Experimental Report of General Chemistry (Lab) : Group

EXPERIMENTAL REPORT OF GENERAL CHEMISTRY (LAB)
GROUP:
UNIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETRIC ANALYSIS
Exp 1: Determination of calorimeter Exp. 2: Titration of HCl by NaOH using

constant phenolphtalein
1st time 2nd time 3 rd time Volume of 1st time 2 nd time 3rd time
ti .32 31 NaOH 0.lN 1,0 g._3
t2 [1 {O
t3 4? Jj-C, ';> Exp. 3: Titration ofHCl by NaOH using methyl
I ►-
, '
orange
Exp 2: Heat of neutralization reaction
Volume of 1st time 2 nd time 3rd time
1st time 2nd time 3 rd time
ti 31 30 31 NaOH0.lN 1,6 ?le f
tz 3/ 3'1 31
t3 ~1 ~5, S-- 31- Exp. 4a: Titration of CH3COOH by NaOH using
phenolphtalein
Exp 3: Heat of dissolution of CuSQ4
Volume of 1st time 2 nd time 3 rd time
1st time 2 nd time 3 rd time
ti 31 JO 31 NaOH 0.lN 10{t !t? if
tz ?_} 7 ~6 3 -;-
Exp. 2: Titration of CH3COOH by NaOH using
Exp 4: Heat of dissolution of NH4Cl methyl orange
st nd rd
1 time 2 time 3 time
ti 31 31 31 G, I :
NaOH 0.lN S-: 9
tz .tr ,26,~ al1
UNIT 4: DETERMINATION OF REACTION ORDER
Exp 1: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO 4
Time (s) 1st time 2 nd time 3rd time Time (s) 1st time 2 nd time 3 rd tiµie
Liti FY+ 1127 ,{JZt Liti G1 t.2_ 53
Lit2 Cf c-r Gt, Litz ~:L S-1 58
Lib o!_ l/- o.2 3 _z; Lib 6( 53 lfE
Lecturer
EXPERIM ENTAL REPORT OF GENERAL CHEMIST RY (LAB)
GROUP:

Exp 1: Determinatio n of calorimeter Exp. 2: Titration of HCl by NaOH using
constant phenolphtalei n
pt time 2 nd time 3 rd time Volume of 1st time 2 nd time 3rd time

h NaOH 0.IN 1~Lf- g_/
ti
Exp. 3: Titration of HCl by NaOH using methyl

orange
1st time 2nd time 3rd time Volume of 1st time 2 nd time 3rd time
h 3-<,5 32, 32, NaOH 0.lN 1'-2.. fl. I
ti 31 J1 31
13 n--. r 3r 3?:> Exp. 4a: Titration of CH3COOH by NaOH using
phenolphtalei n
1st time 2nd time 3 rd time Volume of 1st time 2nd time yd time
ti 30,r 31 ,3(),c> NaOH 0.lN q, I tJ<)_
ti J~;i 3,6 3?6r;-
Exp . 2: Titration of CH3COOH by N aOH using
Exp 4: Heat of dissolution of NH4Cl
methyl orange
I st time 2nd time 3rd time
Volume of 1st time 2nd time 3 rd time
ti 3rJ.:> 31 31
ti ,,z:f_S- ..2,, f
NaOH 0.IN d,:r ;,o
o2-1
Exp I : Reaction order in N a2S2O3 Exp. 2: Reaction order in H2SO4

Time (s) I st time 2nd time yd time Time (s) 1st time 2nd time 3 rd time
Liti /{Jg _g 1f,S- Liti >3, q Slp,f
Litz 5--J+. g ~J Litz 4t tJ q-g
Lih £+- 1 J 7-_g Lih 45_r 4//-..lf
Lecturer
GROUP:

