You are on page 1of 33

PROPERTIES OF GEO-POLYMER

BRICKS MADE WITH FLY-ASH, RICE-


HUSK ASH AND WOODEN POWDER

Project ID: 22039


B.Tech. Minor Project Report
submitted for fulfillment of
the requirements for the
Degree of Bachelor of Technology
Under Biju Pattnaik University of Technology

Submitted By
DEBASHISH GOUDA ROLL NO. 201810550
B HEMANT KUMAR ROLL NO. 201810183

2021 – 2022

Under the guidance of


Prof. Sujit Kumar Rout

NATIONAL INSTITUTE OF SCIENCE & TECHNOLOGY


Autonomous
PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

Palur Hills, Berhampur, Odisha – 761008, India

National Institute of Science & Technology (Autonomous) ii


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

ABSTRACT
This research has aims to study effect between flyash , ggbs and rice husk ash to

properties of bricks. This paper presents an economic analysis of manufacturing

geopolymer bricks for use in the construction sector. The manufacturing processes of

both geopolymer bricks and traditional fired bricks were investigated. For this study,

we collected and analyzed all phases of geopolymer brick production from the

extraction of raw materials to storage. Seven formulations of geopolymer bricks based

on clay and waste bricks were analyzed. We considered the cost of raw materials and

logistics operations in the production line of brick manufacturing.. In the case of

waste bricks, for the same production cost, the compressive strength of the

geopolymer bricks is double that of fired bricks. Hence, this study shows the

economic interest in the industrial production of geopolymer bricks. It also confirms

that future research is needed that focuses on necessary changes to the current

industrial production chain required for the manufacture of geopolymer bricks.

Geopolymer bricks contain flayash as the source material and an alkaline activator for

the activation of polymerization reaction. In this study, experimental work has been

performed on geopolymer bricks with flyash and GGBS as source material and

sodium hydroxide and sodium silicate as an activator. The molarity of sodium

hydroxide was maintained at 12M for all the mixtures and the ratio of sodium

hydroxide to sodium silicate was kept as 1:2.5. The brick properties such as

compressive strength, water absorption, acid resistance and efflorescence test were

conducted on the test specimens. Test results indicated that geopolymer concrete with

higher GGBS content resulted in higher compressive strength and better properties

compared to flyash based geopolymer brick.

National Institute of Science & Technology (Autonomous) i


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

ACKNOWLEDGEMENT
It is our proud privilege to epitomize our deepest sense of gratitude and indebtedness

to our advisor, Prof. Sujit Kumar Rout for his valuable guidance, keen and sustained

interest, intuitive ideas and persistent endeavour. His inspiring assistance, laconic

reciprocation and affectionate care enabled us to complete our work smoothly and

successfully.

We extend our sincere thanks to Prof. Padminee Samal, B.Tech. Project

Coordinator, for giving us the opportunity and motivating us to complete the project

within stipulated period of time and providing a helping environment.

We acknowledge with immense pleasure the sustained interest, encouraging attitude

and constant inspiration rendered by Dr. Sukant K. Mohapatra (Chairman), Dr.

Priyadarshi Tripathy (Principal) and Dr. Barada Prasad Sethy (HoD) N.I.S.T.

Their continued drive for better quality in everything that happens at N.I.S.T. and

selfless inspiration has always helped us to move.

We would also like to extend our heartfelt gratitude to our parents and friends for

their unflinching support and help.

