ha

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DATE: /20

Ca

Ca
PAGE No
it-TL
Phormoceulico Hnalysis

naysis gt is lhe bhoch _o_bhomatcutigo humisly

a

a
in hih intludes Stieso oressideniiiLan7
rm

rm

rm
lauoniilication ddexminalion
s lhe tec.hniquewhich s usd iand.adalion_elc,
o f
ha

ha

ha
qualiialive cird
lqaniitaiive analsis a any Somble dubs or
dn-
lP

lP

lP
Coimp byuSinghls mtlhdas
Manual
el

el
2hernital analusis
w

w
3.insisumenlcl
9is a s ubes-Muclfadive or luaiilailive
re

re
Ca

1ualtative analysiudenliliccdon alhe (onstituleq

klemtrisax unional gous stnt Ca
in_oA subs.-
2Dugnlitalive analusi lhe amount o ogiven comp. s
a mixdure_ In
a

3.9dniiicationlheato oa
rm

m
coming duision d
aicirg-0Y
ar

ar
Stting apuàpait
ha

Ph

Ph
DR lec.hnique o analusis
lP

l
el

el

nsxumtnlalNonnslxumnlal
iValuacaic analuiis DBrloaicold
w

Hid aseNen quto iologitol

re

re

Redoz
9n-bo
Ca

Ca

Lomplexomerilx Nni malLsludies

heiption Mixabiosial hgy
a

a
m

m
ar

ar

ar

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tDATE: 20

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PAGE No

Ca

Ca
SbAdral gnaluSLS in Chemical
lColo imdry Hod- dcomm >AL chemical st
lLN-Sbudum (2os -Åoomm
TR
NMR
a

a
EIMaSS
rm

rm

rm
ha

ha

ha
CibChxomioghaphit
CaD |Panne chramaioqabhy.
lP

lP

lP
aperchxomaioaph
el

el
PHPTU
w

w
re

re
cb)olumn chxologopb.-
Ca

Ca
4as chYomoiogaphy
umn chiorhaoaaphy
HP1
hize exlation chxomabazxpl
EGL Elec txaphaisi
a

lecioche mcalmeihod.
rm

m
V
ar

ar
PondulOmftel
ha

leuiiomixu
Ph

Ph
lP

z|meromtla
l

6aoqoph
el

el
w

_V Hupanalot i.hniqucs.
re

re
Ca

Ca

|GC-MS=PS-
a

a
m

m
ar

ar

ar

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Ca

Ca
PAGE No

V Olhex mahds
ES-diential álylirg (alougmy
TGA- Îhexmo.
RIA- Rocio-Immund Hssau
a

a
E1ISA.
rm

rm

rm
Llock diogam an analylial
ha

ha

ha
iInStaumenialLLgnalysis
instumtnt shousing he sfimuluand 'measuxing
lP

lP

lP
Volumelic akalyLSThe nmeaLuxmenf ok olL Saln. ooa
el

el
non omanixaiion _af the analule. This_bxOKeSS S Call
w

w
ialion and the oln. in he uyete is called titaie
re

re
uther, it is ofou yps
Ca

ta id Lhse
saln. aue
n
Ca
belau9:0 a sauy asle
ainP"alez
Eid
easehydxoxy ion ad uxn Hems_bapir
edqHydochbaic acid, nitnic acid and salphuai acid
ap level gxedtey tha
a

