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CE 321: PRINCIPLES OF REINFORCED CONCRETE

CONCRETE
MATERIALS AND PROPERTIES
By Dr. Ernesto Tan Anacta, BSCE, MSCE, Ph.D.CE

Lesson No. 1
FRESH CONCRETE

2. Identify the different workability and


1.1 Introduction consistency tests;
Although fresh concrete is only of transient 3. Study the correct procedures in dealing with
fresh concrete; and
interest, we should note that the strength of
concrete of given mix proportions is very 4. Identify the latest standards on
seriously affected by the degree of its terminologies, nomenclature, specifications,
compaction. It is vital, therefore, that the test methods and practice related to fresh
consistency of the mix be such that the concrete concrete;
can be transported, placed, compacted, and
finished sufficiently easily and without 1.3 Density
segregation. This lesson is, therefore, devoted
to the properties of fresh concrete which will Density, also called unit mass or unit weight in
contribute to such an objective. air, can be determined experimentally by using
ASTM standard C 138-17 or BS EN 12350-1:
It should be observed that the first three 2019. Theoretically, density is the sum of
ingredients (cement, aggregates and water) masses of all the ingredients of a batch of
discussed earlier are all essential ingredients of concrete divided by the volume filled by the
fresh concrete. concrete.

1.2 Lesson Objectives Alternatively, knowing the density of fresh


concrete, the yield per batch can be determined
After this completing this Lesson, you will be as the mass of all the ingredients in a batch
able to: divided by the density.
1. Familiarize the different properties and
behaviour of fresh concrete;
1.4 Workability and Consistecy The need for compaction becomes apparent
from a study of the relation between the degree
A concrete which can be readily compacted is of compaction and the resulting strength. It is
convenient to express the former as a density
said to be workable, but to say merely that
ratio, i.e. a ratio of the actual density of the given
workability determines the ease of placement
concrete to the density of the same mix when
and the resistance to segregation is too loose a
fully compacted. Likewise, the ratio of the
description of this vital property of concrete.
strength of the concrete is actually (partially)
Furthermore, the desired workability in any
compacted to the strength of the same mix when
particular case would depend on the means of
fully compacted can be called the strength ratio.
compaction available; likewise, a workability
The presence of voids in concrete greatly
suitable for mass concrete is not necessarily
reduces its strength: 5 per cent of voids can
sufficient for thin, inaccessible, or heavily
lower strength by as much as 30 per cent, and
reinforced sections.
even 2 per cent voids can result in a drop of
For these reasons, workability should be defined
strength of more than 10 per cent.
as a physical property of concrete alone without
reference to the circumstances of a particular Voids in concrete are in fact either bubbles of
type of construction. entrapped air or spaces left after excess water
has been removed. The volume of the latter
To obtain such a definition it is necessary to
depends primarily on the water/cement ratio of
consider what happens when concrete is being
the mix; to a lesser extent, there may be spaces
compacted. Whether compaction is achieved by
arising from water trapped underneath large
ramming or by vibration, the process consists
particles of aggregate or underneath
essentially of the elimination of entrapped air
reinforcement. The air bubbles, which represent
from the concrete until it has achieved as close
„accidental‟ air, i.e. voids within an originally
a configuration as is possible for a given mix.
loose granular material, are governed by the
Thus, the work done is used to overcome the
grading of the finest particles in the mix and are
friction between the individual particles in the
more easily expelled from a wetter mix than from
concrete and also between the concrete and the
a dry one.
surface of the mould or of the reinforcement.
These two can be called internal friction and
1.4.2—Factors Affecting Workability
surface friction, respectively. In addition, some
of the work done is used in vibrating the mould The main factor is the water content of the mix,
or in shock and, indeed, in vibrating those parts expressed in kilograms (or litres) of water per
of the concrete which have already been fully cubic meter of concrete: it is convenient, though
consolidated. approximate, to assume that, for a given type
and grading of aggregate and workability of
Another term used to describe the state of fresh
concrete, the water content is independent of
concrete is consistency which is taken to mean
the aggregate/cement ratio or of the cement
the degree of wetness; within limits, wet
content of the mix.
concretes are more workable than dry
concretes, but concretes of the same The effect of entrained air on workability
consistency may vary in workability. The ACI depends on the mix proportions.
definition of consistency is: “the relative mobility
or ability of freshly mixed concrete or mortar to If the water content and the other mix
flow”; this is measured by slump. proportions are fixed, workability is governed by
the maximum size of aggregate, its grading,
Some other related terms such as: flowability, shape and texture. However, the grading and
mobility, and the water/cement ratio have to be considered
Pumpability are also used. There is also a term together, as a grading producing the most
„stability‟ which refers to the cohesion of the mix, workable concrete for one particular value of
that is, its resistance to segregation. These water/cement ratio may not be the best for
terms do have specific meaning but only under a another value of the ratio. In particular, the
set of given circumstances; they can rarely be higher the water/cement ratio the finer the
used as an objective and quantifiable description grading required for the highest workability. In
of a concrete mix. actual fact, for a given value of water/cement
ratio, there is one value of the coarse/fine
1.4.1—The Need for Sufficient Workability aggregate ratio (using given materials) that
gives the highest workability. Conversely, for a
Concrete must have a workability such that given workability, there is one value of the
compaction to maximum density is possible with coarse/fine aggregate ratio which needs the
a reasonable amount of work or with the amount lowest water content.
that we are prepared to put in under given
conditions.
In practice, predicting the influence of mix the shear type, or even to collapse, and widely
proportions on workability requires care since, of different values of slump can be obtained in
the three factors, water/cement ratio, different samples from the same mix.
aggregate/cement ratio and water content, only
two are independent. It should be remembered, however, that with
different aggregates, especially a different
For instance, if the aggregate/cement ratio is content of fine aggregate, the same slump can
reduced, but the water/cement ratio is kept be recorded for different workabilities, as indeed
constant, the water content increases, and the slump bears no unique relation to the
consequently the workability also increases. If, workability as defined earlier. Moreover, slump
on the other hand, the water content is kept does not measure the ease of compaction of
constant when the aggregate/cement ratio is concrete and, as slump occurs under the self-
reduced, then the water/cement ratio decreases weight of the test concrete only, it does not
but workability is not seriously affected. reflect behaviour under dynamic conditions such
as vibration, finishing, pumping or moving
The last qualification is necessary because of through a tremie. Rather, slump reflects the
some secondary effects: a lower „yield‟ of concrete (Table 1.1).
aggregate/cement ratio means a higher total
surface area of solids (aggregate and cement) Table 1.1 – Values of slump
so that the same amount of water results in a
somewhat decreased workability. This could be Description of
Slump (mm)
offset by the use of a slightly coarser grading of Workability
aggregate. There are also other minor factors No slump 0
such as fineness of cement, but the influence of
this is still controversial. Very low 5 – 10

