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Transportation Geotechnics 22 (2020) 100305

Contents lists available at ScienceDirect

Transportation Geotechnics
journal homepage: www.elsevier.com/locate/trgeo

Influence of water and frost on the performance of natural and recycled T


materials used in unpaved roads and road shoulders

Stefan Huber , Christoph Henzinger, Dirk Heyer
Department of Civil, Geo and Environmental Engineering, Chair of Soil Mechanics and Foundation Engineering, Rock Mechanics and Tunnelling, Technical University of
Munich, Munich, Germany

A R T I C LE I N FO A B S T R A C T

Keywords: In recent years, recycled materials from construction and demolition waste (C&D materials) have gained ever
Degradation of geomaterials more importance as secondary construction materials in civil engineering, especially for road construction
Strength purposes. Their use in high-grade applications is an important contribution to a circular economy. However,
Testing of materials from a technical viewpoint, reservations remain about the use of such materials. Such reservations typically
Waste management
concern their performance when exposed to water and frost. The aim of this study was to evaluate the field
Disposal
performance of unbound mixed C&D materials used in surface applications like road shoulders or unpaved roads
and exposed to the weather conditions of central Europe and to compare the mixed C&D material with two
natural reference materials. Two mixed C&D materials and two natural reference materials were field compacted
and exposed to the weather during the winter of 2017/2018 and early summer of 2018. The parameters
monitored during the period of observation were dry density, stiffness and particle breakdown due to weath-
ering. The results highlight the possible technical benefits of using C&D materials derived from construction and
demolition waste instead of natural raw materials in applications such as road shoulders or unpaved roads.

Introduction an increase in strength and stiffness over time [34,33,63], which was
attributed to the self-cementing properties of the C&D materials in each
In recent years, recycled materials from construction and demolition case. In addition to the application of C&D materials for road con-
waste (C&D materials) have gained ever more importance as secondary struction purposes there are several more applications reported in the
construction materials in civil engineering, and especially for road literature illustrating the manifold application possibilities of C&D
construction purposes. By using C&D materials as construction mate- materials. Thus, C&D materials, for example, can be used as material for
rials, the consumption of valuable primary construction materials such bedding pipes [14,13] and backfilling pipe trenches [81], for soil
as gravel and sand can be decreased. Additionally, the consumption of [52,53,54] and ground improvement purposes [62,66], as landfill cover
land that would be required for the extraction of primary construction layers [51] or in mineral sealing systems [46].
materials and the disposal of residual mineral masses can be reduced. Despite all these research efforts, there are still doubts remaining
The use of C&D materials for construction purposes is therefore an about the use of recycled aggregates from construction and demolition
important contribution to a circular economy. waste, especially for applications in which they are subjected to
A considerable number of laboratory studies has shown that C&D freezing temperatures or changes in water content, for instance in un-
materials can meet the respective requirements for the use in unbound paved roads or road shoulders. The aim of this study was to evaluate the
base or subbase layers [31,89,13,11,16,9,10,50,8,57,64,88,73], road field performance (changes in density, stiffness, durability) of mixed C&
embankments [29,84,85] or low-volume unpaved roads [58,59]. D materials for use in road shoulders and unpaved roads compared to
However, the suitability of such materials depends on the physical and natural aggregates, under realistic weather conditions of central
chemical properties of their individual constituents [17], and therefore Europe. Crushed limestone (LS), which is a well-established and fre-
some C&D materials may be more appropriate for use in certain ap- quently used material for road construction purposes in Germany (e.g.
plications than others [18,69]. frost protection layer, base and sub-base layer, road shoulders), was
A number of field studies also support the use of C&D materials for used as the natural reference material.
road applications [65,34,32,33,72,55,63,77]. Some have even reported Two C&D and natural aggregates (grain size 0/8 mm and 0/32 mm)


Corresponding author at: Lehrstuhl für Grundbau, Bodenmechanik, Felsmechanik und Tunnelbau (Zentrum Geotechnik), Baumbachstraße 7, 81245 Munich,
Germany.

https://doi.org/10.1016/j.trgeo.2019.100305
Received 27 September 2019; Received in revised form 3 December 2019; Accepted 4 December 2019
Available online 09 December 2019
2214-3912/ © 2019 Elsevier Ltd. All rights reserved.
S. Huber, et al. Transportation Geotechnics 22 (2020) 100305

