Qualitatia dralys

Qaualitatie nalysu involreadteclio ohcalñbno

anien
ska salt/ Asysttasaedott
JhAytematic pkeckéuehainvelus 4olleting ua
GA iPliminay tut usel aad tadtieax
sIiLet tos qel anienk
3GA ib Let tost hor catiesk Calioed bapc hadicals

Prclininany tust
A)hyical examination e sat/mbctihe
iColeuk Stunc
Blus Bluik tuu Cut
NR

Liog Fe
Fe
pnk Co
ight jnk/b/Llsk Mu Lelid)
almest celeh Mn (aguGu)
yelle Fe 3
 colstukadaali Alstsing-dalo
sa,PT- d B L deadiol dus to Satouautt
Date L
t)
i Smal Sngetunte
ammenlacallcharacteeistit odeu NH
C Co0-(acdai)
vinagah liks jnul
Jotteso rulLHS)

lideltutscntHyghoxcofi ratuu
celoussd Aoalfheting deliamACIce ed
Crmetly
tut calsuuo
Ca 2

(8) yy hsating fut

cotaudutdguhteig , Limasatn uly
Cogaa uesed c o H t O

colouslus ga soten sg Lmall kgdatud

AulphidlJbiulfhids
colounles gal uacatiy/ elholieg So HS0
AmalSo

H9+-Pb PhSHodk)
H,S+C GS lle)
Celeunlox gasR
ho acidilies K,
dt RA
celsehla urgr(H)
ungont Amull hydratad chleid
 ate
glakhsd dipd n NH,C hauglt
clase dulk wtbit uma o oGnad
HC, HC, HI
Celoules ga witl vugoh Lhe :acdde ion
Nmull

CBloukloss gs wth chahacteutic sdoul NH

dmunenig
KlgI Nosbs Raagot
Qmmei gob heait wt Nedong
aagtt te guwt

Celouhaol gos AU aht pug)

pals yullo FT
guwiulh-yelle gal CCLo
Rrdde-auh/thangeArd-B1)BA
Nielt
(gaves Huie Hack coleuh nstakc sel").
Raddul ban(N0 0 NONOZ
B r h r oret 1odid papo tHu-tHouk
ubst OA, t can convet1 I
guwe blur slauk cslsusi wth Maucl
Limpce Pelusity isdidu pop
o,+ 0 s t disphopot
,K04 KMnOat
(pustpla gt) Blhuk
KCrOp+ Ca,0+ 0,Tchaye
MnD
 NHNO th calauthud old
oly ibddas a otmad mainly hy -blol doyato

Ohuating. alt cuollu to a velurinoutmak

elles twha ist and t i t wtar cold Xn0 (Zn

Bhsw wrtiav hst and yclles wt cold PbO (Pb

Oial salt Mut becemal httebe u CO5H0

n t btames blut adolisg ulale

iginal salt gitso belte uthie Fe 90 5H0

ecsm 6 adding a b l

MCO Metal ide +Co

eocutptNa, Co K CO3, Rb, C0, C Co)
doult daCempe on haatinp

ti NHC NH+ Coi Hh0t

MNO, MOxiol 0
tacap Nand KNO,,RbAN03, CNO

MNO+0 Na 0+Na +02

Nounal 0ide

ttNA,NO NOFHD
 Hast stalls 0. rtegn it O
Feo &uldenourudFe,E, FeoaCohc
NH, NO, H u t
dypr 101H0

pid
(ubah) NH4 NO 1 + H,01 haadse

NaHCO Na 0, + co, t H,O

FeSO Fe,0, t S0, +90,

4), Cx0, C0, 1. t H0
Pange caleud
NH NHT+ H0.1

(NH),SO NH,1Hs SO,

(CChauceal Cauity Jet
Mdallit cotleratt uhu Aaatud ioo chacaal taitiy
dicomposu te guM c pording snidu
JA idu sdontinaa oppuol. au Ccaloadidus
Sn berntgthil colts, th odid getmalndbge
Auduclie fetming mitbl Jrad. 2cals (celesy

ZnSO, No0,
caltQhalepped
to l
ZnCO, Zn0 Xn0 +0
yellas
E absexsalines Pb*
guy bead hick manks tha paser Po-
radlucals a Hetmd Cu Cu
 Hbopding not 4heun lalge alam Date 18e5 2

