − 0.77
= × 100% = −1.95%
0.77