resulting from the crushing process [18]. It is well known that such
Nomenclature
granulometric parameters influence the mechanical behaviour (and of
course the friction angle) of granular materials [90,4,26,68,67]. As
List of notations
known from natural materials, stress-strain behaviour and the shear
strength of such recycled aggregates strongly depend on the respective
DPr is degree of compaction
degree of compaction [5,74].
EV1 is the elastic modulus determined with the static plate
Regarding resilient modulus MR, which often is recognised as the
load test at initial loading
parameter best reflecting a materials response to traffic loads (since it
EV2 is the elastic modulus determined with the static plate
describes materials stiffness after undergoing many load-cycles) a lot of
load test at reloading
work has been done by several researchers on C&D materials
EVd is the elastic modulus determined with the dynamic
[19,86,60,12,28,22,64,83,70,7,6,71,21,76]. However, there is no con-
plate load test
sensus in the literature on the influence of recycled aggregates on MR of
MR is the resilient modulus
construction materials. Some researchers report that the MR of C&D
materials is similar or even higher than the MR of natural aggregates
[25,13,64,7,21,76], while others have shown that an increasing pro-
were compacted at a test site near Munich in the autumn of 2017. Field
portion of recycled aggregates leads to a reduced MR [83]. Since MR of
tests were performed at several different times during the winter of
CC is reported to be higher than MR of CB [13], this probably is also a
2017/2018 and early summer of 2018. During this period, the surfaces
consequence of the different material compositions of various C&D
of the compacted materials lay fully exposed to the weather, and the
materials. For C&D materials containing CC, an increase of MR due to
dry density, static and dynamic modulus of deformation and particle
hydraulically active components has also been reported [6].
breakdown were monitored. This paper summarises the results of this
The influence of frost action on MR was for example studied by
field study.
Soleimanbeigi et al. [86] for CC and natural aggregates. They found MR
to decrease after several initial freeze-thaw cycles for both materials.
Literature review However, only the MR of the crushed concrete material increased
during further freeze-thaw cycles. This was attributed to secondary
Recycled aggregates from construction and demolition waste (e.g. hardening effects (the self-cementing ability of the crushed concrete).
crushed concrete and mixed recycled material) differ from natural ag- Comparable tendencies for the development of the MR of mixed C&D
gregates in terms of a range of material properties, one of the most materials subjected to freeze-thaw cycles were reported by Bassani &
important being particle density. There is a consensus in the scientific Tefa [19]. However, they also identified the moulding parameters as
literature that this particle density influences the overall behaviour and crucial for the development of the MR during freeze-thaw cycles (i.e.
suitability of such materials to a great extent: aggregates with higher decrease in MR for samples prepared on the dry side of optimum, in-
particle densities provide higher grain strength and stiffness, as well as crease in MR for samples prepared at optimum water content and at
reduced water absorption capacity and particle breakage potential due water contents slightly above that).
to compaction [25]. The resistance of individual particles to frost action One special characteristic of C&D materials containing CC is, as
depends on the particle strength [19,75], which is usually directly re- already mentioned, their self-cementing-ability. In the presence of
lated to the particle density. water, unhydrated cement can lead to secondary hydration processes
Other studies reveal the influence of particle density on the load- and therefore to an increase in stiffness and strength
bearing capacity (typically measured as CBR strength, resilient mod- [60,27,88,78,80,34,33,63,6]. Non-active proportions other than CC, for
ulus, stiffness) of such materials; crushed concrete (CC) usually has a instance CB, do seem to lessen the self-cementation potential though
higher particle density than crushed bricks (CB) [30,35], and the load- [60].
bearing capacity typically increases with increasing proportions of CC
and decreases with increasing proportions of CB [25,78,79]. Compared Materials and methods
to natural aggregates, the load-bearing capacity is reported to be
slightly lower or similar for materials primarily constituted of CC Description of materials used in the field study
[78,80,57,64], and lower for mixed C&D materials containing relevant
amounts of CB or other components such as mortar or plaster [79,73]. Four materials from two material classes were considered in this
Particle breakdown due to frost action is also attributed to low study: crushed limestone of grain size 0/32 mm and 0/8 mm (named LS
particle strength and the low particle density of porous aggregates: 1 and LS 2 respectively) and mixed C&D materials from processed
freezing water contained in the porous aggregates is able to weaken the construction and demolition waste of grain size 0/32 mm and 0/8 mm
structure of the single grains. This weakening process begins when the (named C&D 1 and C&D 2 respectively). For the purpose of laboratory
water temperature falls below 4 °C (decreasing density of water, frost testing, a sample of approximately 100 kg of each material was taken
action). After several cycles or if the frost pressure exceeds the re- from the heaps on site in accordance with DIN EN 932-1 [36] before
spective particle strength, a particle may break (c.f. [19,25]). However, construction of the test fields. The samples were homogenised and split
the situation cannot be reduced to particle strength and density alone. up several times using a sample splitter as described in DIN EN 932-2
The number and size of pores accessible to water also seem to play an [38]. The laboratory tests were performed on the resulting test samples.
important role [19,25]. Results from Bazaz et al. [20], who exposed CC The particle size distributions of all the materials tested are shown
and CB to the same number of freeze–thaw cycles and found a sig- in Fig. 1, and relevant engineering properties are given in Table 1. The
nificantly higher amount of particle breakdown both for coarse (9.5 mm particle size distributions all individually show a continuous grading
to 50 mm) and fine (0.3 mm to 9.5 mm) CC than for CB, were explained and a fines content of about 7–8%. The maximum dry densities (MDD)
by Cardoso et al. [25] by a lower number of accessible pores in the CB. and the corresponding optimum water contents (OWC) provided in
In this context, it would seem logical that the resistance of natural Table 1 were determined using the Standard-Proctor test according to
aggregates to frost action is generally reported to be higher than with C DIN 18127 [41]. The air pycnometer procedure according to TP BF-StB
&D materials [20,75]. Part B 3.3 [48] was used to determine the particle density ρs (dry mass
With regard to shear strength, comparably high friction angles are of a single grain in relation to its volume), and a special procedure was
reported for C&D materials [86,81,13,82,74,73]. This is considered to used for the sample preparation of the C&D materials: first the particle
be due to their typically angular and sharp-edged individual particles density ρs was determined immediately after mixing with water

2
S. Huber, et al. Transportation Geotechnics 22 (2020) 100305

100 Design and construction of the test fields


LS 1
90
LS 2 The test fields were constructed in a backfilling pit on 22 and 23
Percent passing by weight [%]