1st time 2nd time 3rd time Volume of 1st time 2nd time 3rd time
ti c<.,<? J_,f ,i?_7 NaOH 0.lN q,f ~-q
ti 60 5E £'9
h 4~ 41+ 4~,r Exp. 3: Titration of HCl by NaOH using methyl
orange
1st time 2 nd time 3rd time Volume of 1st time 2nd time 3rd time
ti ~r 2.. 'f NaOH 0.lN ~6 1<- f
ti d6 <£{'
13 ,?.9 ~ 33 Exp. 4a: Titration of CH3COOH by NaOH using
phenolphtalein
Exp 3: Heat of dissolution of CuSO4
1st time 2nd time 3rd time Volume of 1st time 2 nd time 3 rd tin1e
NaOH 0.lN 1,_q qtR
ti .Zf cJ,f J;:;-
ti Jq, 3,9,( s- S3
Exp 4: Heat of dissolution ofNH4Cl
me thy1orange
ti $9 ,,Z~ oiP, ~
NaOH 0.lN ,1, f £};
ti c23f: ~3 .z:2.. )
Exp 1: Reaction order in Na2S2O3 Exp. 2: Reaction order in H 2SO4

Time (s) 1st time 2nd time 3 rd time Time (s) 1st time 2 nd time 3rd time
t.ti II~ ;(16 t.ti 6 ).,, Ci
t.ti )5' >ft llt2 $-fJ S1f
t.h .JC) ,J f th !f-7 5V
Lecturer
GROUP:
UNIT 2: HEAT OF THE REACTION UNIT 8: VOLUM ETRIC ANALYSIS
Exp 1: Determin ation of calorimet er Exp. 2: Titration ofHCl by NaOH using
constant phenolph talein

1st time 2nd time 3rd time Volume of
NaOH 0.lN 1Jt g_ g
ti !JD 11 30
ti JI; tr t?-
t3 l+P 77) lf_q Exp. 3: Titration ofHCl by NaOH using methyl
orange
Exp 2: Heat of neutraliza tion reaction
1st time 2nd time 3rd time
ti )c!Jc~ ?JO }O NaOH 0.lN ·:rvf fO
ti 30, S- otl3~) o2_q~ (
h 3> 3r 5~~ Exp. 4a: Titration of CH3COO H by NaOH using
phenolph talein
Exp 3: Heat of dissolutio n of CuSO4
rd Volume of 1st time 2 nd time 3 rd time
1st time 2 nd time 3 time
NaOH 0.lN -10 q.g
ti 3D 3(? $ 30<~
t2 3;> }6, ~ 76, >
Exp,hb,T itration of CH3COO H by NaOH using
Exp 4: Heat of dissolutio n ofNH4Cl methy 1 orange
rd
Volume of 1st time 2 nd time 3rd time
ti '} O ~ ~()~c_,-
NaOH 0.lN 4, f 770
ti ~r ..2£ ,,ZGS
Time (s) 1st time 2nd time 3rd time Time (s) 1st time 2 nd time 3rd time
6h L03 1°1 6h c:1 01
6ti 159 t'O 6ti :;-r- 5o
6t3 50 alt 6t3 !r-4 (;?)
Lecturer
GRO~~~ERIMENTAL RE P~ F GENERAL CHEMISTRY (LAB)

ti ;>.2.., 31 NaOH 0.lN ,{{2 {{J<- f
ti i{g ~{ $
13 L+ I Lf-2_ Exp. 3: Titration of HCl by NaOH using methyl
orange
Volume of 1st time 2nd time 3rd time
ti 3?1 51
NaOH 0.lN 11 /Oc>
ti 82 81
b J;r 81 Exp. 4a: Titration of CH3COOH by NaOH using
phenolphtalein
Exp 3: Heat of dissolution of CuSO4 2 nd time 3rd time
rd Volume of 1st time
1st time 2nd time 3 time
NaOH 0.lN tJ✓ E /0,D
ti 32 31
tz /!;6 :7 ~
Exp 4: Heat of dissolution ofNH4Cl methyl orange
nd rd
1st time 2 time 3 time 1st time 2nd time 3 rd time
Volume of
ti 31 81 NaOH 0.lN 1, S- ) <- 1
tz olf? al,%
UNIT 4: DETE RMIN ATIO N OF REACTION ORDE R
Exp. 2: Reaction order in H2SO4
Exp 1: Reaction order in Na2S2O3
3rd time Time (s) 1st time 2nd time 3rd time
Time (s) 1st time 2nd time
Liti /08 jO'J /6'> Liti 6( Cf 62
Litz {9 t!O t ic r Liti S') ~ sr-
.!_1 Lih tf1 SZ) y/
Lit3 ;;O o29
Lectur er
L CHEMISTRY (LAB)
GROUP: - (1) -
EX PER IM EN TA L RE PO RT OF GENERA
UNIT 8: VOLUMETRIC ANALYSIS