1.4.3—Measurement of Workability Low 15 – 30

Unfortunately, there is no acceptable test which Medium 35 – 75


will measure directly the workability as given by High 80 – 155
any of the definitions. Numerous attempts have
been made, however, to correlate workability Very high 160 to collapse
with some easily determinable physical
measurement, but none of these is fully An increase in slump may mean, for instance,
satisfactory although they may provide useful that the moisture content of aggregate has
information within a range of variation in unexpectedly increased; another cause would
workability. be a change in the grading of the aggregate,
such as a deficiency of sand. Too high or too
1.4.3.1—Slump Test low a slump gives immediate warning and
enables the mixer operator to remedy the
This is a test used extensively in site work all situation.
over the world. The slump test does not
measure the workability of concrete, although This application of the slump test, as well as its
ACI 116R-90 describes it as a measure of simplicity, is responsible for its widespread use.
consistency, but the test is very useful in
detecting variations in the uniformity of a mix of 1.4.3.2—Compacting Factor Test
given nominal proportions. The slump test is
prescribed by ASTM C 143-15a and BS 1881- There is no generally accepted method of
103: 1993. directly measuring the amount of work
necessary to achieve full compaction, which is a
If instead of slumping evenly all round as in a definition of workability.
true slump, one half of the cone slides down an
inclined plane, a shear slump is said to have The degree of compaction, called the
taken place, and the test should be repeated. If compacting factor, is measured by the density
shear slump persists, as may be the case with ratio, i.e. the ratio of the density actually
harsh mixes, this is an indication of lack of achieved in
cohesion in the mix. the test to the density of the same concrete fully
compacted.
Mixes of stiff consistency have a zero slump, so
that, in the rather dry range, no variation can be This test is described in BS 1881-103:1993 and
detected between mixes of different workability. in ACI 211.3-02 (Reapproved 2009), and is
Rich mixes behave satisfactorily, their slump appropriate for concrete with a maximum size of
being sensitive to variations in workability. aggregate up to 40 mm (or ½ in.).
However, in a lean mix with a tendency to
harshness, a true slump can easily change to
Unlike the slump test, variations in the
workability of dry concrete are reflected in a The use of this test is similar to that of the slump
large change in the compacting factor, i.e. the test, that is, routine checking of consistency for
test is more sensitive at the low workability end control purposes. This test is an alternative to
of the scale than at high workability. the slump test, over which it has some
Nevertheless, the compacting factor test advantages. In particular, the ball test is simpler
undoubtedly provides a good measure of and quicker to perform and, what is more
workability. important, it can be applied to concrete in a
buggy or actually in the form. In order to avoid
1.4.3.3—Remoulding Test the effects of a boundary, the depth of the
concrete being tested should be not less than
Developed by Powers, this test uses a jolted 200 mm (8 in.), and the least lateral dimension
table in which an assessment of workability is should be 460 mm (18 in.).
made on the basis of the effort involved in
changing the shape of a sample of concrete. 1.4.3.7—Compactability Test
The test is purely a laboratory one but is A compactability test was introduced by BS EN
valuable because the remoulding effort appears 12350-4:2019, which determines the reduction
to be closely related to workability. in volume of a loosely-packed concrete after
vibration in a cylinder. The degree of
1.4.3.4—Vebe Test compactability is the ratio of the height of the
cylinder to the height of the compacted concrete.
This is a development of the remoulding test in The compaction is effected by a vibrating table
which the inner ring of Powers‟ apparatus is or by an internal vibrator.
omitted and compaction is achieved by vibration
instead of jolting. The name „Vebe‟ is derived
1.4.3.8—Nasser’s K-tester
from the initials of V. Bährner of Sweden who
developed the test. The test is covered by BS Among the various attempts to devise a simple
EN 12350-3:2019; it is referred to also in ACI workability test, the probe test of Nasser
211.3-02. deserves mention. This test uses a hollow probe
19 mm (3/4 in.) in diameter with openings
Vebe is a good laboratory test, particularly from
through which mortar can enter the tube. The
very dry mixes. This is in contrast to the
probe is inserted vertically into fresh concrete in
compacting factor test where error may be
situ (and thus avoids using a sample). The
introduced by the tendency of some dry mixes to
height of the mortar in the tube after 1 minute
stick in the hoppers. The Vebe test also has the
and also the residual height following withdrawal
additional advantage that the treatment of
of the probe are measured.
concrete during the test is comparatively closely
related to the method of placing in practice. Both The K-tester has not been standardized and is
the Vebe test and the remoulding tests not widely used.
determine the time required to achieve
compaction, which is related to the total work 1.4.3.9—Two-point Test
done.
This test was initiated by Tattersall based on the
1.4.3.5—Flow Table Test flow of concrete described in the Bingham
model. Using a modified food mixer, techniques
This test, which was developed in Germany in
of torque measurement wherein data related to
1933, was covered by BS 1881-105:1984. The
the shear stress at a given rate of shear and to
test is appropriate for concrete of high and very
constants representing the yield stress, 0, and
high workability, including flowing concrete
which would exhibit a collapse slump, as well as plastic viscosity, , of the mix was
for mixes having a flow of 340 to 600 mm. experimentally developed.