DEBASHISH GOUDA

ROLL NO. 201810550

B HEMANT KUMAR

ROLL NO. 201810183

National Institute of Science & Technology (Autonomous) ii


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

TABLE OF CONTENTS
ABSTRACT...................................................................................................................i
ACKNOWLEDGEMENT.............................................................................................ii
TABLE OF CONTENTS.............................................................................................iii
LIST OF FIGURES......................................................................................................iv
1. INTRODUCTION.....................................................................................................1
2. LITERATURE REVIEW..........................................................................................2
3. MATERIALS USED.................................................................................................6
3.1 FLY-ASH.....................................................................................................6
3.2 GGBS (Ground Granulated blast-furnace slag)...........................................7
3.3 Alkali Activators.........................................................................................9
4. METHODOLOGY..................................................................................................11
4.1 Consistency Test of Fly-Ash......................................................................11
4.1.1 Mould.................................................................................................12
4.1.2 Casting of Mould...............................................................................12
4.2 Testing of Brick Sample............................................................................14
5. RESULTS................................................................................................................15
6.COST ANAYISIS…………………………………………………………………
15
6.1 Geopolymer Brick……………………………………………………
16
6.2 Clay Brick…………………………………………………………….16
6.3 FLY Ash Brick………………………………………………………..16
7. CONCLUSION........................................................................................................16
REFERENCES............................................................................................................17

National Institute of Science & Technology (Autonomous) iii


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

LIST OF FIGURES
Fig. 1 Fly-Ash................................................................................................................6
Fig. 2 Fly-Ash and GGBS..............................................................................................9
Fig. 3 Alkali Activators..................................................................................................9
Fig. 4 Mixing of NaOH and Na2SiO3...........................................................................10
Fig. 5 Vicat Apparatus.................................................................................................11
Fig. 6. Mould................................................................................................................12
Fig. 7. Casting of Mould..............................................................................................12
Fig. 8. Bricks after 7 Days of oven curing...................................................................13
Fig. 9 Digital Compression Testing Machine.........................................................................14

National Institute of Science & Technology (Autonomous) iv


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

National Institute of Science & Technology (Autonomous) 0


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

1. INTRODUCTION

Brick is the most commonly used building material in India for more than 1000 years. Fired

clay bricks are most commonly used in India. But nowadays fly ash bricks have been

tremendously being used due to the reduction in cost as well as its light weight. Geopolymer

bricks are the latest innovation in the brick industry which consist of supplementary

cementitious materials such as fly ash or GGBS activated by an alkaline activator .The

application of geopolymer technology gained importance due to the reduction of the CO2

emissions by utilizing the supplementary cementitious materials in place of cement . It has

been noted that geopolymer bricks made with flyash requires higher curing temperature to

achieve higher compressive strength and lower absorption. Prepared geopolymer bricks using

waste raw materials such as clay brick waste, slaked lime waste, de-aluminated kaolin and

caustic soda. They were able to produce light weight bricks with densities around 1000

kg/m3 with a compressive strength of 1.4MPa. Formulated geopolymer bricks using ceramic

dust waste. They found that the cost of the geopolymer bricks produced from ceramic waste

resulted in the reduction of production cost of bricks. Studied the durability and leaching

behavior of geopolymer bricks made from mine tailings. They found that there was

substantial reduction in the strength of the geopolymer bricks immersed in pH=4 and seven

solutions. Performed optimization studies to find the optimum curing conditions of Fired clay

bricks and Natural pozzolona based geopolymers. Their results indicated the compressive

strength of 37 to 26 MPa has been achieved when proper production conditions are adopted.

Reviewed the development of geopolymer bricks using industrial wastes and reported that the

variation in the source materials can significantly affect the physical, chemical and

mechanical properties of alkali-activated bricks. In this research work, we aimed at

National Institute of Science & Technology (Autonomous) 1


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

developing geopolymer bricks and studying its properties such as compressive strength, water

absorption and acid resistance test.