M PLgay Cu hud
Cauly

(D Csbalt Nithat Jest / Blespip tst

AB, Celouhs of ion ahe sten Lit ahen't enpecttd te,Celp
huidu sltaind c m CC ut wtit jw
caYeu th odol duep st cebalt nikat
slutie and bhrat coleuhed a s s h obtained
indicali setm metal ient u n t
Rirgmarns grau)
(Jharasd Mue)
lu mas Ce0 , 03-
pink mals Co0 yo
Juuilsit mak Co0 SnO Snt

ecess cobalt sizbat u nt adaled becawe bladk

bead sltained and ustuing i derttkiud

(Elam tut
Leleuh lam

imsen Rd S b
eldatr 4ellen No
LilacUV islut K
Byrich Ra
Cu
 Onidising Alom(Nov lumtrous Hona)

Raducing Pount of man

tnf (of t ho
klame Poiut ot min m
(Auphirous famt)
to max tmpelatuua liA in idustug qlom

(EBoxax head tat

Na,0-10O Na,C.0,aNa60,1+,0
bransparni
ghy kead
Gn haaliny wit a anilienmdal salt, celsulad
mda-bkhtu ake obtained oxidiing 4larnt ard
colouksolmtalu ake elbtainad u hukucirg hm

GusO Cu0t S0
Cu0 t60, CuCe0)L)
taok
Howeveh n heducing lame
Culmetal eltinsd and hd bead etna

Cg t2 always blu rad

hy gusskad
Celeus ahs ften CA Cu 2
NO NO NO NO
No,

SP
180 132

NO NG) NO NO
 GuSO4 KI
K,S04 GulI+ dalz/Is
yules Jre (4
pmd s KI JelueDate 9 sT 2
Taksu m endCRA
E Soluliity Chad
CO HC0 ALL caltlornates ae hatn inlslurh
encupt thast o g 1 and (NH), COg

AL icarbenatu akt uot zeluble-(NaHCO A takigiy

ppL elubilit inuOARA dou tha (biarb)
2elubilat decHeases dewn h
all i-ol ake elubl)
So2 all Aulphitu akt nites iuselulle exct
the o 4 1ad H), S03
ALL lphidas aht watth inselilbla except the

NO U nibits ae ate elube enczpt o

CH,COO U acetates aka iatk selublk_enapt

CHCOCAgand CHh CoO2 Ho
C Met chlouides ak wnt solube excokt
laCe PbC4lubla_iuhot wat), H,
CuCt O1O& SbOC

6A Hest bremides akt andoh.soluube excepl

eb (Lslubla in. hat wateh ). Hg Br,Cur

AL
iedidas a ntok Aslubu _encapt dg I Pb
H u l BIL,
wtub pot
 Vonadins, Jitnriumn, Sh, Bi tolm mo cako und Loua othaa

6rocL, SbOCt hauy whih pp Date

So tost sulphats a ppt Sr50, PbS0,
GaS0, CakO, HaSo O
Aaingydatusbla
Po Most phephataso 4pt q,Fo, Ea,l
Pe, (eD AeD), Fetko aehy
NO, LL nibatu ase ut selubla

2Nibates Phephalsaburdoesy cotils Lst

TwtJest Arise
ater ibact WED andNaCO, bact (SE)
WE Salt dsound in disillud wab and e
Lolilinn eltaind eallud WE
SE wd uhn snlt u partially selubl/inuehdbe
Jn iath e catins otut salt inteoras a t the
t t e anien e c d i a pAoducu se dark cslauhad
Lolutiba that fus nf arien 0 net cleat
hufaxaliei Jak 1-2gm salt/8alt min ad ths
Tims t am puha old NG co
a Hash ddd 20m o distilld wat and

Coel th
and th ilbaAslu
itrat ostainad icollad sodiuh tordenat extrat
 Date 11 2

BaCl + Na,CO +2la C

Ba C0, 1 og)
salt to be)
Gnalysed
Net A SE Crtains excA o t t d easily
No,
it sheuld bt naudraligad widlhco3a duitabe aid

be ocuudig e t t ustoanienk
(A)insn shicl evolue gas t t dil HC/ dil HD4
(co, S0, 2 NO C,Coo