UNIT 2: HEA T OF THE REACTION
Exp. 2: Titration of HCl by NaOH using
Exp 1: Determination of calorimeter
phenolphtalein
constant
1st time 2nd time yd time
st
1 time 2nd time 3rd time Volume of
h 82 33 NaOH 0.lN 1✓ 1 16
ti r.2; f1
h 54 53 Exp. 3: Titration of HCl by NaOH using meth
yl
orange
Exp 2: Heat of neutralization reaction nd 3rd time
Volume of 1 time 2 time
st
rd
1st time 2nd time 3 time
NaOH 0.lN ff t 1, 5"
h c2i elf
ti o2_9 o2B
g
h -3 3 33 Exp. 4a: Titration of CH3COOH by NaOH usin
phenolphtalein
Exp 3: Heat of dissolution of CuSO4 Volume of 1st time 2nd time 3rd time
rd
NaOH 0.lN { 6 { 6
h ;j,6 31r
ti l+D _3q
g
Exp. 2: Titration of CH3COOH by NaOH usin
Exp 4: Heat of dissolution of NH4Cl methyl orange
rd
ti
t2
3 5}
yq
~It
50
Volume of
NaOH 0.lN ,~ r-
1st time 2nd time
3(2--
3rd time
ON ORDER
UNIT 4: DETERMINATION OF REACTI
Exp . 2: Reac tion order in H2SO4
Exp 1: Reaction order in Na2 S2O3
nd 3rd
time
st
Tim e (s) I time 2nd time 3rd time
Time (s) I st time 2 time
6t1 §3 51{-
6h 11 10
kt 4--1
6t2
613
4-S
.!_//
)f 6
J_ 3
Liti
Lib -
'+ > )f-6
Lecturer
C'{OUP:
1lNIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETRIC ANALYSIS

r :; p 1: Determination of calorimeter Exp. 2: Titration ofHCl by NaOH using
v ·1 stant phenolphtalein
NaOH 0.lN 16 g_g
Exp. 3: Titration of HCl by NaOH using methyl

orange
l \ p 2: Heat of neutralization reaction
flf g___q
91 3:l NaOH 0.lN
1,,- ?/ 32
I 86 51 Exp. 4a: Titration of CH3COOH by NaOH using
phenolphtalein
I '·p 3: Heat of dissolution of CuSO4
I fi
I. t k"'
1st time
Sf
37
2nd time 3rd time
31l<>
91
NaOH 0.lN ,{0 1/._g

I · n 4: Heat of dissolution ofNH4Cl methyl orange
r Volume of 1st time 2nd time 3rd time
31 :}{
II ~ NaOH 0.lN c£S- 3<-0
b.2::: £? ell=>
I ., p I: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO4
·me (s) Ist time 2nd time 3rd time Time (s) 1st time 2nd time 3 rd time
Al 1 11D 10~ .6.ti 5:5 Sr
11 12 f;f Ji'O ,6.tz 4-l )fj
,I). 13 o2S- ol> b.b k-2- /-f 3
Lecturer
-
(i)
G!~ OUP:
1
• INIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETRIC ANALYSIS
J·\ p 1: Determination of calorimeter Exp. 2: Titration of HCl by NaOH using
c 1stant phenolphtalein
I ?JL 32- NaOH 0.IN (I. ,;- fJt
2- Gq- tC-
J J+g s:v Exp. 3: Titration ofHCl by NaOH using methyl
orange
I·"' p 2: Heat of neutralization reaction
f 3.t ,;~ NaOH 0.IN cts {c.6