80 C&D 1 November 2017 roughly 60 km north-west of Munich, Germany. The


planum (formation level) on which the test fields were constructed
70 C&D 2
mainly consisted of recycled material (crushed concrete and crushed
60 brick), which had been previously placed and compacted. Dynamic
plate load tests (Light Falling Weight Deflectometer, Portable Impulse
50
Plate Load Test Device), conducted prior to the construction of the test
40 fields, indicated EVd values mostly between 30 MN/m2 and 55 MN/m2.
Only in the southwestern part low EVd values between 8 MN/m2 and
30
12 MN/m2 were measured, which were attributed to the locally soaked
20 area of the subsoil below the planum. A schematic illustration of the EVd
values measured on the planum is shown in Fig. 2. Due to limited time,
10
space and construction equipment available on the test site, it was
0 unfortunately not possible to construct the test field at a different time,
0.01 0.1 1 10 100 at another location with more homogeneous subsoil conditions or after
Particle size [mm] replacing the soaked subsoil. However, the comparison of the results
Fig. 1. Particle size distributions of the materials used in this study. between the embankment built on inadequate subsoil (southern area of
lane 1) and the embankment built on adequate subsoil (northern area of
lane 1) is an illustrative example of the importance of subgrade quality
Table 1 for the performance of any material used in unpaved roads or road
Engineering properties of the materials used in this study.
embankments.
Material property mixed C&D material (C&D) Limestone (LS) Each material was distributed over a length of around 25 m and a
base-width of about 3.5 m with a wheel loader in two layers, each
C&D 1 C&D 2 LS 1 LS 2
roughly 0.3–0.4 m. Each of the two layers was compacted with a
Max. Grain [mm] 1
40 8 36 10 compaction roller (operating weight ~6.5 tonnes) in six dynamic passes
≤31.5 mm1 [%] 98.8 – 98.3 – (3 times forward, 3 times backward) and two static passes (1 time
≤2 mm1 [%] 31.9 61.4 28.6 40.7 forward, 1 time backward) to compensate for the shallow loosening
≤0.06 mm1 [%] 7.2 7.6 8.4 8.7
effects caused by the dynamic compaction process. After compaction (at
CU2 36.8 22.6 82.8 41.3
CC2 2.7 1.6 5.3 4.6 final height), each testing lane had a length of around 25 m and a width
ρS3 [Mg/m3] 2.666/2.717 2.676/2.727 2.71 2.72 of about 1,5 m and the total thickness of the compacted test fields was
OWC4 [%] 15.7 20.6 8.8 9.9 found to be between 0.5 m and 0.6 m. In the area of the soaked sub-
MDD 4 [Mg/m3] 1.870 1.680 2.150 2.070
surface, however, only a total layer thickness between 0.3 m and 0.4 m
Permeability k5 [m/s] 1.9 ∙ 10-6 8.1 ∙ 10-7 – 2.9 ∙ 10-7
was achieved. A picture of the completed test fields is given in Fig. 3.
1
particle size distribution according to DIN EN ISO 17892–4 [44].
2
Coefficient of uniformity (CU) and Coeficient of curvature (CC) according to
DIN EN ISO 14688–2[45]. Field testing methods
3
Particle density determined with the air pycnometer according to TP BF StB
Part B 3.3 [48]. Each lane shown in Fig. 3 was divided into a northern and a
4
Maximum dry density (MDD) and Optimum water content (OWC) deter- southern area and each area was further subdivided into four individual
minded using the Standard-Proctor test according to DIN 18127 [41]. sub-fields, each about 2 m long and 1.5 m width. This was done to
5
Permeability according to DIN 18130 [37], for DPr ≈ 100%. obtain two individual data sets per date of testing and material (re-
6
immediately after mixing with water.
7 plicates). With the exception of the soaked area of lane 1, the northern
4 days after mixing with water.
and southern areas and sub-fields can be considered as identical. The
four individual sub-fields were numbered, with the numbering in-
(original procedure used for natural, non-porous materials) and then
creasing from the outside to the inside (see Fig. 4). The locally soaked
the particle density ρs was determined after four days of soaking (with
area of the subsoil in the northwestern part of lane 1 again is indicated
the purpose of allowing the water to penetrate most accessible pores).
in Fig. 4 (sub-fields 1S to 3S). Since the static and dynamic moduli of
The measured values of particle density ρs immideately after mixing
deformation determined on the compacted test material in this area
with water approximately correspond to the “oven-dried particle den-
sity ρrd” according to DIN EN 1097-6 [43], which relates the dry mass of
Table 2
a single particle in relation to its volume including intraparticulate
Material composition of C&D 1.
sealed voids and including water accessible voids. The measured values
of particle density ρs after four days of soaking approximately corre- Class Type Percent by mass (%)
spond to the “apparent particle density ρa” according to DIN EN 1097-6 Rc Concrete and mortar1)
58.90
[43], which relates the dry mass of a single particle in relation to its Ru Unbound aggregates2) 26.46
volume including intraparticulate sealed voids, but excluding water Rb Fired clay bricks and ceramics 8.87
accessible voids. Rbm Lightweight particles3) 5.35
Rg Glass 0.13
The material composition of C&D 1 determined on the fraction of
Ra Asphalt 0.07
particles of the material greater than 4 mm in accordance with DIN EN X Non-mineral constituents4) 0.15
933-11 [40] is shown in Table 2. For C&D 2, the material composition Xi Ferrous and non-ferrous metals 0.07
was not determined due to the smaller grain sizes. However, C&D 2 was
1
produced from the same base material as C&D 1. Also natural aggregates predominantly with cement mortar.
2
Also natural aggregates with low adhesion of cement mortar.
3
Aerated concrete, pumice, sand-lime brick, gypsum.
4
Wood, plastic, textiles and paper.