Jest 1 A HC/H, SO tot

csleulus,sdousus g0 t i bisk ehloeescernu
i ebsenwed (ising ound
CO+H Col+ H.O
Jest2 Limusath /Baxyta wto ost b
gas olutd utns dimaunelbi. / batyta taat mlky ludik

CaloH)/Ba(oH), +CO CaCO +HO

HO
Gaco,
Crulkirans
21pan pielenged paug gas, thheugl abe sl,
itkinass dbkapprb seckula ot kelising n.
CO++Co +H 0 CaHCO)
Selube (mlkinak disata
 Millin N0apLak nbeilirg ekaddingLunasol
oka.ddig Aormtamneria Otitionhmbues auidi
H
CoHCO), CacO+ Co,+ H,D (hsrnaval of tump
hordrasso uat
ethe tus precsA eLLd as aticdic H o Sicatlenate
honetd and Gco Matprahs
Jest 3 N/a/z"/C Leluilion fetmud due
t hydslys
whide tomindhuha ok MCO and MloH), end

Jest 41 No,spluiims
uhida tpt oh gCo, erad, uhiclh i elubl
in iNH, seluti and diHHO
to du to homaf WA Rem SA
du cemplor kond)
ard Agnio, u iuble a t

ft betene yllae/ btautn n beilirg

Ag 00 be:lAg.ol+c
tyaio fiveno
Juts Hg olutiom Iasic mtuiu sonb6nate

Jst6 Phenelphthalein
Phenelththalti tuuns pik by seluile
Couberats but xamaina celoulbs d i Lelubl
bicrbonatts
 NaOH, No,CO%, NaHC0
in kudee chaugat, S' >so, (pottly)
Nek elubkbicanberatus gue wAi ppt di g0
JEG
gnly on beiling
So
Jost 1 i HCLHSO tt
a coleurlu gas t ullacating edsute u e l u d
w t eisl elreAMCnC
sO +HSO, (a) S02 HO+ S0, T
Jest2Acidilind k,Cr 0,lkMnD, s t t
dehitien n g u o pick sleuh oecolsunises
apreducing G 'and So
S

Cr 7ta+So
d MrDt +H*

st tauo Jodata et
Blur-Lbk Celouh taintol dus te fotnation o I

IOg+S0790,+H* I , +S0

Atah Spaliou n t
didtae
et 7 an0 Nel

Ag-S0-S0f Rse,fs
(Pauk pë (het diprope leua aol
 Basa, poltially d selule un ect Cond (bod, Cou pHO
BasO elub w dul HCe
xallust uduug agud n elovuntasRao 2
Jest3 ktmattl, /Baujtaaauk test

,tBa"/Sx/PhAaluidi
sLt Bas0,/S S0 PbCo1) founad
iar6aSa,, n 4touding uaming witk Steni a h
Conc HO /HLO
RKSO, buill get exidlisnd ta wie 4uta BaSoe (inseluble ja
dal- vninual acida)
Jet5nt H S0, tast
HS gat evohed lulh
SOs+Zn+Ht H,9T Z+ H,0
ost6 Sooluu KtHopuide del
Heed xud colouraltitea elitainad
(aluadeyMad Lelkkcemts moe kd

S
otL AHCH S04 ust
elouelask pes t Hetien gs Amll is obinad

SHS0 HSTSo2
TetP/CA 1olhiie
Gauk (ylls pt PESTTS othinad
 Lf 6uNcidijiud KC, 0, /KMu0, 4ol
SsZues gltt/drceaukisus te g G/M
alaguk ailphuak (0 odatias t yelle ) se
t Sodias Nitopeuskideusta
Na Sr Na[reCCRro)NaecNOS
nen- ubx) purpla uislt colsuwnat
his tut is hathou by HSa) HST d
to La Scec
Heveu h mdhuin umade baic, ths abeue
ust ksheshs

a NO seluilio utus
dack pt S erad,

est 5Mthyane Bha aa

ONN-dindttytparapkncytizdibmint oRt
yFecls aud HS i stengl audii Lelutton
te a atek saluble dylitt Malhylt ue
tPblon P S tait
iNO
est1 HCJ,So, tst
a celsules gas eusluea (NO)licl tuns
kersu ehia cou in Cotact tuitt aih (NO,
N+H HNO
Luntalde pal blut is)
unitant)
found NO H.O

el phast NO 0 NOT
tPaona){paBama {paanag
 So+HS
(aligtiyg colsukad pat)
Date 6

at3Starck Jadidt st
Bluurblasd ttlau ia obtainad
NOIH 1+ND

t seluitits
Lahith phacipilat en temas
est n/alNaOH
RA
NL (9) i euglutal oiti Za A