National Institute of Science & Technology (Autonomous) 2


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

2. LITERATURE REVIEW
Subharajit Roy, Sanjith J, Jagath H R, Chethan G

Fly ash, also known as “pulverized fuel ash” in many countries such as England, Northern

Ireland, and Scotland etc. is a coal combustion product. It is composed of fine particles of

burnt fuels and fuel gases emitted from coalfired boilers. Though it was causing severe air

pollution, in the past, fly ash was usually released into the atmosphere as it is mainly a

thermal waste of coal firing thermal plants. But presently, according to air pollution control

standards, it is captured prior to release by fitting pollution control equipment. Due to its

pozzolanic nature, recycled fly ash is usually used as the production of hydraulic cement and

a complete and/or partial replacement for Portland cement in concrete production. Potential

of fly ash as a material is not only restricted to cement and concrete industries. It can be

utilized as a raw material for brick production, which will be a positive answer towards both

environmental and economic complications. The purpose of this particular study is to explore

the performance of Geopolymer brick consists of fly ash as one of its chief material. The

bricks were casted with clay soil to fly ash in the different proportion of 100:0, 80:20, 70:30,

60:40 and 50:50. Sodium fume solution was applied as an alkaline-activator and a ratio 1:2 of

water to NaOH solution was used as the binder solution. With an optimum water/binder ratio

of 0.416 and adopted dimension of (200 X 100 X 100) mm. The experimental outcomes were

compared with locally available conventional bricks.

Nicolas Youssef, Zoubeir Lafhaj and Christophe Chapiseau “Economic Analysis of

Geopolymer Brick Manufacturing: A French Case Study.”

National Institute of Science & Technology (Autonomous) 3


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

In this paper, we studied an economic analysis of the use of geopolymer brick at the

industrial level. The research presents a French case study of the brickworks in the North of

France. Different geopolymer brick formulations based on clay and waste bricks were

studied. The production cost of one metric ton of bricks and the compressive strength of the

geopolymer bricks were the two parameters used to evaluate the feasibility of production of

geopolymer bricks at the industrial level. The determination of the production cost of the

geopolymer bricks was based on the annual business model of the brickworks, which was

used to find all data sources needed. The results of this study demonstrated that the

production cost of geopolymer bricks changes significantly depending on the ingredients

used in the formulation. The geopolymer brick based on clay gives a financial gain of 5%

compared to traditional fired brick for the same compressive strength of 20 MPa. In the case

of the geopolymer bricks manufactured with waste brick, an improvement of 100% in

compressive strength can be achieved with the same production cost as fired bricks. These

results can be considered as a database for use in the production of geopolymer-based

building materials at the industrial level.

S. Sasikumar, Dr. M. Natarajan, Dr. N. Balasundaram, Dr. V. Karthik “Study on the

Behavior of Geopolymer Brick Under Different Curing Temperatures and Alkaline

Solution Concentration”

Conclusions are arrived from the experimental study done on GPB with different

concentrations of alkaline solution and curing temperatures.

 Geopolymer bricks can be used as a viable alternative to the conventional clay bricks.

 Class F fly ash produces better strength values than the GPB specimens made with

Class C fly ash.

National Institute of Science & Technology (Autonomous) 4


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

 It was concluded that the optimum results are obtained at 10M alkaline solution and

600C hot air oven curing temperature. Beyond 10M, the strength property doesn’t

show better results than other concentrations and increases the cost of GPB. Increase

in curing temperature increases the strength of GPB mixes, but 900C also doesn’t

produce viable results.

 Thermal curing temperature of 600C shows better results with the ratio of

Na2SiO3/NaOH is 2.5, whereas the previous literatures shows that the curing

temperature increases to 1000C when the ratio of alkaline activator is around 1.5.

 At 7 days, the crushing strength GPB specimen with 10M and 600C is 137.01% and

77.18% higher than the specimens with room temperature and 900C respectively.

 Increment in alkaline solution concentration reduces that pores on the surface of the

GPB. It results in reduced water absorption at optimum parameters.

 Generally, GPB is alkali resistive nature and shows appreciable results when the

specimens are immersed in 3% H2SO4 solution, whereas the reduction in molarity of

solution shows less than 1% loss of weight will be observed

Wan Mastura Wan Ibrahim, Kamarudin Hussin, Mohd Mustafa Al Bakri Abdullah,

Aeslina, Abdul Kadir “Geopolymer lightweight bricks manufactured from fly-ash and

foaming-agent.”