'V 3.2 33
1 51 st Exp. 4a: Titration of CH3COOH by NaOH using
phenolphtalein
I·-.: p 3: Heat of dissolution of CuSO4
I st time 2nd time 3rd time Volume of I st time 2nd time 3rd time
r~
NaOH 0.lN {O~O
32 32 {O" L
y jf 5P
I ·., I) 4: Heat of dissolution of NH4Cl methy 1orange
1 1st time 2nd time 3rd time
3,2_ Volume of I st time 2nd time 3rd time
-/;, 32
I NaOH 0.IN 4-f 3J(
hv if -?_/(
I
1· · p I: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO4

ime (s) 1st time 211d time 3rd time Time (s) 1st time 2nd time 3rd time
ffi'i j<;O r'.
[4-g ~ti 5-s- Sf .D
,l)'G 6~ C> t Lf- ~t2 ?2 !;.7J J:'f
/j 3 ~ 22 o2 ~ t3 Lrt Lf-7 J+fl
Lecturer
EXPERIMENTAL REPORT OF GENERAL CHEMIST RY (LAB)
GROUP:
UNIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETR IC ANALYSIS
Exp 1: Determination of calorimeter Exp. 2: Titration ofHCl by NaOH using

constant phenolphtalei n
2nd time 3rd time 1st time 2 nd time 3rd time

1st time Volume of
3· L~ 6 {or Lr
ti 30 31 3 {l > NaOH 0.IN [Oc
ti r ~ 0 /LS
h +3 Lb~ 4-1 Exp. 3: Titration ofHCl by NaOH using methyl
l ..
orange
(t/S-
ti ;3(); ~ JO ?{r > NaOH 0.lN 10e,3 .((}l0
ti 11 3:r~ 50,_~
t3 S6c> J?r 76rS--
'
Exp. 4a: Titration of CH3COOH by NaOH using

\ ..
phenolphtalei n · ··
1st time 2nd time 3rd time ..
3 (._f' 3-Z, 0 5 (<> NaOH 0.lN 16 q, (j
ti
ti /~£<> 3~r J>r.0
Exp. 4b: Titration of CH3COOH by NaOH using
Exp 4: Heat of dissolution ofNH4Cl methyl orange
ti ?{c c;- -,,;~~D ;; [<~
NaOH 0.IN 3,3 3cb
t2 cL rs- cl§,0 ,z1;rJ
UNIT 4: DETERMIN ATION OF REACTION ORDER
Time (s) 1st time 2nd time 3rd time Time (s) 1st time 2nd time 3rd t_ime
6h ,()fO ;(l;--f' 1/f> 6ti 7:J 0 ~
6t2 11 fq 06 6ti 4-? /+;;' 0g
613 ~3 5,2_ 33 6t3 4.2, 4,L 43
Lecturer
EXPERIMENTAL REPORJ-,0 ·F--- ENERAL CHEMISTRY (LAB)
( " ' n UP:
1 1
NIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETRIC ANALYSIS
I ·\ ') 1: Determination of calorimeter Exp. 2: Titration of HCl by NaOH using
, Stant phenolphtalein
1st time 2nd time 3rd time Volume of 1st time 2 nd time yd time
l*-~--+-~~____j
I f 2--:.
-._--+----=--..L..i.......,:::_+.-----.!:.---+-~__.:______i
NaOH 0.lN [O/j /0,_0
l ~ _ > - ~ ~ - ' - - - ' - - - - { - - - ' - ~___, Exp. 3: Titration ofHCl by NaOH using methyl
orange
! · p 2: Heat of neutralization reaction
1
151 time 2 nd time 3 rd time Volume of 1st time 2 nd time yd time
, -b 31;- 32-- NaOH 0.lN ((2 0 1tlO