3
S. Huber, et al. Transportation Geotechnics 22 (2020) 100305

soaked
Lane 1 –
Limestone 1
8 MPa 12 MPa 28 MPa 34 MPa 34 MPa 30 MPa 1.5 m

Lane 2 –
C&D 1
47 MPa 44 MPa 45 MPa 27 MPa 44 MPa 42 MPa 1.5 m

Lane 3 –
Limestone 2
48 MPa 44 MPa 42 MPa 35 MPa 38 MPa 41 MPa 1.5 m

Lane 4 –
C&D 2
55 MPa 54 MPa 52 MPa 48 MPa 47 MPa 51 MPa 1.5 m

S N

3.0 m 8.0 m 8.0 m 3.0 m


Fig. 2. Dynamic moduli of deformation EVd determined on the planum before the construction of the test fields.

were largely influenced by the soaked subsoil (the moduli of de- [°C × days] was calculated from the mean daily temperatures within
formation were considerably lower, see Fig. 2) these results are shown this period [92]. Using design curves of the US Corps of Engineers for
dashed and are discussed separately in the discussion of the results (see prediction of the frost penetration in a well-drained, non-frost suscep-
Sections ‘Static modulus of deformation on initial loading (EV1)’, ‘Static tible base course as a function of the freezing-index FI (see e.g.
modulus of deformation on reloading (EV2)’ and ‘Dynamic modulus of [92,93]), a frost penetration depth of about 0.4 m was obtained. The
deformation (EVd)’). frost penetration depth is thus well below 80 cm, which are usually
Field tests were performed on several occasions during the winter of used as design parameter for the frost penetration depth in traffic en-
2017/2018 and early summer of 2018. The relevant weather data re- gineering in Germany [87].
presentative for the area of the test site and test period were provided as Testing of the individual sub-fields was carried out in ascending
daily mean values by four weather stations located approximately order according to the numbering, with one sub-field from the north
11 km, 14 km, 19 km and 35 km around the test fields. All of the and one from the south being tested on each testing date (replicates). In
weather stations show very similar values for precipitation and tem- total, there were four testing dates. The first testing was conducted on
perature. Using the weather data in the vicinity of the test site, the 22 November 2017 (lane 1 and 2: materials LS 1 and C&D 1) and 23
relevant weather data at the test site were calculated using a 1/r2 November 2017 (lane 3 and 4: materials LS 2 and C&D 2), immediately
weighting scheme [91]. The weather data from the four weather sta- after the installation and compaction of the respective materials (tested
tions and the virtual data for the test site are illustrated in Fig. 5. sub-fields: 1S and 1N). After a period without any significant frost
The relevant freezing-period occurred during 4th February and 3rd periods but with occasional precipitation, the second series of tests were
March 2018 (marked in Fig. 5) and a freezing-index FI of 103 performed on 10 January 2018 (2S and 2N). It was ensured that there

Fig. 3. Test fields after construction.

4
S. Huber, et al. Transportation Geotechnics 22 (2020) 100305

soaked area

Lane 1: LS 1 1S 2S 3S 4S 4N 3N 2N 1N 1.5 m

Lane 2: C&D 1 1S 2S 3S 4S 4N 3N 2N 1N 1.5 m

Lane 3: LS 2 1S 2S 3S 4S 4N 3N 2N 1N 1.5 m

Lane 4: C&D 2 1S 2S 3S 4S 4N 3N 2N 1N 1.5 m

S N

3.0 m 2.0 m 2.0 m 3.0 m


Fig. 4. Subdivision of the test fields.

had been no groundfrost to influence the measurements before any tests results per material). On the first and last testing date, the dry density
were carried out. This was done by excavating a small pit in one of the was additionally determined using a nuclear gauge as per TP BF-StB
sub-fields which had already been tested, and by checking the tem- Part B 4.3 [94]. Again, two tests with the nuclear gauge were performed
perature of the now open cross-section with an infrared thermometer. in each sub-field on the first testing date (four results per material)
The third testing date was on 4 April 2018 (3S and 3N) after a cold while on the last testing date just one test was conducted (two results
phase with periods of very low temperatures and snowfall. Again, it was per material). Measurements with the nuclear gauge were performed in
ensured that there was no groundfrost to influence the measurements. any case at three different measuring depths per measuring point (0.05,
Between the penultimate and the final testing date on 7 June 2018 (4S 0.15 and 0.30 m) and the dry densities obtained were evaluated both as
and 4N), no more temperatures below zero Celsius were recorded. The individual and averaged values.
heavy precipitation shown in Fig. 5 on the last testing date occurred in The stiffness of the compacted materials was monitored by means of
the late afternoon/evening of that day and only after the tests had been static and dynamic plate load tests. Both test methods allow the mea-
completed. surement of the stiffness of the uppermost compacted layer and are
The field tests performed on each of the individual sub-fields on the used in German earthworks practice either as an indicator of the per-
respective testing dates included density checks and a check of stiffness formance of the compacted material when subjected to loading or as an
(static and dynamic plate load tests). Table 3 shows a summary of the indirect measure of relative compaction.
number of tests performed at each testing date. The dry density was The static modulus of deformation at initial loading (EV1) and re-
investigated using the rubber balloon method and a nuclear gauge (type loading (EV2) was determined in the centre of each individual sub-field
“Troxler 3440”). The rubber balloon method was used on each testing (one static plate load test per sub-field, this means two results per
date and testing was performed in each sub-field of the northern and testing date and material) according to German standard DIN 18134
southern areas in accordance with the German standard DIN 18125-2 [42]. A static plate load of 0.3 m in diameter (thickness 25 mm) was
[39]. On the first testing date, two tests with the rubber balloon method used in each case. The load plate was set on the level surface (if ne-
were performed in each sub-field of the northern and southern areas cessary on a thin bed of dry middle sand) and the test setup was ar-
(four results per material) while on the other testing dates only one test ranged properly. To measure the settlements, a single dial gauge was
with the rubber balloon method was performed in each sub-field (two placed in the centre of the load plate. After preloading of the load plate