On the basis of the experimental work it is concluded that the compressive strength of

foamed geopolymer bricks foaming agent to water ratio (1:10) reduced in strength between

49.3- 68.6% while for the (1:20) ratio, the strength decreases between 66.7-72.9% of

strength. However, the strength for all samples increases as the curing temperature increased.

It is also analysed that water absorption of foamed geopolymer bricks for samples with 1:10

ratio of foaming agent to water was increases about 56-66% from the control samples without

National Institute of Science & Technology (Autonomous) 5


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

foaming agent added and 62-63% more as compared to the control samples when 1:20 of

foaming agent to water ratio was used. The samples obtained in present work shows promise

in application of wall insulation materials.

This paper deals with the development of lightweight geopolymer bricks by using foaming

agent and flyash. The mix parameters analysed through a laboratory experiment with fix ratio

of sodium silicate/sodium hydroxide solution mass ratio 2.5, fly ash/alkaline activator

solution mass ratio 2.0, foaming agent/paste mass ratio 1:2 and molarity of sodium hydroxide

solution used was 12M. Different curing temperature (Room Temperature,60, 80) and

foaming agent/water mass ratio (1:10 and 1:20) were studied. Compressive strength, density

analysis, and water absorption has been investigated. The results show that the foamed

geopolymer bricks with a lowerfoam/water mass ratio (1:10)and high curing temperature

(80°C) leading to a better properties. Mixtures with a lowdensity of around 1420 kg/m3 and a

compressive strength of around 10 MPa were achieve.

Arya K.C., Alester Joseph Vanreyk and Chinku Alphons Tom “A REVIEW ON GGBS,

PAPER SLUDGE AND LATERITE SOIL IN BRICK MANUFACTURING”

From the reviewed literatures the following conclusions were made,

 Compressive strength of bricks made with Lime:GGBS and PC:GGBS shows higher

strength and less water absorption rate for 28days. Bricks made with sand and GGBS

shows better compressive strength, lesser water absorption rate and thermal

conductivity as age increases.

 Bricks made with paper sludge shows better compressive strength upto 5-15% and the

thermal conductivity decreases with increase in paper sludge.

National Institute of Science & Technology (Autonomous) 6


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

 Increase in water absorption is the main limitation observed in increase in addition of

paper sludge.

 Bricks made with laterite soil shows improved compressive strength and water

absorption rate. Laterite soils have similar properties to that of clay whereas laterite-

clay bricks show more water absorption than that of clay bricks.

National Institute of Science & Technology (Autonomous) 7


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

R.Divahar, S. P. Sangeetha, P. S. Aravind Raj, S. Ispara Xavier “Bricks Manufacturing

With GGBS.

Good quality bricks can be produced from stipulated proportions of slag, lime mixture and

sand. The strength characteristics of the unfired bricks tested in this study were improved

with the use of lime and GGBS as a binder.

 The amount of the clay is reduced to 20% of total use. The manufacturing process of

the bricks is simple and does not require any firing or autoclaving, specialized plant or

machinery. Therefore, the energy consumption will be much less compared with

conventional burnt clay bricks and calcium silicate bricks.

 Sufficient strength is obtained by moulding the bricks at significantly lower pressure

compared to that for calcium silicate bricks.

 Brick production using GGBS as the main stabilising agent will reduce the energy and

cost of the firing process. Appropriate research and development into new

technologies that reduce energy usage and carbon dioxideemissions are vital for

sustainable building construction. More significant engagement in the development of

new materials will help the construction industry meet global challenges and develop

business.

A. Sumathi, K. Saravana, Raja Mohan “Compressive Strength of Fly Ash Brick with

Addition of Lime, Gypsum and Quarry Dust”.

