ENperiment Name /No.

:
Bynthe8is0 Asphun amlin Page No. 1
Date of O4I 2021
Aim AynthesuS oAShin

Aaratus Required Cenical tlask, blas hod, beake.

measutung cylincle and ofhetgental afparats
Chenucals Requireo daliayuc acid, bulphuuc acid
Hhanet, Methanel,Acektc anhydiud and Fehtuc
LChleude

Peineihal Felic
HemanA in 1817attemfuking
to nd a vcdug to ease hu truthes i
athitus uithout
taustng hebevere tmach
Urutatio, asociatesl utm he standaAd ant
athsuties diugsc that Hme, bocliwmn
halicytate Cause the ds coveyo
Ain
H nam Afin beteved to Jse clotir ed
ne A o Acet and shir e
Shirea he botomicalvame th
meadou8 weat plant rom thich balicylic
aad Lwag
vst vchemically isolated
Ahsin On e the oldest amel met
JMBeul dug nown. alucylates ahe ant'
yhettes é hey lowe the body
temhsetu COhe2 who has eve Aut
itle etect a he AemhaOtu natma
ali ctate also LOld avalgenc, whuch
elieves Cctain yhe hain

30

Teacher's Signature:
 o

OH

stutin -aLetoxy benzoic acid

oH

O c
C-OH H

oH
Ashin
CH,-C-OH
6alicc tud

A - O-H
7oH

:
C
o-H
CH - C

+ H
H
CHCOoH
 OH
OH2 13
I1CO eH 2
Fe
coOH t -2H
D'IFe.
oH
- o

son
ot oH
Calculateyns
Moles Daluey cluc acid 2 . 0 o oI4Y moles
138.12
Hence, moleS e Acetto Anhydride o. 0144X 2.7 o.o 38
(nam5 Acetc anhydude 0 - 0 388 X 102 - 08 g/mol
3.16
Volume Acettc Anhydrudla 3.96 3.4 mi
1.c8

Theeuucal yeild= 0.ol4 4 moles -2-594 gn ot

auet c Saly ycue a

hercentag e yreld = 34 x loo

2 534
Sl.66 .
 arTe/ Mo, Camlin Pago No.
fi
petitrent
Date

Poceduwo

) Taxe
lake) Laicyuc aud ane l'tonsjer it Lnto a
I50 m dy onucal ftask

ad2 Sauvalent eh acehc antydraide ( 3.67 m)

neazuing ytinder to h e 2inyic acid
Loyaurirgontal laxk Now add 5- d n
chLcnt. H,S04 to t h
Hask d tih
ll the
balicyiicacid disclved
eave the enckn mixu wndistubed l e
-20 ninut04

me uoue to he Hask and_&ue

mirue uand filie LUSinga uenoL

nn

e th old Suoduct om the kilte

d2iee h uude fnduct fn ml o ethanol

dutMled unte tleat on
add 1Srnl
uwntes. lyoth tl ya et a clea Soluuttom

toCopt in La c e bath
)ALow the soutlon
withoutdistubtvg

TeachersSignature
Experiment Name / No.:.
Synthest o Ashin Camlin |Page No. 2
Date ofl OyI 202

S)ilte the w hsoduct amd dlAy u

lacngin betuscon neets the
ahes Kenett the- k
hescennge yield
Qissolue aeu Cuystals the d u comhoud
n 0.5 m methame
and add uanaA
feclzsalutin Note_ the csl
chang
Keheit he Laleove test_ ui th
Salioyic acid bimila amount
amd note he tolei change
1o eteamine the meltna
Aid oint eky Salicytic

ObelkVatim
weghtk ur Cuystascbtaineo 1.34
tex addition methanntuanel teckz ceer
olution uesnained ight ellow

Resulk

pecentage yield A 51. 66 .

Meltina pint Lo acetyl Aalicylic a c i d

134 136 C

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Experiment Name / No:`yntheAs a %in Camlin p 3
Date1 0 4 | 2024

Foclg
Feclg test tonirms the absenc o phenduicgk0uh
n acetai dalicyic Lacid.

Acekglsaliquclic acid uas ynthesized om altul

ud

ecaukiama
ake h Aalicylic aud in dk conical laak
Conc HaSo &haulsl se handled uih caks
3Cybtal hould loegEntly dRied

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3O