25 100
Air temperature 0.2 m above surfa ce at test site
Pre cipi tation at test site
20 90
Air temperature 0.2 m above surfa ce at surr oundin g wea ther sta tio ns
Pre cipi tation at surro unding weather sta tion s
15 80

10 FI = 103 70
Precipitation [mm]
Tem perature [°C]

[°C x days]

5 60

0 50
4th testing
2nd testing

3rd testing
1st testing
construction

-5 40

-10 30

-15 20

-20 10

-25 0
12.10.2017 13.12.2017 13.02.2018 16.04.2018 17.06.2018

Fig. 5. Weather data from the four weather stations, located approximately 11 km, 14 km, 19 km and 35 km around the test fields and virtual weather data at the test
site.

5
S. Huber, et al. Transportation Geotechnics 22 (2020) 100305

Table 3
Summary of the tests performed at each testing date.
1st testing date 2nd testing date 3rd testing date 4th testing date

Sub-fields LS 1-1S, LS 1-1N LS 1-2S, LS 1-2N LS 1-3S, LS 1-3N LS 1-4S, LS 1-4N


C&D 1-1S, C&D 1-1N C&D 1-2S, C&D 1-2N
LS 2-1S, LS 2-1N LS 2-2S, LS 2-2N C&D 1-3S, C&D 1-3N C&D 1-4S, C&D 1-4N
C&D 2-1S, C&D 2-1N C&D 2-2S, C&D 2-2N LS 2-3S, LS 2-3N LS 2-4S, LS 2-4N
C&D 2-3S, C&D 2-3N C&D 2-4S, C&D 2-4N
Rubber balloon 2 tests/sub-field 1 test/sub-field 1 test/sub-field 1 test/sub-field
Nuclear gauge 2 tests/sub-field 1 test/sub-field 1 test/sub-field 1 test/sub-field
Static plate load 1 test/sub-field 1 test/sub-field 1 test/sub-field 1 test/sub-field
Dynamic plate load 2 tests/sub-field 2 tests/sub-field 2 tests/sub-field 2 tests/sub-field
Grain size distribution 1 test/sub-field 1 test/sub-field 1 test/sub-field 1 test/sub-field

(0.01 MN/m2 for at least 30 s) a loading/unloading/reloading sequence results of the northern area with the results of the southern area).
(0.08/0.16/0.25/0.33/0.42/0.50/0.25/0.125/0.01/0.08/0.16/0.25/
0.33/0.42 MN/m2) was applied. The single load steps were applied Results and discussion
uniformly and continuously each within 60 s and each load step was
held for 120 s. Subsequently, static moduli of deformation were cal- Dry density
culated using the procedure described in DIN 18134 [42] from the slope
of the secant through the points corresponding to 0.3 ∙ σmax and The initial relative degree of compaction of material LS 1 was found
0.7 ∙ σmax (EV1 from initial loading, EV2 from reloading). to be between DPr ≈ 94% and 98%, for LS 2 between DPr ≈ 93% and
The dynamic modulus of deformation EVd was determined using the 100%, for C&D 1 between DPr ≈ 96% and 101%, and for C&D 2 be-
dynamic plate load test (Light Falling Weight Deflectometer, Portable tween DPr ≈ 94% and 99%. The measured dry density of each material
Impulse Plate Load Test Device) according to TP BF-StB Part B 8.3 [49] directly after compaction and at each following testing day is shown in
again using a plate load of 0.3 m in diameter (thickness 20 mm). The Fig. 6 (note: a mean value is shown in cases where more than one test
load plate was set on the level prepared test surface (if necessary on a was performed per sub-field). The dry densities are depicted separately
thin bed of dry middle sand) and the loading device was placed on the in each case for the northern (ending “-N”) and southern (ending “-S”)
load plate. Then six drops with the falling mass (10 kg) were carried testing area for each material and, with a few exceptions, show good
out. The first three drops were used as preloading impacts and the next agreement. The dry densities determined by the rubber balloon method
three drops were used for determination of EVd. EVd was determined at (“rb”) and the nuclear gauge (“ng”) on the first and last testing dates
two points of each sub-field (four results per testing date and material) correspond well for each material. An influence of the soaked area
and the mean value of these two measurements per sub-field is given in below LS 1-S on the dry densities achieved in the compacted layer in
the evaluation below (see Section ‘Dynamic modulus of deformation this area cannot be deduced.
(EVd)’). When comparing the results of the rubber balloon method and the
Samples of uncompacted material (taken from between the lanes) nuclear gauge, however, the differences between both methods should
were obtained at each testing date for grain-size analyses to quantify be considered. With the rubber balloon method, the density is de-
the effect of particle breakdown due to frost action. termined approximately in the uppermost 0.2 m of a compacted layer.
The selected procedure of dividing the lanes into northern and The dry densities measured with the nuclear gauge represent mean
southern areas and these areas into individual sub-fields allowed for values from three measurements at different depths (0.05, 0.15 and
double data sets (replicates) for all of the materials (except the crushed 0.30 m).
limestone LS 1 in lane 1 (soaked area). The dispersion of results can The data illustrated in Fig. 6 indicate in most cases a trend of de-
therefore be seen from the figures presented hereafter (comparing the creasing dry density for both limestone and C&D materials, especially

2.2
LS1-S,rb
LS1-S,ng
2.1 LS 1-N
LS 1-S LS1-N,rb
LS 2-S LS1-N,ng
2.0
LS 2-N LS2-S,rb
Dry density ρd [Mg/m³]

LS2-S,ng
1.9
C&D 1-N LS2-N,rb
LS2-N,ng
1.8 C&D 1-S
C&D 1-S,rb
C&D 1-S,ng
1.7
C&D 1-N,rb
C&D 2-N C&D 1-N,ng
1.6 C&D 2-S C&D 2-S,rb
C&D 2-S,ng
1.5
C&D 2-N,rb
C&D 2-N,ng
1.4
22.09.2017 31.12.2017 10.04.2018 19.07.2018

Fig. 6. Development of dry density determined by the rubber balloon method (rb) and the nuclear gauge (ng) over time.