Based on the experimental study, following conclusions can be drawn regarding the strength

behavior of flyash brick.The study was conducted to find the optimum mix percentage of

flyash brick. However the brick specimen of size 230mm x 110mm x 90mm were cast for

different mix percentage of Flyash (15 to 50%), Gypsum (2%), Lime (5 to 30%) and Quarry

dust (45 to 55%). However the specimens have been tested for seven mix proportions. The

National Institute of Science & Technology (Autonomous) 8


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

mechanical properties such as compressive strength were studied for different mix

proportions, at different curing ages. From the results it was inferred that, among the seven

proportions the maximum optimized compressive strength is obtained for optimal mix

percentage of Flyash-15% Lime-30% Gypsum-2% Quarry dust-53% as 7.91 N/mm².

National Institute of Science & Technology (Autonomous) 9


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

3. MATERIALS USED

3.1 FLY-ASH

Fly ash is a fine gray powder consisting mostly of spherical, glassy particles that are

produced as a byproduct in coal-fired power stations. Fly ash has pozzolanic properties,

meaning that it reacts with lime to form cementations compounds. It is commonly known as a

supplementary cementations material.

Fly ash is a residue generated in combustion and comprises the fine particles that rise with the

flue gases. Ash that does not rise is called bottom ash. In an industrial context, fly ash usually

refers to ash produced during combustion of coal. Fly ash is a heterogeneous material. The

main chemical components present in fly ash are:

1. Silicon dioxide

2. Aluminum oxide

3. Ferric oxide

Fly ash material solidifies while suspended in the exhaust gases and is collected by

electrostatic precipitators or filter bags. Since the particles solidify rapidly while suspended in

the exhaust gases, fly ash particles are generally spherical in shape and range in size from 0.5

µm to 300 µm.

National Institute of Science & Technology (Autonomous) 10


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

Fig. 1 Fly-Ash

National Institute of Science & Technology (Autonomous) 11


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

3.2 GGBS (Ground Granulated blast-furnace slag)

Ground-granulated blast-furnace slag (GGBS or GGBFS) is obtained by quenching molten

iron slag (a by-product of iron and steel-making) from a blast furnace in water or steam, to

produce a glassy , granular product that is then dried and ground into a fine powder. Ground-

granulated blast furnace slag is highly cementitious and high in calcium silicate hydrates

(CSH) which is a strength enhancing compound which improves the strength, durability and

appearance of the concrete.

A. COMPOSITION

The main components of blast furnace slag are CaO (30-50%), SiO2 (28-38%), Al2O3 (8-

24%), and MgO (1-18%). In general increasing the CaO content of the slag results in raised

slag basicity and an increase in compressive strength. The MgO and Al2O3 content show the

same trend up to respectively 10-12% and 14%, beyond which no further improvement can

be obtained. Several compositional ratios or so-called hydraulic indices have been used to

correlate slag composition with hydraulic activity the latter being mostly expressed as the

binder compressive strength.

B. APPLICATION

GGBS cement can be added to concrete in the concrete manufacturer's batching plant, along

with Portland cement, aggregates and water. The normal ratios of aggregates and water to

cementitious material in the mix remain unchanged. GGBS is used as a direct replacement for

Portland cement, on a one-to-one basis by weight. Replacement levels for GGBS vary from

30% to up to 85%. Typically 40 to 50% is used in most instances.

National Institute of Science & Technology (Autonomous) 12


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

C. DURABILITY

GGBS cement is routinely specified in concrete to provide protection against both sulfate

attack and chloride attack. GGBS has now effectively replaced sulfate-resisting Portland

cement (SRPC) on the market for sulfate resistance because of its superior performance and

greatly reduced cost compared to SRPC. Most projects in Dublin's Docklands

including Spencer Dock are using GGBS in subsurface concrete for sulfate resistance.

Bulk Electrical Resistivity is a test method that can measure the resistivity of concrete

samples. (ASTM 1876-19) The higher electrical resistivity can be an indication of higher ion

transfer resistivity and thus higher durability. By replacing up to 50% GGBS in concrete,

researchers have shown that durability can be significantly improved.

To protect against chloride attack, GGBS is used at a replacement level of 50% in concrete.