~ ----t--~-+------t----------1
3 /- - - -ot9
f k·- - - ~ - - - - - + ---!
I B ~ ~ - -~ "~bc_~ ~ 5~ ~ Exp. 4a: Titration of CH3COOH by NaOH using
phenolphtalein
: p 3: Heat of dissolution of CuSO4
1st time 2 nd time 3 rd time Volume of 1st time 2 nd time yd time
NaOH 0.lN q,_tJ /f)tO

' ·1 4: Heat of dissolution ofNH4Cl methyl orange
1st time 2 nd time 3rd time
4✓i ,29 ,,zg ctR NaOH 0.lN 1J) /{c f
rv oP_ r;- c!J_lf, 21r-cr-
,, 1: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO4
•ne (s) pt time 2nd time 3 rd time Time (s) 1st time 2nd time 3rd time
'A- -fr( 11lf- 1N1 ;(1't t-.ti ~ '),>
73
Ai;,, ~,2 0i 7 Jj~ t-.ti )3 lf?- !:>1
4 t? /
,-.;_q ,x r:; .,22 L1t3 43 ~!!> /j-6
Lecturer
EXP ERIM ENT AL REPORT OF GENERAL CHEMISTRY (LAB
)
C "OUP:
: INIT 2: HEAT OF THE REAC UNIT 8: VOLUMETRIC ANALYSIS

I_. ., p 1: Determ inatio n of calorim eter Exp. 2: Titrati on of HCl by NaOH using
, Stant pheno lphtale in
1st time 2nd time 3 rd time Volum e of 1st time 2 nd time 3rd time
$2_,. 3/ NaOH 0.lN IOc O g_g
i L/:f 57)
4-1 J+I Exp. 3: Titrati on of HCl by NaOH using methy l
I ·· p 2: Heat of neutra lizatio n reactio n orange
\ 1st time 2 nd time 3 rd time Volum e of 1st time 2 nd time 3rd time
I f1_-- ---+- ~-..+ ---L' ----~- --l
NaOH 0.lN tJ6 (}/}-
: t--2--
"-------+ -_:;__ '-----+ -----" "----+ ---- --4
l h-+-- ~~_j_ ____ __,:.~ __L_ ____ _, Exp. 4a: Titrati on of CH3C OOH by NaOH using
pheno lphtale in
1· p 3: Heat of dissol ution of CuSO4
1st time 2 nd time 3rd time Volum e of 1st time 2 nd time 3rd time
11-I S1 '}0 NaOH 0.lN
1V.n <J~tJ
1 -b,7,,, 31 S?
Exp. 2: Titrati on of CH3C OOH by NaOH using
•1 4: Heat of dissolu tion of NH4Cl
methy l orange
Volum e of 1st time 2 nd time 3rd time
t t7 31 3/
t-✓ .2-g C( g NaOH 0.lN
~1 1>
UNIT 4: DETERMINATION OF REACTION ORDE R
p l: Reacti on order in N a2S2O 3 Exp. 2: Reacti on order in H2SO4

· ine (s) 1st time 2 nd time 3 rd time Time (s) 1st time 2 nd time 3rd time
·h•I ll 6 11~ 6ti ~ f;lf
(1-h, lf-4 03 612 4~ )Af
4-t-7 o<.7 J_'g 613 !+O If2---
Lectu rer
··: XPERIMENT AL REPORT OF GENERAL CHEMISTRY (LAB)
UP:
1'' 'IT 2: HEAT OF THE REACTION