6
S. Huber, et al. Transportation Geotechnics 22 (2020) 100305

during the frost period in winter 2017/18. This loosening of the par- the third testing date (areas LS 1-N and LS 2-S and LS 2-N). This is
ticulate structure of the compacted surface can be attributed to the attributed to the decreasing dry densities by the third testing date due
influence of weathering, most probably in the form of phase transition to weathering effects (see Section ‘Dry density’). A lower dry density at
of the pore-water from liquid to solid and vice versa. This process is the surface indicates a looser grain structure, which leads to lower
cyclic (at least during transition seasons there are low temperatures at stiffness and thus lower EV1 values. After the third testing date (after the
night and warm temperatures during the day) and is expected to loosen frost phase), the EV1 values remain almost unchanged, as do the dry
particle contacts. However, this process is limited to the uppermost part densities (see Section ‘Dry density’).
of the compacted layer (see Fig. 7). Between the third and the fourth It is interesting to note that an increase of stiffness over time was
testing date, no more temperatures below freezing point were recorded recorded for the southern area of lane 1 (LS 1-S), where the planum
(see Fig. 5) and there was almost no further significant loosening of the showed low initial stiffness (soaked area) and the compacted layer
materials (exception: C&D 1-N). In half of the cases, even an increase of thickness was only between 0.3 m and 0.4 m (see Section ‘Design and
dry densities was observed. construction of the test fields’). Beginning from the first testing date
Fig. 7 summarises the dry densities determined with the nuclear (EV1 value in the southern area was well below EV1 value in the
gauge on the first and fourth day of testing (before and after the frost northern area), the EV1 values in the southern region of lane 1 increased
period, note: a mean value is shown in cases where more than one test from sub-field LS 1-1S to LS 1-4S, until LS 1-4S reached a quite similar
was performed per sub-field). The dry densities are shown for each level like LS 1-4N at last testing date. However, this increase cannot be
material separately for the northern (ending “-N”) and the southern seen as an increase over time, because the stiffness of the planum
(ending “-S”) sub-field, and again, they agree well for all materials at gradually increased from sub-field LS 1-1S to sub-field LS 1-4S and was
the respective testing dates. In addition, no clear differences can be comparable to the stiffness of the planum below LS 1-4N at the last
observed between limestone and the C&D materials. The dry densities testing date (see Fig. 2). Moreover, the compacted layer thickness was
shown in this figure are the individual results obtained with the nuclear not constant in lane 1 but increased from 0.3–0.4 m to 0.5–0.6 m to-
gauge at different depths. The figure clearly indicates that the decrease wards the northern end of the southern area (i.e. sub-field LS 1-4S).
in dry density was mostly constrained to the uppermost layer of the Using a plate of 0.3 m in diameter, the depth of influence of static plate
compacted materials (irrespective of maximum grain size). With in- load tests is approximately 0.3–0.6 m according to various authors and
creasing measuring depth, however, no systematic decrease of the dry the respective Austrian standard [15,1,24,23,3,61]. Therefore, the in-
densities could be observed. This is due to the fact that weathering and fluence of the stiffness of the subbase on the measured values of EV1
low temperatures affect in particular the near-surface areas and is in decreased as testing proceeded from sub-field LS 1-1S to LS 1-4S. The
accordance with the estimated frost penetration depth of about 0.4 m increase of stiffness over time for LS 1-S is therefore predominantly due
(see Section ‘Field testing methods’). Long-lasting temperatures well to the increasing thickness of the compacted layer as well as to the
below freezing, which could cause the loosening of even deeper areas increasing stiffness of the planum from sub-field LS 1-1S to LS1-4S (see
by frost, were not measured during the measurement campaign (see Fig. 2 and Fig. 4).
temperatures in Fig. 5). By way of contrast, the two recycled materials C&D 1 and C&D 2
show increasing or decreasing EV1 values in the period between first
and third testing (winter). After the frost period, however, EV1 increases
Static modulus of deformation on initial loading (EV1) consistently both for C&D 1 and C&D 2. In particular, C&D 1 shows a
significant increase in EV1. This increase in stiffness is expected to be a
The static moduli of deformation on initial loading (EV1) as de- consequence of secondary hardening effects in deeper parts of the
termined on the surface of the individual sub-fields are shown in Fig. 8. compacted layer, which were obviously dominant compared to the
With the exception of LS1, where the southern part of lane 1 was partly superficial loosening effects shown in Fig. 7.
constructed on the soaked subsoil (see Fig. 2), the EV1 values de-
termined on the northern and southern sub-fields show good agreement
for all other materials (LS 2, C&D1, C&D 2). For the natural materials,
the stiffness on initial loading (EV1) tended to decrease over time until

Dry density ρd [Mg/m³] Dry density ρd [Mg/m³]


1.6 1.8 2.0 2.2 1.5 1.7 1.9 2.1
0.00 0.00

0.05 0.05 1st testing

0.10 0.10 4th testing


Measuring depth [m]

4th testing
Measuring depth [m]

4th testing

0.15 0.15
4th testing
0.20 0.20
1st testing

0.25 0.25 1st testing


1st testing

0.30 0.30

LS 1-S LS 1-N C&D 1-S C&D 1-N LS 2-S LS 2-N C&D 2-S C&D 2-N
0.35 0.35

Fig. 7. Dry density determined by the nuclear gauge over measuring depth – left: LS 1 and C&D 1 (both 0/32 mm), right: LS 2 and C&D 2 (both 0/8 mm).