Instances of chloride attack occur in reinforced concrete in marine environments and in road

bridges where the concrete is exposed to splashing from road de-icing salts. In

most NRA projects in Ireland GGBS is now specified in structural concrete for bridge piers

and abutments for protection against chloride attack. The use of GGBS in such instances will

increase the life of the structure by up to 50% had only Portland cement been used, and

precludes the need for more expensive  reinforcing.

GGBS is also routinely used to limit the temperature rise in large concrete pours. The more

gradual hydration of GGBS cement generates both lower peak and less total overall heat than

Portland cement. This reduces thermal gradients in the concrete, which prevents the

occurrence of micro cracking which can weaken the concrete and reduce its durability, and

was used for this purpose in the construction.

National Institute of Science & Technology (Autonomous) 13


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

D. APPEARANCE

In contrast to the stony grey of concrete made with Portland cement, the near-white color of

GGBS cement permits architects to achieve a lighter color for exposed fair-faced concrete

finishes, at no extra cost. To achieve a lighter color finish, GGBS is usually specified at

between 50% to 70% replacement levels, although levels as high as 85% can be used. GGBS

cement also produces a smoother, more defect-free surface, due to the fineness of the GGBS

particles.

E. STRENGTH

Concrete containing GGBS cement has a higher ultimate strength than concrete made with

Portland cement. It has a higher proportion of the strength-enhancing calcium silicate

hydrates (CSH) than concrete made with Portland cement only, and a reduced content of free

lime, which does not contribute to concrete strength. Concrete made with GGBS continues to

gain strength over time, and has been shown to double its 28-days.

Fig. 2 Fly-Ash and GGBS

3.3. Alkali Activators

National Institute of Science & Technology (Autonomous) 14


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

Geopolymericaction was induced in the brick element through alkaline activators such as

NaOH and Na2SiO3 which are commercially available ,by taking into account the high cost

of K-based chemicals. NaOH with 98% purity have been dissolved in distilled water to make

NaOH solution.Commercially available Na2SiO3 is in a solution form which was used as

such.

The Alkali Activators used in this experiment are

A. Sodium Hydroxide (NaOH) 12M

B. Sodium Silicate (Na2SiO3) 12M

Fig. 3 Alkali Activators

Mixing of Alkali Activators

Alkaline activator binder is a solution of sodium hydroxide and sodium silicate. The ratio of

sodium silicate to sodium hydroxide was kept at 2.5.

National Institute of Science & Technology (Autonomous) 15


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

Fig. 4 Mixing of NaOH and Na2SiO3

National Institute of Science & Technology (Autonomous) 16


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

4. METHODOLOGY

 Different priliminary properties such as specific gravity, water absorption etc of fly

ash, ggbs and rice husk ash was found out.

 Consistency of flyash and ggbs was found out to determine the water required for

paste.

 Initial and final setting time of fly ash was found out to find out whether mix sets at a

suitable rate for a particular work.

 Batching for different combinations of rice husk ash, flyash, ggbs and wooden

powder (by weight) was done.

 Mixing of materials was done according to the calculation.

 Cubes of size 70.6mm×70.6mm×70.6mm were casted.

 Then thereafter they were put in oven at a temp of 100 degree celcius for curing

purpose.

 Compressive strength was found out after 7, 14 & 28 days of curing respective.

4.1. Consistency Test of Fly-Ash

Consistency of flyash is defined as minimum quantity of water added in to form uniform

paste that provides sufficient viscosity and desirable strength for different type of structural

work. Adding less or excess amount of water in flyash causes reduction in its strength.

National Institute of Science & Technology (Autonomous) 17


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

Fig. 5 Vicat Apparatus

Result: The consistency of Flyash is found 37%.

