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CONCRETE
MATERIALS AND PROPERTIES
By Dr. Ernesto Tan Anacta, BSCE, MSCE, Ph.D.CE
Lesson No. 1
FRESH CONCRETE
The flow test is valuable in assessing the Freshly mixed concrete stiffens with time. This
cohesiveness and workability of very high
workability concrete or flowing concrete. should not be confused with setting of cement. It
is simply that some water from the mix is
The slump and penetration tests are purely absorbed by the aggregate if not saturated,
comparative and, in that capacity, both are very some is lost by evaporation, particularly if the
useful except that the slump test is unreliable concrete is exposed to sun or wind, and some is
with lean mixes, for which good control is often removed by the initial chemical reactions. The
of considerable importance. compacting factor decreases by up to about 0.1
during a period of one hour from mixing.
The slump test is periodically attacked as
useless and as a poor indicator of the strength The exact value of the loss in workability
of concrete. Such criticism may well be depends on several factors. First, the higher the
misplaced because the slump test does not initial workability the greater the slump loss.
purport to measure the potential strength of Second, the rate of loss of slump is higher in rich
concrete: the purpose of the slump test is to mixes. Furthermore, the rate of loss depends on
verify the uniformity of the slump from batch to the properties of the cement used: the rate is
batch; and no more. higher when the alkali content is high and when
the sulfate content is too low.
It has to be admitted that the slump test, which
represents a single rate of shear situation, The change in workability with time depends
cannot fully characterize the workability of also on the moisture condition of aggregate (at a
concrete. given total water content): the loss is greater
with dry aggregate due to the absorption of
A perfect, practical test for workability has yet to water by aggregate, as of course would be
be devised. Although this seems primitive, there expected. Water-reducing admixtures, although
is value in visual assessment of workability by they delay the initial stiffening of concrete, often
patting concrete with a trowel in order to see the lead to a somewhat increased rate of loss of
ease of finishing. Experience is clearly slump with time.
necessary but, once it has been acquired, the
„by eye‟ test, particularly for the purpose of The workability of a mix is also affected by the
checking uniformity, is both rapid and reliable. ambient temperature, although, strictly speaking,
we are concerned with the temperature of the
concrete itself. It is apparent that on a hot day
1.5 Stiffening of Concrete
the water content of the mix would have to be
It is possible to determine whether concrete increased for a constant early workability to be
maintained. The loss of slump in stiff mixes is
has stiffened to a given degree by testing mortar less influenced by temperature because such
sieved out of the concrete, using a 5 mm (No. mixes are less affected by changes in water
4 ASTM) sieve. A spring reaction-type probe, content.
known as Proctor probe, is used to determine
the times when the resistance to penetration is Because workability decreases with time, it is
3.5 MPa (500 psi) and 27.6 MPa (4000 psi). The important to measure, say, slump after a
former is referred to as initial setting time and predetermined time lapse since mixing. There is
indicates that the concrete has become too stiff value in determining slump immediately after the
to be made mobile by vibration. The time when discharge of the concrete from the mixer for the
the resistance to penetration has reached 27.6 purpose of control of batching. There is also
MPa (4000 psi) is the final setting time; the value in determining slump at the time of placing
compressive strength of concrete measured on the concrete in the formwork for the purpose of
a standard cylinder is then about 0.7 MPa (100
ensuring that the workability is appropriate for vibrator is increased. This is particularly so when
the means of compaction to be used. vibration is allowed to continue too long: with
many mixes, separation of coarse aggregate
1.7 Seggregation toward the bottom of the form and of the cement
paste towards the top may result. Such concrete
Segregation can be defined as separation of would obviously be weak, and the laitance
(scum) on its surface would be too rich and too
the constituents of a heterogeneous mixture so
wet so that a crazed surface with a tendency to
that their distribution is no longer uniform. In the
dusting might result. Laitance should be
case of concrete, it is the differences in the size
distinguished from bleed water, which is
of particles and in the specific gravity of the mix
considered in the next section.
constituents that are the primary causes of
segregation, but its extent can be controlled by It may be noted that entrained air reduces the
the choice of suitable grading and by care in danger of segregation. On the other hand, the
handling. use of coarse aggregate whose specific gravity
differs appreciably from that of the fine
It is worth noting that a higher viscosity of the
aggregate would lead to increased segregation.
fresh cement paste component militates against
the downward movement of the heavier
Segregation is difficult to measure quantitatively,
aggregate particles; consequently, mixes with
but is easily detected when concrete is handled
low water/cement ratios are less prone to
on a site in any of the ways listed earlier as
segregation.