@ UNIT 8: VOLUMETRIC ANALYSIS
I : Determination of calorimeter Exp. 2: Titration of HCI by NaOH using

lant phenolphtalein
pt time 2nd time 3rd time Volume of 1st time 2nd time 3rd time
NaOH 0.lN l Oc,2.__ 11
fr
h- - to
-+--"'----"---+---= ---=---e---__:__:----i
Vj -'-------'..l...-------'-___:.__i_=_____J__4-...!.......L__j Exp. 3: Titration ofHCI by NaOH using methyl
orange
, 2: Heat of neutralization reaction
NaOH 0.lN ,(0< 6 JO J_
3/ 31 3~
1 ~'-
oU
'31
2-.q
_?~
c1,g
71 Exp. 4a: Titration of CH3COOH by NaOH using
phenolphtalein
1 3: Heat of dissolution of CuSO4
3(
NaOH 0.lN ;(Ot ti /Ot 1
3o 30
"') _ :>£ 86 !J{
·, 4: Heat of dissolution ofNH4Cl methyl orange
-b, 3D 30 30
ri:.,S--
NaOH 0.lN ;7c.? -3. >
-b-v c!!.t cl~
' · •i I: Reaction order in Na2S2O3 Exp. 2: Reaction order in H 2SO4
,ne (s) 1st time 2nd time 3rd time Time (s) 1st time 2nd time 3rd time
1to 1>D lw liti
At-;,,- -:;-s J-3 ?3
f)f-i, 4~ 4.L 3q
Lecturer

Experimental Report of General Chemistry (Lab) : Group

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Experimental Report of General Chemistry (Lab) : Group

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EXPERIMENTAL REPORT OF GENERAL CHEMISTRY (LAB)

UNIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETRIC ANALYSIS

Exp 1: Determination of calorimeter Exp. 2: Titration of HCl by NaOH using

Exp 1: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO 4

UNIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETRIC ANALYSIS

pt time 2 nd time 3 rd time Volume of 1st time 2 nd time 3rd time

Exp. 3: Titration of HCl by NaOH using methyl

Exp I : Reaction order in N a2S2O3 Exp. 2: Reaction order in H2SO4

UNIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETRIC ANALYSIS

UNIT 4: DETERMINATION OF REACTION ORDER

Exp 1: Reaction order in Na2S2O3 Exp. 2: Reaction order in H 2SO4

UNIT 2: HEAT OF THE REACTION UNIT 8: VOLUM ETRIC ANALYSIS

Exp 1: Determin ation of calorimet er Exp. 2: Titration ofHCl by NaOH using

constant phenolph talein

1st time 2nd time 3 rd time

UNIT 4: DETERMINATION OF REACTION ORDER

Exp 1: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO 4

UNIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETRIC ANALYSIS

Exp 1: Determination of calorimeter Exp. 2: Titration of HCl by NaOH using

UNIT 8: VOLUMETRIC ANALYSIS

1lNIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETRIC ANALYSIS

Exp. 3: Titration of HCl by NaOH using methyl

Exp. 2: Titration of CH3COOH by NaOH using

I ., p I: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO4

f 3.t ,;~ NaOH 0.IN cts {c.6

UNIT 4: DETERMINATION OF REACTION ORDER

1· · p I: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO4

UNIT 2: HEAT OF THE REACTION UNIT 8: VOLUMETR IC ANALYSIS

Exp 1: Determination of calorimeter Exp. 2: Titration ofHCl by NaOH using

2nd time 3rd time 1st time 2 nd time 3rd time

Exp. 4a: Titration of CH3COOH by NaOH using

UNIT 4: DETERMIN ATION OF REACTION ORDER

Exp 1: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO 4

, -b 31;- 32-- NaOH 0.lN ((2 0 1tlO

Exp. 2: Titration of CH3COOH by NaOH using

,, 1: Reaction order in Na2S2O3 Exp. 2: Reaction order in H2SO4

: INIT 2: HEAT OF THE REAC UNIT 8: VOLUMETRIC ANALYSIS

I ·· p 2: Heat of neutra lizatio n reactio n orange

p l: Reacti on order in N a2S2O 3 Exp. 2: Reacti on order in H2SO4

1'' 'IT 2: HEAT OF THE REACTION

I : Determination of calorimeter Exp. 2: Titration of HCI by NaOH using

UNIT 4: DETERMINATION OF REACTION ORDER

' · •i I: Reaction order in Na2S2O3 Exp. 2: Reaction order in H 2SO4

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