If the concrete at this stage does not appear 1.4.4—Comparison of Tests


uniform and cohesive, this is an indication of a It should be said at the outset that no
lack of cohesiveness of the mix. comparison is really possible as each test
measures the behavior of concrete under
1.4.3.6—Ball Penetration Test different conditions.
This simple field, devised by J. W. Kelly and The compacting factor test is closely related to
known as the Kelly ball, consists of the the reciprocal of workability, whereas the
determination of the depth to which a 152 mm (6 remoulding, flow, and Vebe tests are direct
in.) diameter metal hemisphere, weighing 13.6 functions of workability.
kg (30 lb), will be made to sink under its own
weight into fresh concrete.
The Vebe test measures the properties of psi). These setting times are distinct from the
concrete under vibration as compared with the setting times of cement.
free-fall conditions of the compacting factor test
and the jolting in the remoulding and flow tests. The test method is prescribed by ASTM C 403-
All four tests are satisfactory in the laboratory, 16 and can be used for comparative purposes. It
but the compacting factor apparatus is also cannot be an absolute measure because the
suitable for site use. test is performed on mortar and not on the
parent concrete. British Standard BS 5075-1:
For specific mixes, the relation between 1982 (superseded by BS EN 480-1:2014) also
compacting factor and slump has been obtained, prescribes a stiffening time test.
but such a relation is also a function of the
properties of the mix. The relation between the
number of jolts in Powers‟ remoulding test and 1.6. Effect of Time and
slump is also only broadly defined. Temperature on Workability

The flow test is valuable in assessing the Freshly mixed concrete stiffens with time. This
cohesiveness and workability of very high
workability concrete or flowing concrete. should not be confused with setting of cement. It
is simply that some water from the mix is
The slump and penetration tests are purely absorbed by the aggregate if not saturated,
comparative and, in that capacity, both are very some is lost by evaporation, particularly if the
useful except that the slump test is unreliable concrete is exposed to sun or wind, and some is
with lean mixes, for which good control is often removed by the initial chemical reactions. The
of considerable importance. compacting factor decreases by up to about 0.1
during a period of one hour from mixing.
The slump test is periodically attacked as
useless and as a poor indicator of the strength The exact value of the loss in workability
of concrete. Such criticism may well be depends on several factors. First, the higher the
misplaced because the slump test does not initial workability the greater the slump loss.
purport to measure the potential strength of Second, the rate of loss of slump is higher in rich
concrete: the purpose of the slump test is to mixes. Furthermore, the rate of loss depends on
verify the uniformity of the slump from batch to the properties of the cement used: the rate is
batch; and no more. higher when the alkali content is high and when
the sulfate content is too low.
It has to be admitted that the slump test, which
represents a single rate of shear situation, The change in workability with time depends
cannot fully characterize the workability of also on the moisture condition of aggregate (at a
concrete. given total water content): the loss is greater
with dry aggregate due to the absorption of
A perfect, practical test for workability has yet to water by aggregate, as of course would be
be devised. Although this seems primitive, there expected. Water-reducing admixtures, although
is value in visual assessment of workability by they delay the initial stiffening of concrete, often
patting concrete with a trowel in order to see the lead to a somewhat increased rate of loss of
ease of finishing. Experience is clearly slump with time.
necessary but, once it has been acquired, the
„by eye‟ test, particularly for the purpose of The workability of a mix is also affected by the
checking uniformity, is both rapid and reliable. ambient temperature, although, strictly speaking,
we are concerned with the temperature of the
concrete itself. It is apparent that on a hot day
1.5 Stiffening of Concrete
the water content of the mix would have to be
It is possible to determine whether concrete increased for a constant early workability to be
maintained. The loss of slump in stiff mixes is
has stiffened to a given degree by testing mortar less influenced by temperature because such
sieved out of the concrete, using a 5 mm (No. mixes are less affected by changes in water
4 ASTM) sieve. A spring reaction-type probe, content.
known as Proctor probe, is used to determine
the times when the resistance to penetration is Because workability decreases with time, it is
3.5 MPa (500 psi) and 27.6 MPa (4000 psi). The important to measure, say, slump after a
former is referred to as initial setting time and predetermined time lapse since mixing. There is
indicates that the concrete has become too stiff value in determining slump immediately after the
to be made mobile by vibration. The time when discharge of the concrete from the mixer for the
the resistance to penetration has reached 27.6 purpose of control of batching. There is also
MPa (4000 psi) is the final setting time; the value in determining slump at the time of placing
compressive strength of concrete measured on the concrete in the formwork for the purpose of
a standard cylinder is then about 0.7 MPa (100
ensuring that the workability is appropriate for vibrator is increased. This is particularly so when
the means of compaction to be used. vibration is allowed to continue too long: with
many mixes, separation of coarse aggregate
1.7 Seggregation toward the bottom of the form and of the cement
paste towards the top may result. Such concrete
Segregation can be defined as separation of would obviously be weak, and the laitance
(scum) on its surface would be too rich and too
the constituents of a heterogeneous mixture so
wet so that a crazed surface with a tendency to
that their distribution is no longer uniform. In the
dusting might result. Laitance should be
case of concrete, it is the differences in the size
distinguished from bleed water, which is
of particles and in the specific gravity of the mix
considered in the next section.
constituents that are the primary causes of