aseohen diss.in 4nlr houe

rm

m
Seen asle bilex ad elspben
ar

ar
-4_aSe aneufxalizat ioh aid C ib the o ean_
ha

Ph

Ph
is a
lP

qufous91 Saln.
in ohich ihe sohueni in unir
q
l

mos1lyShoSn ihchemitaloxmui hSaln

ois lablet alt, Nac
el

el
w

w
re

re

Nan-0queaus SalngH on_0quepus soln. Ate aln in

u
Ca

Ca

hich inter is hof dhe. Saluenf eggE

da Clonlng
a

a
m

m
ar

ar

ar

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TDATE:
120
PAGE No
a

a
rm

rm

rm
bRdoxRtdon n inualuES_elechron lont Ah
ha

ha

ha
SDeCLes_galns lltcfxon oihea Sþrcias.
lP

lP

lP
Oomplexomily is_potiuular uselul or he deer.
el

el
amiz di mtlal ions
w

w
idh|Precibialiona Inmdologybretipikilion is an
re

re
xoclurto tht lordensarn 'o am iany pau
Ca

naalls_unde Q3auly he maih amL

include digale ainSled srouxaupel ard al Ca
pteplai

) Sbeclxal AmlgsisSbeciaol anagsig isanalusi isin-

tamsola Such
SpEcium Oxquinieo Xtlolec
a

auaniifizs as tnexqirsalveh inlues el_

rm

m
ar

s a ight
ar
ha

oolouimelyyzqt Senstive
dauitc usedLor
Ph

Ph
measuig Ke iransi-mtsing ihyough o liquid Samhle
lP

he demasux å lakiel sa The de inilnid

l

deueops uan
el

el

(onge ohe
olatux hat iiecui
sheCli Xgqntino a saln.
w

w
re

re
Ca

Ca
a

a
m

m
ar

ar

ar

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DATE: I20

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Ca
PAGE No

RIn{xa Ned speiroscobyThe

irdudlion aR_0dicnliop,
lh ofler Jt couEK_a ge a lezhniqurs mosily_hpsrd
on aboralion spechascobuLcan_be'uted do idkhfil
and ludy chtmital subs Samble pmay be alid Iimuid1
a

a
rm

rm

rm
Ld NHR Spectnascopy(Nulea ognci xeion (e)
ha

ha

ha
his I MO SCOP9-mos (omnionly Dnor0n a UR
-
lP

lP

lP
seinasop omgntli yeonaKesbe1SoPg
S QLoby Technque lo 6bseue local
mihilic-
el

el
Lirlc oAKOUNd
aömic nUrlei
w

w
re

re
eMass_ shectascopyi-Mausisþecthomehy is on aalyiic
Ca

Ca
Rhhique dhat measuae-he asS t6 chage xib oiokE

( homchqraphy gnolusischromeioqmphy is Sepexaily o

mix inš Indiuidual comonenls Ciing salionayyphaue
ond a unobile phase i
a

Phnar chxšmatogxoph
rm

m
ib olumn chxomafoaxobhy
ar

ar
ha

Ph

Ph
* Plpraa chxomab4aphyPbu chxoaio.gabhy Is_onelyhe
lP

o chxomaloqabh, 1thniqueIn ohichhe hlioai

l

l
el

el

phase 1s Oh alaTþlile.a
h mobile pháse tuK
HhroughSbiliorazyphase due. la apilaxyadion
w

hisuHnique as usec
oseaale.lhe milgH i
re

re

ooxthr allounirg 1Dsi

Ca

Ca

perhbomabqmph4is ón anallical meihod uscl lo

Se basale_Colouaed LHÉmllal OY us
a

a
m

m
ar

ar

ar

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DATE
I20
PAGE No

Ca

Ca
chyomatogaphy: CThib layea chaomabgauph
LLsA chxdnaloqiophy iechiqus Lud 8texcile
on-nlatule_miu
*HPTC chromatogxaphy -Hah_prrloymant ihin:lay
a

a
rm

rm

rm
homalogiabhy High þerdtmantt thin loyeà chsoio
obhy anYn
xoodn mahin - layea chxamctog ko
ha

ha

ha
mo eheenRnis con be mde to tHe basic mefhcd
s
ayen chkomiagaphy Cuiomatihe di{exe|
lP

lP

lP
ihin yenlbionaheved ad h alou
Sebsb hx he.
el

el
moe Quxale_Quantitaiive meCALIne menis
w

w
K alaumn_chomdogiabhy loloumn chO KLdhemttal
re

re
omandecbniqu dsed Ya Sebrateldivdual óp_
Ca

om a miluie 4i o uilhtr olbulr

Ca yp
4aschxomasqaph9f ia Lopommn yo
Lsed in ámlica chemislay pa Sebdiling árdfho-
analuaing camb. hatahbe hpauxRdoithau
decdhobrilion
a

a
rm

m
ar

ar
ibHPLC chxanmabgaabhyalHiah bealprmacc liquicd chxa.
ha

HP a oxm_o tolumn sannple mixoaduli,

Ph

Ph
bat umsa high pes thxough a cdumn_odh
lP

mderial
l

Chxommchi
el

el

ae Lalsooon as
w

j extlusian chxabaogabhy 9H
re

re

hale culaà sieue chxo ehoin (ohich maleculks in

saln aYe seþsale_by heir Sige od ih omt
Ca

Ca

(Ats_
mleculax L2eiah i SallaPpliedo1aige
alecualoxay iiLn.maleculaa tomplexies Such apratein.
and irlusinal mmex.
a

a
m

m
ar

ar

ar

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DATE: / 20
PAGE No

Ca

Ca
Gelecdaophoziks291 1s a
onms o chxo speíall
Lv Pxcluuion chxam. melod intohih
a sird ofSize aeSehxaldhynLomplishedLhy-
Shemitalombnenis 1he Ya-
i mmlbix, ohith
gl eltiiophacsis his get
S39n
abblying an eledaical CunenTh
a

a
rm

rm

rm
undion asamieCulad SiEVe.
ha

ha

ha
Melhods £lecliochemical methed
ase
Dlecihochemical
ihal Siud
in aah lulita chemaly
lP