7
S. Huber, et al. Transportation Geotechnics 22 (2020) 100305

80
LS 1-S LS 1-N

Static m odulus of deformation Ev 1 [MN/m 2]


LS 2-S LS 2-N C&D 1-S
70
C&D 1-S C&D 1-N
60 C&D 2-S C&D 2-N

C&D 1-N
50

40 C&D 2-S
LS 1-N
C&D 2-N
30
LS 2-N
20
LS 2-S
LS 1-S
10
measurement
on soaked area
0
22.09.2017 31.12.2017 10.04.2018 19.07.2018

Fig. 8. Development of the static modulus of deformation EV1 on initial loading over time.

Static modulus of deformation on reloading (EV2) loosening during the frost period of the winter of 2017/2018 (see
Section ‘Dry density’). Since the superficial loosenings are compensated
The evolution of static moduli of deformation on reloading (EV2) during the initial loading for the determination of EV1, EV2 is influenced
determined on the surface of the individual test fields on the respective predominantely by secondary hardening effects of deeper areas and
testing dates is shown in Fig. 9. Again, the results from the southern and thereby increases significantly over time.
northern sub-fields are in good agreement for all materials (except LS Comparison of the available data (dry density, EV1 and EV2) strongly
1). The data shows that the stiffness on reloading (EV2) of the natural suggests that the dry density of all of the compacted materials in the
materials LS 1-N and LS 2 is practically constant over time (no marked uppermost layers is decreasing there due to weathering (rain and frost
increase or decrease). The stiffness increased with time exclusively in action). At the same time, secondary hardening effects take place in the
the southern area of lane 1 (LS 1-S), where the planum showed low compacted layers of the C&D materials (C&D1 and C&D 2), while they
initial stiffness due to the soaked subsoil and where the compacted do not occur for the natural materials. As a result the EV1 value of the
layer thickness was only between 0.3 m and 0.4 m (see Section ‘Design natural materials (LS 1 and LS 2) decreases due to weathering (super-
and construction of the test fields’). Again, the increasing stiffness of LS ficial loosening). Because the EV2 values of the natural materials are
1-S from sub-field LS 1-1S to sub-field LS 1-4S can be attributed to an practically constant over time (no secondary hardening effects), this
increasing stiffness of the planum and a decreasing influence of the weathering does not seem to be substantial (and its effect is apparently
stiffness of the planum on the measured values of EV2 as testing pro- compensated during initial loading). In layers constructed with C&D
ceeded from sub-field LS 1-1S to LS 1-4S, away from the soaked area materials from construction and demolition waste, both effects (de-
(see Fig. 2). crease of density due to weathering and secondary hardening) are ex-
The measured values for EV2 of materials C&D 1 and C&D 2, on the pected to occur simultaneously. However, the influence of strength
other hand, show a substantial increase over time despite the superficial increase due to secondary hardening effects seems to compensate for

400
LS 1-S LS 1-N
C&D 1-S
LS 2-S LS 2-N
Static m odulus of deformation Ev 2 [MN/m 2]

350 C&D 1-N


C&D 1-S C&D 1-N
C&D 2-S C&D 2-N
300

250
C&D 2-S

200 C&D 2-N

150
LS 1-N
LS 2-S
LS 2-N
100

50 LS 1-S
measurement
on soaked area
0
22.09.2017 31.12.2017 10.04.2018 19.07.2018

Fig. 9. Development of the static modulus of deformation EV2 on reloading over time.

8
S. Huber, et al. Transportation Geotechnics 22 (2020) 100305

superficial loosening effects due to weathering even for initial loading already achieved EVd values equal to those of the coarser-grained nat-
(EV1). For reloading (EV2) the effect of superficial loosening is also ural material (LS 1). From the third testing date onwards, higher EVd
compensated during initial loading, and therefore secondary hardening values are achieved with all C&D materials than with the natural ma-
effects are all the more dominant, leading to an increase of EV2 values terials. The distinct increase of the EVd values for the C&D materials
over time. These joining effects of superficial loosening, secondary over the testing period is again expected to be due to secondary hard-
hardening, and recompaction during initial loading (EV1) typically lead ening effects of unhydrated cement components. While the final values
to increasing ratios EV2/EV1 with time for recycled materials from de- of the coarse C&D 1 material were still about three times their initial
molition waste, which already do exhibit high ratios EV2/EV1 directly values, the sharp decrease between the 3rd and 4th testing could not be
after compaction (see [56]). explained.