4.1.1 Mould

Fig. 6. Mould

Dimension – (70.6mmx70.6mmx70.6mm)

4.1.2 Casting of Mould

National Institute of Science & Technology (Autonomous) 18


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

Fig. 7. Casting of Mould

National Institute of Science & Technology (Autonomous) 19


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

Bricks after 7 Days of oven curing

Fig. 8. Bricks after 7 Days of oven curing

National Institute of Science & Technology (Autonomous) 20


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

4.2 Testing of Brick Sample

1. COMPRESSIVE STRENGTH TEST

Compressive strength test, mechanical test measuring the maximum amount of compressive

load a material can bear before fracturing. The test piece, usually in the form of a cube,

prism, or cylinder, is compressed between the platens of a compression-testing machine by a

gradually applied load.

Fig. 9 Digital Compression Testing Machine

National Institute of Science & Technology (Autonomous) 21


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

5. RESULTS

SL. FLYASH GGBS RHA MIX DESIGN CS (N/ mm2)


NO.

1 50% 50% ----- M1 6.02N/mm2

2 50% ----- 50% M2 BROKEN

3 50% 20% 30% M3 14.58N/mm2

4 50% 30% 20% M4 15.36N/mm2

5 50% 40% 10% M5 14.306N/mm2

6 40% 40% 20% M6 14.030N/mm2

7 40% 30% 30% M7 12.25N/mm2

8 30% 50% 20% M8 8.04N/mm2

9 70% ----- 30% M9 5.9N/mm2

CS – Compressive Strength

National Institute of Science & Technology (Autonomous) 22


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

6. COST ANALYSIS

6.1 GEOPOLYMER BRICK


FOR 1 GEOPOLYMER BRICK
FLYASH REQUIRED 1KG = 0.8RS
GGBS REQUIRED 0.6KG= 0.15RS
RHA REQUIRED 0.4KG =0.1RS
ALKALINE ACTIVATOR = 0.16RS
MAN POWER + PROFIT = 2 RS
TOTAL = 3.21 RS
= 3.5 RS Approx
(after adding some additional cost)

National Institute of Science & Technology (Autonomous) 23


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

6.2 CLAY BRICK

FOR 1 CLAY BRICK


AFTER ADDING
( CLAY + COAL + MANPOWER)
COST OF 1 BRICK = 7RS

6.3 FLY ASH BRICK

FOR 1 FLY ASH BRICK


AFTER ADDING
( FLYASH + MACHINERY COST + MAN POWER )
COST OF 1 BRICK = 5.5 RS APPROX

From above cost analysis it is clear that geopolymer bricks are more cost effective
as compare to both Clay Brick and Flyash brick.

National Institute of Science & Technology (Autonomous) 24


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

6. CONCLUSION
Highest compressive is exhibited by the geopolyer brick with the F/A -50%, RHA – 20% and
GGBS – 30% (with a constant solid to liquid ratio 1.5) shows better result compared to other
trial mixes.

National Institute of Science & Technology (Autonomous) 25


PROPERTIES OF GEO-POLYMER BRICKS MADE WITH FLY-ASH, RICE-HUSK ASH AND WOODEN POWDER B.Tech 2021-2022

REFERENCES
[1] Kulkarni A, Raje S, Peerzada J and Rajgor M, (2014). “A miniscule endeavour for
accomplishing hypo sludge fly ash brick in Indian context”, International Journal of
Engineering Trends and Technology, 10, 361-365.
[2] Cusido J. A., Cremades L. V., Soriano, C. and Devant, M.(2015). “Incorporation of
paper sludge in clay brick formulation”: Ten years of industrial experience, Applied
Clay Science, 108, 191–198.
[3] Okunade E. A, (2008). “The effect of wood ash and sawdust admixture on the
engineering properties of a burnt laterite” – clay brick, Journal of Applied Science 8,
(1042-1048).
[4] Gaurav Goel and Ajay S Kalamdhad, (2017). “An investigation on use of paper mill
sludge in brick manufacturing”, Construction and Building Materials, 148, 334–343.
[5] Malhotra, S. K. and Tehri, S. I (1996). “Development of bricks from granulated blast
furnace slag, Construction and Building Materials”, 10, 191-1

National Institute of Science & Technology (Autonomous) 26

You might also like