Test SBxe ig tut obseruedcatia

(net praunt i PE EaS9
Lwh NQol adaud cakulully s à ceucl
Lelulie s FeSO acidikiud isttdit aati
auid/dl G, a bra ung ahpaht at h
juunclieso tiweli
Ksmatinas biocs celsciaties slexuead
NO H HO
3HNO HelOs2NC H 0
Fe $o +NO +5H0 Fe O5 NO1SO,

8M
 Vest 6huewea tut
NO H HNO
HNO, NHL, C SlH N,+ HSCrlt H,0
Ahdssapnic aid

Tecky +3FISCN FeCw+

2t

kst 7deidijad KMaD,laiudikiud k, Cr,O, sel

pirk colouh gts decolouwsadk,C0, Tinsian
Hotening M aleung uitt NO
(CHCoo-

Jest LaAd HC/H.SO4 tst

inga Li mal i obtaind cdsbe (CH,coOH

Jot2h NOg el
i ppt e CHCO0dg omad whicl
uadilp Aslul-iaNH,iel

est SNeibhal Fel ust

deup ad celouation w ebtauaoldut to founalisn

tfeg (o,CH¢O0% fwe-hdo

w h Lo s dil wilh ate aud boilo

Ppt CH, C00 ba oue

huddulcm oF OH), Lttat
 peoleliak bionAP elo), CH,coo
obtained 9basic nicacilalo

oith Conc ,SO

Anions hich evolego
Co NO
Cgmanen lsA tor halede ienA A
co Te

( Cenc Hso at=

HO, Br 4 qasosano 2ralord.
coloun k Pddhsk

HCo ve4Gs0d do
t does molnyast
 C , tH,O HU HOC
ale
Sownd HOCe H&* nu bleocgand /Fu

He PAt Addutssyella Ond bdneib

C6)MnD,inDLOHIt cmcH,k e A A kO Od A A:D
enaMa.lalon9lthn

Na Ro2Na, Aro, paelasey

dicm0288muk odium anala
n
ganak
Opap ond hlaachs
yallas gaa, lock
stanch iodielapapea la/hlack Ld) PENDG4o PLu1Phb
hifekije bghtyss ppt
Ba adosh baen 9aa blacb me
Llenandpape aens taack iedid -
Po and P%lr, ouAolunainhetisat
aaa ue Lhlack ad ahedutta
áranglxed spatal enutauck papa
terK, Cr0,ut cenc H,sO tat
a C salttK,U CxO
inlet vaau aaducss blueblack Sld ,so 5chve
caleunih tacRap Chiaud.
HD aoilabla z heba
LO BaND, sol
kta paleyellesght yullanappt:a hO, Na
DHlag Na Cxay Nh C
osol
Na CxO, Lag)t Pena"Ag PhLalc0, If
Aalukh an dlag NH
i akally solukla n dag NH
but adl solue n Cenc: "N Note )losalublh C haasy mala C ndcoela-t C
htlyoluble in conc NH so
2Ba1
Sn Ba OPh0,H Sn Sb,Ha
Ix. 6deng di HN et
toxrmig ha NH

tNLCN ad yfpa col paducsd alenq ith

darmingHjC ede2020/08
 Lahsdayp nsdaaaa
Br tum e a g a t 2sd
athaee aciel
aed-violet
24, O H,Co 2HU
CO
2) NO, itat)
CR
a_Cont o at
nddishbbdn20-oa g
ECrganic layeteitBChlaxintotudnat= ermladalong ith
NO nd O
So
B
0ddlidn lusningaA
.1 dhaddishbro
/4tCuCs,lCH ane iokt _celen inteknias the
bro
slutiaehaddish
obiaint
Oaniclayex +NO + C