Dynamic modulus of deformation (EVd) Particle breakdown due to frost action

Fig. 10 shows the evolution of the dynamic moduli of deformation Fig. 11 shows all the particle size distributions determined for the
(EVd) determined during the testing period (note: a mean value from materials tested on the respective testing dates. The particle size dis-
two test results is shown in every case). The EVd values obtained on the tributions of the two natural materials (LS 1 and LS 2) are given in
southern (ending “-S”) and northern (ending “-N”) sub-fields at the Fig. 11 (left), while Fig. 11 (right) shows the particle size distributions
respective testing dates are again consistent for all materials (exception of the two C&D materials (C&D 1 and C&D 2). In particular, for the
LS 1). At the first testing date (immediately after compaction of the finer-grained materials LS 2 and C&D 2 with their maximum particle
respective materials), significantly higher deformation moduli EVd were size of 8 mm, the particle size distributions determined on the in-
measured for the natural materials (with the exception of LS 1-S due to dividual testing dates hardly differ from one another. Changes in grain-
the soaked subsoil) than for the C&D materials. In addition, for both the size distribution are also listed in Table 4. The data indicates a high
natural and the C&D materials (exception LS 1-S), higher EVd values are homogeneity for both materials (LS 2 and C&D 2) with regard to their
achieved on the coarser-grained materials (0/32 mm) than on the finer- particle size distribution. It also can be seen that no reduction in the size
grained materials (0/8 mm). of the particles occurred due to the influence of freeze-thaw cycles. The
As a result of the measuring depth of the dynamic load plate, which grain-size distributions of the two coarser-grained materials LS 1 and C
is between 1 and 2 times the diameter of the load plate (0.3–0.6 m using &D 1 show a more pronounced scattering. Nor could any refinement of
a load plate of 0.3 m diameter) according to several authors the materials due to freeze-thaw cycles be observed. For C&D 2 the fines
[47,1,2,24,3,61], the influence of the soaked area of the planum below content even seems to decrease during the observational period. There
the southern part of lane 1 is again clearly visible from the data ob- is no plausible explanation for an increase in fines and so the relatively
tained in sub-field LS 1-S. The area again displayed significantly lower minor differences in fines content may be attributed to local variations
EVd values compared to LS 1-N. of material composition.
Despite the decreasing dry densities near the surface (see Section
‘Dry density’), the EVd values for all the materials tested increased Conclusions
during the winter of 2017/2018 and the trends generally accord with
the increase in the EV2 values shown in Fig. 9. A decrease of the EVd This study reports on the behaviour of two processed materials from
values due to surface loosening, such as that observed for the EV1 values mixed construction and demolition waste (C&D materials) and two
of the natural materials (see Section ‘Dry density’), was not observed. natural materials (crushed limestone, LS) used for applications in which
This is due to the fact that the dynamic modulus of deformation EVd was they are exposed to natural weathering in the form of water and frost
determined after three drops of the falling mass (preloading impacts), action (e.g. road shoulders, unpaved roads). The test fields were con-
as suggested by TP BF-StB Part B 8.3 [49]. It is assumed that these structed in November 2017, and field tests were conducted several
preloading impacts effectively compensated for the loosening of the times during the winter of 2017/2018 and the early summer of 2018.
compacted materials due to weathering near the surface. The parameters monitored for the compacted materials were dry den-
At the second testing date, the finer-grained C&D material (C&D 2) sity (rubber balloon method and nuclear gauge), load-bearing capacity

120
C&D 1-N, C&D 1-S:
errors in the last
Dynam ic m odulus of deformation EVd [MN/m 2]

measurement?
100 C&D 1-N

C&D 1-S
80 C&D 2-N

C&D 2-S

60

LS 1-N
40 LS 2-S
LS 2-N

LS 1-S LS 1-S LS 1-N


20 measurement LS 2-S LS 2-N
on soaked area
C&D 1-S C&D 1-N
C&D 2-S C&D 2-N
0
22.09.2017 31.12.2017 10.04.2018 19.07.2018

Fig. 10. Development of the dynamic modulus of deformation EVd over time.

9
S. Huber, et al. Transportation Geotechnics 22 (2020) 100305

100 100
1st testing 1st testing
90 90
2nd testing 2nd testing

Percent passing by weight [%]


Percent passing by weight [%]
80 3rd testing 80 3rd testing
4th testing 4th testing
70 70

60 60

50 50 C&D 2
LS 2 C&D 1
40 40

30 LS 1 30

20 20

10 10

0 0
0,01 0,1 1 10 100 0,01 0,1 1 10 100
Particle size [mm] Particle size [mm]

Fig. 11. Particle size distributions determined on the individual testing dates – natural materials (left) and C&D materials (right).

Table 4 perform over the long term compared to natural materials when the
Gradation of the base material compared to the gradation samples taken on the compacted surface is run over regularly by wheels (during wet and frost
individual testing days (cumulative). periods).
Fraction LS 1 LS 2 C&D 1 C&D 2
Declaration of Competing Interest
Base material < 0.063 mm 8–9% 9% 6–8% 8%
< 2 mm 28–29% 40–42% 29–34% 61–62%
The authors declare that they have no known competing financial
Data from all testing < 0.063 mm 7–10% 8–11% 2–8% 6–10%
dates < 2 mm 26–39% 38–47% 23–34% 57–62% interests or personal relationships that could have appeared to influ-
ence the work reported in this paper.

(static and dynamic plate load tests) and particle breakdown due to Acknowledgements
frost action (particle size distributions). The following conclusions can
be drawn from this study: This report is based on a research project funded by the Bavarian
Research Foundation, under research project No. 1135-14, as well as a
• Weathering (especially in the form of rain and freezing tempera- research project funded by the Federal Ministry of Transport and Digital
tures) leads to reduced dry densities at the surface of both the Infrastructure, represented by the Federal Highway Research Institute,
compacted natural and C&D materials. As a result of this effect, the under research project No. 05.0194/2016/MGB. The authors are ex-
stiffness on initial loading EV1 (static plate load test) decreases clusively responsible for the content.
during winter periods. One practical consequence of such an effect
observed on all of the materials is the possibility that track ruts may References
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