segregation, but its extent can be controlled by It may be noted that entrained air reduces the
the choice of suitable grading and by care in danger of segregation. On the other hand, the
handling. use of coarse aggregate whose specific gravity
differs appreciably from that of the fine
It is worth noting that a higher viscosity of the
aggregate would lead to increased segregation.
fresh cement paste component militates against
the downward movement of the heavier
Segregation is difficult to measure quantitatively,
aggregate particles; consequently, mixes with
but is easily detected when concrete is handled
low water/cement ratios are less prone to
on a site in any of the ways listed earlier as
segregation.
undesirable. Another form of segregation is
There are two forms of segregation. In the first, possible: in a sloppy mix the cement paste tends
the coarser particles tend to separate out to run away from the centre of the table leaving
because they tend to travel further along a slope the coarser material behind. As far as proneness
or to settle more than finer particles. The second to segregation on over-vibration is concerned, a
form of segregation, occurring particularly in wet good test is to vibrate a and then to strip it and
mixes, is manifested by the separation of grout observe the distribution of coarse aggregate:
(cement plus water) from the mix. With some any segregation will be easily seen.
gradings, when a lean mix is used, the first type
of segregation may occur if the mix is too dry; 1.8 Bleeding
addition of water would improve the cohesion of
the mix, but when the mix becomes too wet the Bleeding, known also as water gain, is a form
second type of segregation would take place. of segregation in which some of the water in the
mix tends to rise to the surface of freshly placed
The grading influences segregation, but the concrete. This is caused by the inability of the
actual extent of segregation depends on the solid constituents of the mix to hold all of the
method of handling and placing of concrete. If mixing water when they settle downwards, water
the concrete does not have far to travel and is having the lowest specific gravity of all the mix
transferred directly from the skip or bucket to the constituents.
final position in the form, the danger of Bleeding can be expressed quantitatively as the
segregation is small. On the other hand, total settlement per unit height of concrete or as
dropping concrete from a considerable height, a percentage of the mixing water; in extreme
passing along a chute, particularly with changes cases, this may reach 20 per cent. ASTM C 232-
of direction, and discharging against an obstacle 14 prescribes two methods of determination of
– all these encourage segregation so that under total bleeding. The rate of bleeding can also be
such circumstances a particularly cohesive mix determined experimentally.
should be used. With a correct method of
handling, transporting and placing, the likelihood The initial bleeding proceeds at a constant rate,
of segregation can be greatly reduced: there are but subsequently the rate of bleeding decreases
many practical rules, which are presented in ACI steadily. Bleeding of concrete continues until the
304R-00 (Reapproved 2009). cement paste has stiffened sufficiently to put an
end to the process of sedimentation.
It should be stressed, however, that concrete
should always be placed direct in the position in If the bleeding water is remixed during finishing
which it is to remain and must not be allowed to of the top surface, a weak wearing surface,
flow or be worked along the form. This consisting of laitance, will be formed. This can
prohibition includes the use of a vibrator to be avoided by delaying the finishing operations
spread a heap of concrete over a larger area. until the bleed water has evaporated, and also
Vibration provides a most valuable means of by the use of wood floats and avoidance of
compacting concrete but, because a large overworking the surface. On the other hand, if
amount of work is being done on the concrete, evaporation of water from the surface of the
the danger of segregation (in placing as distinct concrete is faster than the bleeding rate, plastic
from handling) due to an improper use of a shrinkage cracking may result.
Some of the rising water becomes trapped on A higher temperature, within the normal range,
the underside of coarse aggregate particles or of increases the rate of bleeding, but the total
reinforcement, thus creating zones of poor bond. bleeding capacity is probably unaffected. Very
This water leaves behind air pockets or lenses, low temperature, however, may increase the
and because all the voids are oriented in the bleeding capacity, probably because there is
same direction, the permeability of the concrete more time prior to stiffening for bleeding to
in a horizontal plane may be increased. Hence, occur.
ingress of an attacking medium into concrete is
facilitated. A horizontal zone of weakness may The influence of admixtures is not
also be created. Trapping an appreciable straightforward. Superplasticizers generally
amount of bleed water must be avoided also decrease bleeding except at a very high slump.
because of the danger of frost damage, However, if they are used with a retarder,
especially in road slabs. increased bleeding may occur, possibly because
retardation allows more time for bleeding to
Some bleeding is unavoidable. However, in high
occur. If, at the same time, air entrainment is
elements, such as columns or walls, as bleed
used, its effect in reducing bleeding may be
water moves upwards, the water/cement ratio in
dominant.
the lower part of the element is reduced, but the
water trapped in the upper part of the now stiffer 1.9 Mixing of Concrete
concrete results in an increased water/cement
ratio there, and hence in a reduced strength. It is essential that the ingredients of concrete
are properly mixed so as to produce fresh
The bleed water can also travel upwards along concrete in which the surface of all aggregate
the surface of the form; if a channel is formed particles is coated with cement paste and which
due to some imperfection in the form surface, a is homogeneous on the macro-scale and
preferred drainage path is created with resulting therefore possessing uniform properties. Almost
surface streaking. Vertical bleed channels can invariably, mixing is effected by mechanical
also form in the interior of the concrete. mixers.