lP

lP
aikgayaf Hethnluc
polential ad curden
an aballe by masuting
el

el
el Conidin nihe
comoneni is bn chemicatScienic
w

w
analuie
re

re
epialion_mdhodlthmom. baleuggoph.i
Ca

bedoaaphic melbod Visible specdxogaaphy Ca assspec

oupimiday
spe ullaault
9nomed
HMiscellanaus melhod. e
a

a
rm

m
axiiclethe analuses
ar

ar
Dxenta iheymaonalysis (O1A)
ha

5 lomming coloumlyLSS)
Ph

Ph
lP

Melhad oxpssirg Canonct cs maybeclelintd

l

in_a aln sn ocoln

pnesen
el

el

amunt ooluble
no of us Some ofthah axe
w

Can be izpustd in
re

re

Masspcemage9t my be delined a amount of

Ca

Ca

saluble_ in amiesin lodg of soln.

Mass 7 Mass oSolule laL too
Mass o Sdn
a

a
m

m
ar

ar

ar

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DATE: 20

Ca

Ca
PAGE No

No lumebercenhggf
delintd as bl a soluie Ín olf
bresentin loo mo bln
21oln.
a

a
rm

rm

rm
o ou A means lom a HCO_ is
q ol: saln Hc
in o n ojal
ha

ha

ha
kSent
lP

lP

lP
Mass by pl 2 I idelinedas mss o Salule bxatnt
el

el
7: mass o oluble (g X loo
msal
w

w
Val 1Sedn (m)
re

re
a o o molex aaluie a
Ca

Ca
Malaiy9t maybe delined
H2IPSeni n Jalh

ole ole Oaleg

uniis is mo

my as o. oale
a

Mohiyt be delined oalle

rm

m
esntn 1 Saluent m:mamolrs oolule
ar

ar
(h).
-ass_alvent
ha

unit hol
Ph

Ph
lP

ogamiegLiv ltntesent in eln

l

Nsraliym
el

el

N=m.oaam quiulen oselieu

w

Soln.
re

re

Nbco mtan odla eqiiuleni afsaluia in LLA

Ca

Ca

Seln:
Absmaliy ny mimiliy
Luheneiisacdly or isialy
a

a
m

m
ar

ar

ar

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DATE: 20

Ca

Ca
PAGE No

Mole aacdian mcle adion (nl n

here nH_male osolule
he mole aSolwint
a

a
it is unii quanliiy iri
rm

rm

rm
Hads permillian (ppm
ha

ha

ha
HPPm pais_af (ompannt Ylo
o.of arls a
lP

lP

lP
olal conp
in solnhi
el

el
almabheai ollutiion in.
w

w
1S alo in ppmby alu.nii
fubxessed
re

re
9n case amoles 1 may be Coniten as
mas a solut y
Ca

Ca
n case o ual
Jalume oallie oo
1al. acol
a

asonaliiIt is m: ofonmula mass in (q) peieni in prx

rm

m
rcan be2qual
ar

ar
oln omula massisqLual mlad msS dlia,
o
ha

mlasiy alsa indeadeni on lemp d

Ph

Ph
On ioDic Comp: ih uhicb ihexe is o txSiiance
lP

ale Cule
l

l
el

el

oxli oeiahoSaluien
wciahl X Ualaf saln ()_
w

nla
re

re

1
Ca

Ca

os
a

a
m

m
ar

ar

ar

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OATE: 120
PAGE No

Ca

Ca
HAxLmde iupb as dimtnsin w 24 ocid dis
1uig b. i oaliy.
Malax msa oH, CKaH =ag-
oght saluie
24-
a

a
omula tghisolufe 2 yko= 120
rm

rm

rm
2 2
ha

ha

ha
12aX1 Zao
lP

lP

lP
IAimoy Stondoy
el

el
diordaxd
w

w
daxdi3alion Luhen atggent is nt auailable inpu
re

re
Henmoln. oabproYKmu pomlily 1sODe hen_
Ca

Ca
ilnliongaindt a samaad _xoln. 7hi mozess
i alle
shdadixalich
R.q. me alfai
hydroxide
ándaxdiscclin
NaOH KOH an be
standard on-o Benz20it
_
xalic aid
a ep stoncoad Saln subsshauld Icarlisyallooi
a