Note Cn ss thlaise 2aln itk tHNR CotiNo tH,o

Br me ndapala
ylaasolad alainkd pella

AlHaaliaely Arellien a d b gaa

inlanailis addinqpinckale no
celaunlass ol H10 fomad i adicatad
haa

2 Foxr tealin bsamaneA Acon alaa

6Bx0n un test=-
be und instaad a claube oati
bulcAnd H,SO aicaadaa bau
Lg Eluorásecintest

taooldios eAuiaham acid

 and thah n tan HNO
buaDning teat LRRT)_
Note 1 RRT ahauld met ha paanda
bce ty daalhe Notpi kia lest alsitn and anioi
ND
u) Anionggkichda o olieaeve
m.eutslaschpap henbsaght Lenaa
So PD B0
r g e d spt on stoehpapAaL
lac
0
anck aadioe papan bakt
L2ihthe Laog044than ND ge
blehlaek celass faalua cempasid a- skihRat Baso 5 mad
nco No aestan cid Baso alial solula
Hubsing càncHS0
m Ba
Leeladd alog E Pb o
Pbso, ad huc s
aApl
selu noneuuen tatsol, amonnu
--ld Dipheny Hnine tact Jonbsalh Aal taomonaa LecR,sO

L) HaNDso
NO t HSO, HSQ tHWO,
 n d-bleck lnode. 2 CHCOOH CH,=co kbna
botta aan O607 on- MS tala becomag
Lp
wmoe
table . U ecaclly ba
hal Apans p:black
Ld) H"so tMaqnesla nixtwxe tet
yelloa pt baaic mance Adphah-
LH0Hso, fointd HPO NHOH NH, PO,
SAppt:)
LE Malehlck test M NH,PD P,otH t HD
LES Ball Raso +20
(akte pat WL d:lô a miaandiiokHN
Rsdd Ne hco addd te he akii pat
d d aiatte4s aaly e#aala ) LaPsal
h md a canbaidedl nalehaliako akih ppt o Ba Po,Ph,lea,) d
9er
Le) AL sol
2yellaseh ka fshipjat fe PO.,ALPO
SaSO +a co outaineelL

B0
Na dip the malehetick 0sedum nl
fpusaideCa Ph a salt t cancnH s0, +CHOH a gsal
vialetyello.oHack coloum is shlaioed
laih s ereled vapeiiaia huedin
2 Pa nstecdgsd lant i sblaineol
Amonium Nolibdate teu

HPD £lNH MaO HNON4JPHo,Ot NQ 1e,H_OH

3ikasnen 2020/08/15

Haienat ian
Caay yettss
edasd oc
 Na H&0 t H
N a , 8 , 0 + C, H , o
S n O t cO c o
Nas pdasulplde RO
FNo5,O H, O
No S Na,
r so,
le) P so
omaol D t Ph Po
hte A)
Phs,0,Een
os
PLS +s0 12 H
N)Micellantouionc
fe ,sol
a dank ialet calauralkd0Alaandbce5
cadil-HayH,sO trat fets0,),J
om atandan calau dis4paananaaid ac

thus Hs, dosat taiab) Fa 2 Fe S0

Fe s,O,),
2sal 2el deealauiaio
atubo

Ca canci Ho, teat

hidAdelid uk odomale cO and Cogas a evakud

Ano,sol
2kaRAt Bas,0 knad

d) HanNO l
hida pat ,O mkd
olecsaslsa
p n Calaut oucalaunsaud paduzs lnAad
e *UBI
CO 2020/084
his tarkies Th ath aa aule
 Catalyatthus ala tacdisn ats d) Cas, B"l
jthO prsahe ALaclian
ohaPat _rE oblainad
e Fe 0
LacencR5Osal
Aalaunlassceuat 9aa LH,Ja eaaletd
4a4 N.
mds anmaut a a and
77dande
yanund n
Alca in gaa Lbanálamq9-
halzng
SiE aesud amalamao glas ad
9elalhnasa Aiei acd
h baad

SO LA 1
SE t 2 HD
whte kaad dugasutuadiani
) P* laas dd

alaa ceubl otasneeolAice Hf

2020708