The tendency to bleeding depends largely on 1.9.1—Concrete Mixers


the properties of cement. Bleeding is decreased Concrete mixers must not only achieve the
by increasing the fineness of cement, possibly uniformity of the mix, just referred to, but they
because finer particles hydrate earlier and also must also discharge the mix without disturbing
because their rate of sedimentation is lower. that uniformity. In fact, the method of
Other properties of cement also affect bleeding: discharging is one of the bases of classification
there is less bleeding when the cement has a of concrete mixers.
high alkali content, a high C3A content, or when
calcium chloride is added. Several types exist. In the tilting mixer, the
mixing chamber, known as the drum, is tilted for
The properties of cement, however, are not the discharging. In the non-tilting mixer, the axis of
sole factor influencing the bleeding of concrete the mixer is always horizontal, and discharge is
so that other factors must also be considered. obtained either by inserting a chute into the
Specifically, the presence of an adequate drum or by reversing the direction of rotation of
proportion of very fine aggregate particles the drum (when the mixer is known as a
(especially smaller than 150 m (No. 100 sieve)) reversing drum mixer), or rarely by splitting of
significantly reduces bleeding. The use of the drum. There are also pan-type mixers, rather
crushed fine aggregate does not necessarily similar in operation to an electric cake-mixer;
lead to more bleeding than rounded sand. In these are called forced action mixers, as distinct
fact, when the crushed fine aggregate contains from the tilting and non-tilting mixers which rely
excess very fine material (up to about 15 per on the free fall of concrete in the drum.
cent passing the 150 m (No. 100) sieve),
bleeding is reduced, but the very fine material The efficiency of the mixing operation depends
must consist of crusher dust only, and not of on the details of design, but the discharge action
clay. is always good as all the concrete can be tipped
out rapidly and in an unsegregated mass as
Rich mixes are less prone to bleeding than lean soon as the drum is tilted. For this reason, tilting-
ones. Reduction in bleeding is obtained by the drum mixers are preferable for mixes of low
addition of pozzolanas or other fine material or workability and for those containing large-size
aluminium powder. The addition to mortar of fly aggregate.
ash or silica fume significantly decreases The nominal size of a mixer is described by the
bleeding. Air entrainment effectively reduces volume of concrete after compaction, which may
bleeding so that finishing can follow casting be as low as one-half of the volume of the
without delay. unmixed ingredients in a loose state. Mixers are
made in a variety of sizes from 0.04 m3 (1.5 ft3) the lowest average of pairs of readings for the
for laboratory use up to 13 m3 (17 yd3) known as four samples in each of three test batches; thus
truck or transit mixer. If the quantity mixed one bad mixing operation does not condemn a
represents less than one-third of the nominal mixer.
capacity of the mixer, the resulting mix may not
be uniform, and the operation would, of course, It can be added that tests on the uniformity of
be uneconomical. Overload not exceeding 10 mixing measure not only the performance of a
per cent is generally harmless. mixer, but can also be used to assess the
effects of a sequence of charging the mixer.
All the mixers considered so far are batch
mixers, in that one batch of concrete is mixed 1.9.3—Mixing Time
and discharged before any more materials are
added. As opposed to this, a continuous mixer On a site, there is often a tendency to mix
discharges mixed concrete steadily without concrete as rapidly as possible, and it is,
interruption, being fed by a continuous volume- therefore, important to know what is the
or weigh-batching system. minimum mixing time necessary to produce a
concrete uniform in composition and, as a result,
Other mixers include revolving-drum truck of satisfactory strength. This time varies with the
mixers, twin-fin truck mixers, and some type of mixer and, strictly speaking, it is not the
specialized mixers used in shotcreting and for mixing time but the number of revolutions of the
mortar for preplaced aggregate concrete. mixer that is the criterion of adequate mixing.
Generally, about 20 revolutions are sufficient.
1.9.2—Uniformity of Mixing Because there is an optimum speed of rotation
recommended by the manufacturer of the mixer,
In any mixer, it is essential that sufficient the number of revolutions and the time of mixing
interchange of materials between different parts are interdependent.
of the chamber takes place, so that uniform
concrete is produced. The efficiency of the mixer For a given mixer, there exists a relation
can be measured by the variability of the mix between mixing time and uniformity of the mix. It
discharged into a number of receptacles without is apparent that mixing for less than 1 to minutes
interrupting the flow of concrete. For instance, a produces an appreciably more variable
rather rigid test of ASTM C 94-17a (formally concrete, but prolonging the mixing time beyond
applicable only to truck mixers) lays down that these values results in no significant
samples of concrete should be taken from about improvement in uniformity.
1/6 to 5/6 points of a batch, and the differences
in the properties of the two samples should not The average strength of concrete also increases
exceed any of the following: with an increase in mixing time. The rate of
increase falls rapidly beyond about one minute
Density of concrete 16 kg/m3 (1 lb/ft3) and is not significant beyond two minutes;
sometimes, even a slight decrease in strength
Air content 1% has been observed. Within the first minute,
25 mm (1 in) when the however, the influence of mixing time on
ave. is under 100 mm strength is of considerable importance.
Slump (4”), and 40 mm when
As mentioned before, the exact value of the
the ave. is 100 to 150 minimum mixing time, which is given by the
mm (4” to 6”)
mixer manufacturer, varies with the type of mixer
% of aggregate and depends also on its size. What is essential
retained on a 4.75 mm 6% is to ensure uniformity of mixing, which generally
(3/16”) sieve can be achieved by a minimum mixing time
of 1 minute for a mixer size of 1 yd3 ( m3) and 15
Density of air-free additional seconds for each additional cubic yard
1.6%
mortar ( m3). This guidance is given both by ASTM C
Compressive strength 94-17a and by ACI 304R-00. According to
(ave. 7-day strength of 7.5% ASTM C 94-17a, the mixing time is reckoned
3 cyliders) from the time when all the solid materials have
been put in the mixer, and it is also required that
The sampling accuracy is assured by a limit on all the water has to be added not later than after
the average range of pairs. If two samplers in a one-quarter of the mixing time. ACI 304R-89
pair differ unduly, i.e. their range is an outlier, reckons the mixing time from the time when all
that pair of results can be discarded. the ingredients have been discharged into the
mixer.
The mixer performance is judged by the average
value of the difference between the highest and When lightweight aggregate is used, the mixing
time should be not less than 5 minutes,
sometimes divided into 2 minutes of mixing the The aggregate should be spread in a uniform
aggregate with water, followed by 3 minutes with layer on a hard, clean and non-porous base;
cement added. In general, the length of mixing cement is then spread over the aggregate, and
time required for sufficient uniformity of the mix the dry materials are mixed by turning over from
depends on the quality of blending of materials one end of the tray to the other and „cutting‟ with
during charging of the mixer: simultaneous feed a shovel until the mix appears uniform. Turning
is beneficial. three times is usually required. Water is then
gradually added so that neither water by itself
In the case of air-entrained concrete, prolonged nor with cement can escape. The mix is turned
mixing reduces the air content by about per hour over again, usually three times, until it appears
(depending on the type of air-entraining agent), uniform in color and consistency.
while a delay in placing without continuous
mixing causes a drop in air content by only It is obvious that during hand mixing no soil or
about per hour. On the other hand, a decrease other extraneous material must be allowed to
in mixing time below 2 or 3 minutes may lead to become included in the concrete.
inadequate entrainment of air.