CondtioN
rm

m
1 should be chtmicall PLLKe
ar

ar
ha

Lampolisdion oSubs must (hochond ezadly b i_

Ph

Ph
onmlula
lP

nam qLiuleni shauldbe as lanae aspossible_

l

l
el

el

_of_tondavdE
w

w
re

re

imazy StapdaxolIn Timly (ax tain chemica ane

Ca

Ca

LISEd
quenily in delined onc as inened soln. su
subs aKe
eaSeclAs bimay Saln.
aiarSondoiclsalnihrúld pxocessalloti
a

a
m

m
ar

ar

ar

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DATE:I 20
DA No
PAGE
a

a
19tlbress.mu bea_tau h odin pey o doy a
rm

rm

rm
in ueslole
ha

ha

ha
2he Suhs. should not be hygnastopic 6xididtd hy
lP

lP

lP
aioHeded by: (o
3 should be tapableabeingleased o imbuity
el

el
by quulitn alhe)_jut o Sisiuy
w

w
Eshould be xealidy saluble under Cóhdiion In_uhith
re

re
IRE is_emploued
Ca

Ca
5 mljoh ion shauld be nligible vaa eay d6 dede.
acuxaeby peximeni
olondaxy standazd H Sabs._uhichis ot bimay
slanda& in_ auxe is (olledsecondaxy shdad q
H4ali hdxoxIdES,_xganic OCld..
a

a
rm

m
ordaxd sal is one aving aclukate botb
ar

ar
ha

stxenqthunit is Male
Ph

Ph
lP

l
el

el
w

w
re

re
Ca

Ca
a

a
m

m
ar

ar

ar

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DATE: 20

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PAGE No

Ca

Ca
Kro Lis the. mead o eafiaiedSdif AWtntc ble

the cbseyed ax Callulild viluc aaqlaniKiks

hue value
he kmallex lhe (InOX_qheçiten js CUMNy AF aauSAL
o2 ps
a

a
rm

rm

rm
Delaminate or systemaiic1OThe ebox whieha
ha

ha

ha
oan tus Can_ beLOxIttd OY ao1didgnually
classlied a U
lP

lP

lP
Lnsiaumanal
el

el
20btalive
w

w
Salbo.dic
re

re
ddiliveaY Lonshn exox.
Ca

nuiumen tal eXOxuxy ingdument ma imited

auuXacuThey oginate in instaumtn iltelcan b Ca
auaidsd aiih pxohätalibxale on_o equlbhmtnt i haing
peperaueh _nagin maunfanante
eq diltih alkixic (iui ienp.defltnt_ondediclax
a

a
rm

m
xeralion standaxd isation _oflaxiaus mla)
ar

ar
normal sln._
ha

0x alit acid-
Ph

Ph
alamalax
lP

M.Loighi 26-
l

l
el

el

2H -
w

CcoH q o5 M_oralicacid o loom.

re

re

llcot
Ca

Ca

md-t Y bmalurity Y\jal._

loco
as M: ntY loa
a

a
m

m
ar

ar

ar

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TDATE:I20

Ca

Ca
PAGE No

looo

loed
a

a
rm

rm

rm
INormalL
ha

ha

ha
olN of oxali aud ox loo m
lP

lP

lP
Lt=D4 63

-
el

el
2
ocidniy loo
w

w
2
re

re
Coo
Ca

t63 X ool_Y
la6 Ca
0.63g-
2.Sulphuric aidE4SOu mLwt 92
a

ocidii2
rm

m
ar

ar
ha

Pasonal exxaxlanibe. axísed due to eath o o. or

Ph

Ph
lP

udg mtn ason_Oamly-

l

Rginompleledying o Sampleimppoper medsument

el

el

CSb be ayoidedby creself disdpline xepe

w

conRnlxajlion
re

re

IMthdic exxorlan _be_aised

Ca

Ca

{zdm non-ideal
hemical 00 phsicalbebautour oXragints.iSo xu
bpan hich a medhod is basee b 1
a

a
m

m
ar

ar

ar

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DATE: 20

PAGE No

Ca

Ca
tambleientss o themical bss o
inViatilily t bhowledg
an be nided_aith pioptr Londensalioh_S
abou exlotxi.mtnl.
a

a
rm

rm

rm
1

HdditiNL AYroIShes aKe_he. eaO x_Lhich 1rmaih

Consiant lhxaughout xy" ozphocesS
ha

ha

ha
lP

lP

lP
Can be_auaided olh bnopih Laie ua4menT
el

el
Contn
w

w
2Kahdom or indeler minat erxoxhe hhO dhich aI
re

re
o lootin_ o u Cqn't anided oà_ coTeled by us
Ca

Ca
bonRs indelinieoY lucraling ualues qpobltmns
r
In mchinsm SLuch a bh gnLomble lc
9ideaxee ofagement Bls muliible _mecksune mint|
oSam quaniiu
a

zegsion Relus o lasthess o tous ox mOre

rm

m
mtasuxnmenf lo ochalhe.
ar

ar
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eioe Lorigh.0 sample b limt dogf 3:24 in iach|

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Page 16 of 17
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Credits :- Jaspreet Kaur

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DATE: 120
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Website :- www.carewellpharma.in
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Credits :- Jaspreet Kaur