undesirable. Another form of segregation is
There are two forms of segregation. In the first, possible: in a sloppy mix the cement paste tends
the coarser particles tend to separate out to run away from the centre of the table leaving
because they tend to travel further along a slope the coarser material behind. As far as proneness
or to settle more than finer particles. The second to segregation on over-vibration is concerned, a
form of segregation, occurring particularly in wet good test is to vibrate a and then to strip it and
mixes, is manifested by the separation of grout observe the distribution of coarse aggregate:
(cement plus water) from the mix. With some any segregation will be easily seen.
gradings, when a lean mix is used, the first type
of segregation may occur if the mix is too dry; 1.8 Bleeding
addition of water would improve the cohesion of
the mix, but when the mix becomes too wet the Bleeding, known also as water gain, is a form
second type of segregation would take place. of segregation in which some of the water in the
mix tends to rise to the surface of freshly placed
The grading influences segregation, but the concrete. This is caused by the inability of the
actual extent of segregation depends on the solid constituents of the mix to hold all of the
method of handling and placing of concrete. If mixing water when they settle downwards, water
the concrete does not have far to travel and is having the lowest specific gravity of all the mix
transferred directly from the skip or bucket to the constituents.
final position in the form, the danger of Bleeding can be expressed quantitatively as the
segregation is small. On the other hand, total settlement per unit height of concrete or as
dropping concrete from a considerable height, a percentage of the mixing water; in extreme
passing along a chute, particularly with changes cases, this may reach 20 per cent. ASTM C 232-
of direction, and discharging against an obstacle 14 prescribes two methods of determination of
– all these encourage segregation so that under total bleeding. The rate of bleeding can also be
such circumstances a particularly cohesive mix determined experimentally.
should be used. With a correct method of
handling, transporting and placing, the likelihood The initial bleeding proceeds at a constant rate,
of segregation can be greatly reduced: there are but subsequently the rate of bleeding decreases
many practical rules, which are presented in ACI steadily. Bleeding of concrete continues until the
304R-00 (Reapproved 2009). cement paste has stiffened sufficiently to put an
end to the process of sedimentation.
It should be stressed, however, that concrete
should always be placed direct in the position in If the bleeding water is remixed during finishing
which it is to remain and must not be allowed to of the top surface, a weak wearing surface,
flow or be worked along the form. This consisting of laitance, will be formed. This can
prohibition includes the use of a vibrator to be avoided by delaying the finishing operations
spread a heap of concrete over a larger area. until the bleed water has evaporated, and also
Vibration provides a most valuable means of by the use of wood floats and avoidance of
compacting concrete but, because a large overworking the surface. On the other hand, if
amount of work is being done on the concrete, evaporation of water from the surface of the
the danger of segregation (in placing as distinct concrete is faster than the bleeding rate, plastic
from handling) due to an improper use of a shrinkage cracking may result.
Some of the rising water becomes trapped on A higher temperature, within the normal range,
the underside of coarse aggregate particles or of increases the rate of bleeding, but the total
reinforcement, thus creating zones of poor bond. bleeding capacity is probably unaffected. Very
This water leaves behind air pockets or lenses, low temperature, however, may increase the
and because all the voids are oriented in the bleeding capacity, probably because there is
same direction, the permeability of the concrete more time prior to stiffening for bleeding to
in a horizontal plane may be increased. Hence, occur.
ingress of an attacking medium into concrete is
facilitated. A horizontal zone of weakness may The influence of admixtures is not
also be created. Trapping an appreciable straightforward. Superplasticizers generally
amount of bleed water must be avoided also decrease bleeding except at a very high slump.
because of the danger of frost damage, However, if they are used with a retarder,
especially in road slabs. increased bleeding may occur, possibly because
retardation allows more time for bleeding to
Some bleeding is unavoidable. However, in high
occur. If, at the same time, air entrainment is
elements, such as columns or walls, as bleed
used, its effect in reducing bleeding may be
water moves upwards, the water/cement ratio in
dominant.
the lower part of the element is reduced, but the
water trapped in the upper part of the now stiffer 1.9 Mixing of Concrete
concrete results in an increased water/cement
ratio there, and hence in a reduced strength. It is essential that the ingredients of concrete
are properly mixed so as to produce fresh
The bleed water can also travel upwards along concrete in which the surface of all aggregate
the surface of the form; if a channel is formed particles is coated with cement paste and which
due to some imperfection in the form surface, a is homogeneous on the macro-scale and
preferred drainage path is created with resulting therefore possessing uniform properties. Almost
surface streaking. Vertical bleed channels can invariably, mixing is effected by mechanical
also form in the interior of the concrete. mixers.
Exam to follow…