Intermittent remixing up to about 3 hours, and in 1.9.5—Ready-Mixed Concrete


some cases up to 6 hours, is harmless as far as
strength and durability are concerned, but the Ready-mixed concrete is particularly useful on
workability falls off with time unless loss of congested sites or in road construction where
moisture from the mixer is prevented. Adding little space for a mixing plant and for extensive
water to restore workability, known as aggregate stockpiles is available, but perhaps
retempering, will lower the strength of the the greatest single advantage of ready-mixed
concrete. concrete is that it is made under better
conditions of control than are normally possible
No general rules on the order of feeding the on any but large construction sites. Control has
ingredients into the mixer can be given as they to be enforced but, since the central mixing plant
depend on the properties of the mix and of the operates under near-factory conditions, a really
mixer. Generally, a small amount of water close control of all operations of production of
should be fed first, followed by all the solid fresh concrete is possible. Proper care during
materials, preferably fed uniformly and transportation of the concrete is also ensured by
simultaneously into the mixer. If possible, the the use of agitator trucks, but the placing and
greater part of the water should also be fed compaction remain, of course, the responsibility
during the same time, the remainder of the water of the personnel on the site. The use of ready-
being added after the solids. mixed concrete is also advantageous when only
small quantities of concrete are required or
With some drum mixers, however, when a very when concrete is placed only at intervals.
dry mix is used, it is necessary to feed first some
water and the coarse aggregate, as otherwise its There are two principal categories of ready-
surface does not become sufficiently wetted. mixed concrete. In the first, the mixing is done at
Moreover, if coarse aggregate is totally absent a central plant and the mixed concrete is then
to begin with, sand or sand and cement become transported, usually in an agitator truck which
lodged in the head of the mixer and do not revolves slowly so as to prevent segregation and
become incorporated in the mix; this is known as undue stiffening of the mix. Such concrete is
head pack. If water or cement are fed too fast, or known as central-mixed as distinct from the
are too hot, there is a danger of formation of second category – transit-mixed or truck-mixed
cement balls, sometimes up to 70 mm (or 3 in.) concrete. Here, the materials are batched at a
in diameter. With small laboratory pan mixers central plant but are mixed in a mixer truck
and very stiff mixes, it has been found either in transit to the site or immediately prior to
convenient to feed first the fine aggregate, a part the concrete being discharged. Transit-mixing
of the coarse aggregate and cement, then the permits a longer haul and is less vulnerable in
water, and finally the remainder of the coarse case of delay, but the capacity of a truck used
aggregate so as to break up any nodules of as a mixer is only 63 per cent, or even less, of
mortar. the drum while for central-mixed concrete it is 80
per cent.
1.9.4—Hand Mixing
The main problem in the production of ready-
There may be rare occasions when small mixed concrete is maintaining the workability of
quantities of concrete have to be mixed by hand the mix right up to the time of placing. Concrete
and, because in this case uniformity is more stiffens with time and the stiffening may also be
difficult to achieve, particular care and effort are aggravated by prolonged mixing and by a high
necessary. An appropriate procedure is as temperature. In the case of transit-mixing, water
follows. need not be added till nearer the
commencement of mixing but, according to The properties of shotcrete are no different from
ASTM C 94-17a, the time during which the the properties of conventionally placed mortar or
cement and moist aggregate are allowed to concrete of similar proportions: it is the method
remain in contact is limited to 90 minutes; BS of placing that bestows on shotcrete significant
5328-3:1990 superseded by BS EN 206-1:2000 advantages in many applications. At the same
allows 2 hours. The 90-minute limit can be time, considerable skill and experience are
relaxed by the purchaser of the concrete; there required in the application of shotcrete so that its
is evidence that, with the use of retarders, the quality depends to a large extent on the
time limit can be extended to 3 or even 4 hours, performance of the operators involved,
provided the concrete temperature at delivery is especially in control of the actual placing by the
below 32C (90F). nozzle.

