DOCUMENT CODE AMM-WI-QMS-002 REV. # 00 REV.

DATE 08/05/07 PAGE 1 of 1

WORK INSTRUCTION Ammonia Unit

TITLE: SHUT DOWN INSTRUCTION

STEPS:

1. SHUT DOWN PROCEDURE

1.1. Reduce the plant load at FRCa-104 to 6.8 div.
1.2. Open purge gas vent valve PiC-131 & close purge gas valve to fuel gas circuit of 101-B.
1.3. Stop PGRU.
1.4. Stop syn loop & ensure that SP-4/5 valves are closed.
1.5. Stop 103-J & shift the vent to PiC-121.
1.6. Adjust HS steam flow & pressure.
1.7. Reduce the gas load from 6.8 div to 6.6 div & adjust the firing at furnace accordingly.
1.8. Stop methanator & shift the vent to PiC-119.
1.9. Bypass LTSC & isolate it.
1.10. Close absorber inlet block valve & open SP-7 gradually.
1.11. Stop 107-J & keep catacarb solution running through 108-J.
1.12. Change over jacket water 101-C/103-D & transfer line to demin water.
1.13. Take 111-C online.
1.14. Stop 101-J.Ensure SP-3 valve is closed & steam to steam/air coil is opened.
1.15. Reduce gas load gradually to 4.0 div & adjust the furnace firing accordingly.
1.16. Reduce furnace out let temperature to 750C & stop the process gas to 101-B.
1.17. Isolate 103-B fuel & PRC-102.
1.18. Continue the flushing of 101-B with steam & maintain back pressure at 12
kg/cm2.Gradually reduce the furnace temperature at @ 60C per hour & bring it up
to 400C.
1.19. Stop steam let down from HS to MS header by informing Utilities palnt.Open
superheat vent valve.
1.20. Stop steam to 101-B.close all the corck valves of arch burners.
1.21. Stop auxiliary boiler burners.
1.22. Insert blind in the mixed feed line to 101-B.
1.23. Depressurize fuel gas header & insert blind in main natural gas line at battery limit.
1.24. Open top vent valve of 101-F (steam drum) at 8 kg/cm2 steam pressure.
1.25. Keep I.D fan running at 2500 rpm till the furnace is cooled down to room
temperature for safe entry.
1.26. Stop I.D fan.

PREPARED BY APPROVED BY REFERENCE 4.2.1 (d)

Shafiq Ahmed Muhammad Muazzam
Operating Instruction Manual
Staff Engineer UM