1.9.6—Retempering There are two basic processes by which


shotcrete is applied: the dry mix process and the
The loss of slump in fresh concrete is caused by wet mix process.
two factors: first, from the instant that cement
powder and water come into contact with one Either process can produce excellent shotcrete,
another, chemical reactions of hydration of but the dry mix process is better suited for use
cement take place. As these reactions involve with porous lightweight aggregate and with flash
fixing of water, less water is left to „lubricate‟ the set accelerators, and is also capable of greater
movement of individual particles in the mix, and delivery lengths, as well as of intermittent
second, in most ambient conditions, some of the operation. The consistency of the mix can be
mix water evaporates into the atmosphere and controlled direct at the nozzle, and higher
does so the more rapidly the higher the strengths (up to 50 MPa (or 7000 psi)) can be
temperature and the lower the ambient relative readily achieved. On the other hand, the wet mix
humidity. process gives a better control of the quantity of
We can see, therefore, that, if a specified mixing water (which is metered, as opposed to
workability is required at the point of delivery of judgement by the nozzle operator) and of any
the concrete after a certain passage of time, this admixture used. Also, the wet mix process leads
has to be ensured by the use of appropriate mix to less dust being produced and possibly to
proportions and transport arrangements. lower rebound. The process is suitable for large-
Occasionally, however, delays occur in transport volume operation.
or other mishaps prevent a timely discharge of Shotcrete exhibits durability comparable with
the concrete. If, in the meantime, a loss of slump ordinary concrete. The only reservation
occurs, the question arises as to whether the concerns the resistance to freezing and thawing,
slump can be restored by means of addition of especially in salt water. Air entrainment of
water coupled with remixing. Such an operation shotcrete is possible using the wet process, but
is referred to as retempering. achieving an adequately low bubble spacing
As retempering increases the original factor presents some difficulties. However,
water/cement ratio of the mix, it is arguable that addition of silica fume (7 to 11 per cent by mass
it should not be permitted where the original of cement) leads to adequate resistance to
water/cement ratio was directly or indirectly freezing and thawing.
specified.
1.9.8—Preplaced Aggregate Concrete
Nevertheless, retempering inevitably results in
some loss of strength compared with the original This type of concrete is produced in two stages.
concrete. A loss of 7 to 10 per cent was In the first operation, uniformly graded coarse
reported, but it can be much higher depending aggregate is placed in the forms; either rounded
on the amount of retempering water added to or crushed aggregate is suitable. The volume of
the mix coarse aggregate represents about 65 to 70 per
cent of the overall volume to be concreted. The
1.9.7—Shotcrete remaining voids are filled with mortar in the
second stage.
This is the name given to mortar or concrete
conveyed through a hose and pneumatically It is clear that the aggregate in the resulting
projected at high velocity onto a backup surface. concrete is of the gap-graded type. Optimum
The force of the jet impacting on the surface packing of the aggregate particles leads to great
compacts the material so that it can support theoretical advantages but is not necessarily
itself without sagging or sloughing, even on a achieved in practice.
vertical face or overhead. Other names are also The coarse aggregate must be free from dirt and
used for some types of shotcrete, e.g. gunite, dust because, since these are not removed in
but only sprayed concrete is sufficiently general. mixing, they would impair bond. Flushing the
aggregate in situ might cause an accumulation alternative names of poker- or immersion
of dust in the lower part of the pour which would vibrator.
become a zone of weakness. The aggregate
must be saturated and preferably gently Internal vibrators are comparatively efficient
inundated. because all the work is done directly on the
concrete, unlike other types of vibrators.
Preplaced aggregate concrete can be placed in
locations not easily accessible by ordinary 1.9.9.2—External Vibrators
concreting techniques; it can also be placed in
sections containing a large number of This type of vibrator is rigidly clamped to the
embedded items that have to be precisely formwork resting on an elastic support, so that
located. Likewise, because the coarse and fine both the form and the concrete are vibrated. As
aggregate are placed separately, the danger of a result, a considerable proportion of the work
segregation of heavy coarse aggregate is done is used in vibrating the formwork, which
eliminated. has to be strong and tight so as to prevent
distortion and leakage of grout.
Preplaced aggregate concrete is used also to
External vibrators are used for precast or thin in
provide an exposed aggregate finish: special
situ sections of such shape or thickness that an
aggregates are placed against the surfaces and
internal vibrator cannot be conveniently used.
become subsequently exposed by sandblasting
These vibrators are effective for concrete
or by acid wash.
sections up to 600 mm (24 in.) thick. When an
Preplaced aggregate concrete appears thus to external vibrator is used, concrete has to be
have many useful features but, because of placed in layers of suitable depth as air cannot
numerous practical difficulties, considerable skill be expelled through too great a thickness of
and experience in application of the process are concrete.
necessary for good results to be obtained.
1.9.9.3—Vibrating tables
1.9.9—Vibration of Concrete
This can be considered as a case of formwork
The purpose of compaction of concrete, known clamped to the vibrator, instead of the other way
also as consolidation, is to achieve the highest round, but the principle of vibrating the concrete
possible density of the concrete. The oldest and formwork together is unaltered.
means of achieving this is by ramming or
A vibrating table provides a reliable means of
punning, but nowadays this technique is very
compaction of precast concrete and has the
rarely used. The usual method of compaction is
advantage of offering uniform treatment. A
by vibration.
variant of the vibrating table is a shock table
When concrete is freshly placed in the form, air used sometimes in precast concrete
bubbles can occupy between 5 per cent (in a manufacture.
mix of high workability) and 20 per cent (in a
low-slump concrete) of the total volume. 1.9.9.4—Other Vibrators
Vibration has the effect of fluidifying the mortar
Various types of vibrators include surface
component of the mix so that internal friction is
vibrator which applies vibration through a flat
reduced and packing of coarse aggregate takes
plate direct to the top surface of the concrete; an
place. Continuing vibration expels most of the
electric hammer which can be used as a surface
remainder of entrapped air, but total absence of
vibrator when fitted with a bit having a large flat
entrapped air is not normally achievable.
area, say 100 mm by 100 mm (4 in. by 4 in.) and
Vibration must be applied uniformly to the entire can be used in compacting test cubes; a
concrete mass as otherwise some parts of it vibrating roller which is chiefly used for
would not be fully compacted while others might consolidating thin slabs; and vibrating screeds
be segregated due to over-vibration. However, and finishers for road construction; and a power
with a sufficiently stiff and well-graded mix, the ill float used mainly for granolithic floors to bind the
effects of over-vibration can be largely granolithic layer to the main body of the
eliminated. concrete, and is more an aid in finishing than a
means of compaction.
1.9.9.1—Internal Vibrators
1.9.10—Revibration
Of the several types of vibrators, this is the most
common one. It consists essentially of a poker, It is usual to vibrate concrete immediately after
housing an eccentric shaft driven through a placing so that consolidation is generally
flexible drive from a motor. The poker is completed before the concrete has stiffened.
immersed in concrete and thus applies
approximately harmonic forces to it; hence, the
It has been mentioned, however, that, in order to ASTM test methods for the determination of the
ensure good bond between lifts, the upper part cement and water contents have been
of the underlying lift should be revibrated, withdrawn; a so-called rapid analysis machine
provided the lower lift can still regain a plastic has not proved to be successful; chloride
state; settlement cracks and the internal effects titration for determining the water content and on
of bleeding can thus be eliminated. calcium titration for cement content is also used
but the fine part of calcareous aggregate cannot
This successful application of revibration raises be distinguished from the cement; the use of the
the question whether revibration can be more principle of buoyancy to determine the
generally used. On the basis of experimental water/cement ratio of a mix was used was also
results, it appears that concrete can be developed but it requires the knowledge of the
successfully revibrated up to about 4 hours from aggregate/cement ratio in the mix, which may
the time of mixing provided the vibrator will sink well be uncertain or unreliable.
under its own weight into the concrete.
Revibration at 1 to 2 hours after placing was Some other methods of determination of cement
found to result in an increase in the 28-day content of fresh concrete include pressure-filter
compressive strength. An increase in strength of method in which the material smaller than 150
approximately 14 per cent has been reported but m (No. 100) sieve is separated out by filtering
actual values would depend on the workability of and pressing dry; separation of cement by
the mix and on details of the procedure. flotation; a method using heavy liquid and a
centrifuge.
In general, the improvement in strength is more
pronounced at earlier ages, and is greatest in A recent development to determine the
concretes liable to high bleeding because the water/cement ratio is by the measurement of
trapped water is expelled on revibration. For the electrical resistivity using a probe immersed in
same reason, revibration greatly improves fresh concrete. This approach can be relied on
watertightness and also the bond between only with a given mix, the change in resistivity
concrete and reinforcement near the top surface indicating a departure from the expected w/c.
of the concrete as
trapped bleed water is expelled. It is possible Also, a method of determination of the water
also that some of the improvement in strength is content in fresh concrete by estimating the
due to a relief of the plastic shrinkage stresses degree of scattering of thermal neutrons emitted
around aggregate particles. by a source placed within the bulk of the
aggregate or within a sample of the mix was
2.0 Analysis of Fresh Concrete developed but calibration of its apparatus is
carried out in situ and is a time-consuming
In considering the ingredients of a concrete process. Use of microwave oven drying has
mix, we have so far assumed that the actual been proposed.
proportions correspond to those specified.
Modern batching plants can provide a record of 2.1 Self-Compacting (Self-
materials in each batch, but this does not Consolidating Concrete
include details of aggregate grading nor
sufficient information about the moisture content
of the aggregate. Moreover, if the batch record Self-consolidating concrete (or SCC) expels
could be totally relied upon in all cases, there entrapped air without vibration and travels
would be little need for testing the strength of around obstacles such as reinforcement, to fill
hardened concrete. However, in practice, all space within the formwork. This is useful with
mistakes, errors and even deliberate actions can intricate patterns of prestressing tendons and
lead to incorrect mix proportions, and it is poorly accessible areas near anchorages.
sometimes useful to determine the composition Vibration is noisy and therefore objectionable to
of concrete at an early stage; the two values of neighbors, especially
greatest interest are the cement content and at night and at weekends. Avoiding this noise is
water/cement ratio. It is the procedures for the second argument for the use of self-
determining these values that are referred to as consolidating concrete.
the analysis of fresh concrete.
There is also a third reason, and that is the
We can see that there exist no reliable and health effects of immersion vibrators on
practicable procedures for the measurement of operatives; holding the vibrator damages nerves
the water/cement ratio of fresh concrete. Indeed, and blood vessels and causes the so-called
there exists no test for the composition of fresh „white finger‟ or „hand vibration‟ syndrome which
concrete that is convenient and reliable enough is obviously socially undesirable.
to be used as a preplacement acceptance test.
Interestingly, the impetus for the development of
self-compacting concrete came from the desire
to minimize the use of unskilled labor. There is ASTM C173/C173M-16. Standard Test Method
no doubt that self-consolidating concrete will for Air Content of Freshly Mixed Concrete by the
become more widespread in the near future, Volumetric Method
even for lightweight concrete.
ASTM C231/C231M-17a. Standard Test Method
There are three desiderata for the concrete to be for Air Content of Freshly Mixed Concrete by the
classified as self-consolidating: flowing ability; Pressure Method
passing through closely spaced reinforcement; ASTM ASTM ASTM C403 / C403M – 16.
and resistance to segregation. Standard Test Method for Time of Setting of
Concrete Mixtures by Penetration Resistance
The means of achieving self-compacting
concrete are: the use of more fines (smaller than ASTM ASTM C232/C232M-14. Standard Test
Method for Bleeding of Concrete
600 m) than usual; an appropriate viscosity
achieved by a controlling agent; w/c of about ASTM C940-16. Standard Test Method for
0.4; use of a superplasticizer; a good aggregate Expansion and Bleeding of Freshly Mixed
shape and texture; less coarse aggregate than Grouts for Preplaced-Aggregate Concrete in the
usual (50% by volume of all solids). This may Laboratory
result in lower aggregate interlock, which is
ASTM C1059/C1059M-13. Standard
beneficial in shear resistance.
Specification for Latex Agents for Bonding Fresh
Clearly, very good batching controls are
To Hardened Concrete
necessary.
ASTM C1064/C1064M-17. Standard Test
Self-compacting concrete is very useful for Method for Temperature of Freshly Mixed
heavily reinforced members of any shape and Hydraulic-Cement Concrete
with bottlenecks, both in precast concrete and in ASTM C1688/C1688M-14a. Standard Test
situ. The only limitation is that the top surface Method for Density and Void Content of Freshly
must be horizontal. Mixed Pervious Concrete
ASTM C1798/C1798M-16e1. Standard
2.2 Latest Standards on Specification for Returned Fresh Concrete for
Terminologies, Nomenclature, Use in a New Batch of Ready-Mixed Concrete
Specification, Test Methods and
ASTM C1849/C1849M-17. Standard Test
Practice Related to Fresh Concrete
Method for Density and Air Content (Pressure
Method) of Freshly Mixed Roller-Compacted
The following are the latest standards on Concrete
terminologies, nomenclature, specifications, test ASTM D5971/D5971M-16. Standard Practice for
methods and practice related to fresh concrete. Sampling Freshly Mixed Controlled Low-
Strength Material
ACI 304R-00. Guide to Measuring, Mixing,
Transporting and Placing Concrete BS EN 12350-1:2019. Testing Fresh Concrete
by Slump Test
ACI 116R-90. Cement and Concrete
Terminology BS 1881-103:1993. Testing concrete. Method
for determination of compacting factor.
ACI 211.3-02. Guide for Selecting Proportions
for No-Slump Concrete BS 1881-105:1984. Testing concrete. Method
for determination of Flow.
ASTM C94/C94M-17a. Standard Specification
for Ready-Mixed Concrete BS EN 12350-3:2019. Testing Fresh concrete.
Vebe Test
ASTM C138/C138M-17a. Standard Test Method
for Density (Unit Weight), Yield, and Air Content BS EN 12350-4:2019. Testing Fresh concrete.
(Gravimetric) of Concrete Degree of Compactability
ASTM C143/C143M-15a. Standard Test Method BS EN 480-4:2014. Testing Fresh concrete.
for Slump of Hydraulic-Cement Concrete Determination of Capillary Absorption
ASTM C172/C172M-17. Standard Practice for BS 5328-3:1990. Specification for the
Sampling Freshly Mixed Concrete Procedures to be Used in Producing and
Transporting Concrete
BS EN 206-1:2000. Concrete. Specification,
performance, production and conformity.

Exam to follow…

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