S A T - S: Ilicone Sealant Pplication Raining Ite Team

SILICONE SEALANT
APPLICATION TRAINING - SITE TEAM
DOW CONFIDENTIAL - Do not share without permission

TODAY TOPICS
• Expectation
• Basic SI sealant Chemistry
• SI sealant product application
• PMS, program management system QA QC
• Substrate preparation
• Break 10 mins 1 hrs
• SI sealant site inspection method
• FAQ issue s on site
• Break 5 mins
• Innovation product 30 mins
• DOWSIL ™ 650
• DOWSIL™ Fire seals
DOW CONFIDENTIAL - Do not share without permission 2

TYPES OF JOINT SEALING MATERIALS (BASED ON CHEMISTRY)
• Organic, which consist of a carbon- • Inorganic, which consist of a noncarbon-

based polymer based polymer
(-C-C-O-C-C-) (-Si-O-Si-O-Si-)
– Single-component and – Silicone
multicomponent polyurethane
– Polysulfide
– Acrylic
– Modified silicone

WHY IS SEALANT CHEMISTRY IMPORTANT?
• UV light will degrade the carbon- Si-O 452 KJ/mol
carbon or carbon-oxygen bond of
an organic sealant C-O 357 KJ/mol
• There is not enough energy in
ultraviolet (UV) light to degrade UV±400 KJ/mol
the Si-O bond of a silicone
sealant
• Therefore, an organic sealant will
degrade in sunlight and a
silicone sealant will be
virtually unaffected

UV DEGRADATION

SILICONE VS. ORGANIC SEALANT
Heat &
Weather- Adhesion
Type Durability Cold Paintable Stain
ability (to Glass)
Resistance
Silicone 5 5 5 5 1 1
Modified
Silicone
4 4 3 1 4 4
Polysulfide 3 4 3 3 4 5
Polyurethane 4 3 3 1 5 5
Acryl 2 3 2 1 5 5
Excellent 5 1 Poor
Silicone has a lot of excellent features! But not perfect…
DOW CONFIDENTIAL - Do not share without

DOW CONFIDENTIAL - Do not share without permission permission 12
STAINING AND STREAKING
staining streaking

คำแนะนำในกำรเลื
1 อกสินค้ำ - ผนังนอกอำคำร
structural:
DS 983, DS 995, DS 795, DS 121
IG secondary seal
DS 982, DS 3362
Weather sealing
DS 791, DS 991, DS 793-T

SEALANT CLASSIFICATION: ONE PART VS TWO PART
1 part : all-in-one [ex :DS 795, DS 791]
2 part : Part A + Part B [Ex : DS 983, DS 3362]
Hotmelt [1-part]: applied at high temp [Ex : DS InstantGlaze]
Cure system
1 part : cure with the humidity from the air 2 part : reaction between base and catalyst,
no need of the humidity
From Outside From Inside

Cured Sealant Cured Sealant
15 mm
Max
Un-cured Sealant
Un-cured Sealant
DOW CONFIDENTIAL - Do not share

without permission
JOINT DESIGN CONSIDERATION

SEALANT APPLICATION CONSIDERATION: CURE REQ’T
▪ 1 part ▪ 2 parts
▪ One component (795, 995, 791, 991) ▪ Two components (983, 982, 121)
▪ Factors affecting curing rate of 1-part product: Joint • 2 part products have chemical curing. Curing starts
Depth Temperature and Humidity once the base and the C/A are mixed.
• Spacers and backer rods. • Can fully cure deep section joints.
• Full adhesion is typically achieved fully within 1-3 days
• Deep section sealant must be given enough time to
release by-products during time to avoid reversion

DOWSIL™ Structural Silicone Sealants
One/2 part Movement remark
+-
DS 791 Weather One 50 Typical WS
Seal
DS 793-T Weather One 25 Translucent
Seal Color
DS 991 Weather One 50 Low
Seal staining
DS 795 Structure One 50 Typical
SSG
DS 983 Structure Two 25 Factory
SSG
DS 995 Structure One 50 Bomb blast
DS 121 Structure Two 25 Site SSG
DS 982 Structure Two 25 IGU seal

DOWSIL™ 121 STRUCTURAL GLAZING SEALANT
▪ 2-part Structural Glazing Silicone

▪ On-site bonding, repair Glazing, new constructions,
Weathersealing
▪ Featuring a unique 1- to -1 (“121”) mix ratio
▪ simplified solution that eliminates the need for
specialized pumps and mixing equipment
▪ Minimizes quality assurance issues

LIFE MATTERS

DOW’S PROJECT MANAGEMENT SYSTEM (PMS)
PMS = Quality Check and Systematic Approach for Quality Seal

PRINT REVIEW: DESIGN CONSIDERATIONS
Structural Glazing
•Dimensions
• Sealant Bite = 6mm or computed value considering loads,
whichever is higher
• Glueline = 6mm or computed value considering thermal dilatation,
whichever is higher
• The bite to thickness ratio should be between 1:1 and 3:1
GLUELINE
•Other Aspects
BITE
• For 1 part SG sealant, maximum of 15mm bite. If the bite is more
than 15mm, one must use open cell spacer tape.
• L-joints → Monolithic Glass = Ok!
• L-joints → IGU= Not Ok! (use Split Joint)

FAILURE EXAMPLES
Bad Design Bad Sealant
• Water
Other • Earth
Bad Installation Factors Quake

MATERIAL TESTING
• Adhesion Test With

Primer
Without
Primer
• Compatibility test
• Staining Test

QUALITY ASSURANCES: FACTORY GLAZED SSG
Butterfly Test การทดสอบพับกระดาษเป็ นผีเสื้อ
• Must be performed after each pump start-up or container change. ทดสอบทุกครัง้ ที่มีการเปลี่ยนถัง
• This test verifies proper mix of the two-component sealant. เพื่อการทดสอบตรวจสอบการผสมกันของ ถังเล็กและถังใหญ่
Snap Time Test การทดสอบการแห้งตัวของ ซิลิโคน

• Must be performed after each pump start-up or container change. ทดสอบทุกครัง้ ที่มีการเปลี่ยนถัง
• Is used to determine if the mix ratio is correct and whether the sealant is curing properly เพื่อการทดสอบดุการ
แห้งตัวของวิลิโคน
Snake Test การยิงทดสอบเป็ นรูปงู

• Troubleshooting step to determine if the inconsistency in mix and ratio is due to the pump. เพื่อยิงทดสอบเวลา
มีปัญหาเรื่องการผสมกันของ base & catalyst ที่ไม่เหมาะสม สืบเนื่องมาจากสาเหตุต่างๆ
Mix Ratio Test การทดสอบการผสม

• Can be performed to further investigate problems with mix or snap time ใช้ทดสอบเมื่อมีปัญหาเรื่องส่วนผสมที่ไม่ลงตัวและ
snap time ที่มีปัญหา
• This test can be performed routinely by the customer although Dow Corning does not require it on a
routine basis.
Peel-in Adhesion Test การทดสอบการดึงจากตัวอย่าง
• The most effective daily test to verify sealant adhesion to a substrate and should be performed on all
substrates to which the sealant is expected to have adhesion at the following intervals:เป็ นวิธีที่มีประสิทธิภาพที่สดุ
ผูใ้ ช้ควรทาการทดสอบกับทุกวัสดุที่ใช้ในงาน
Deglazing Tests การแกะแผงเพื่อตรวจสอบ :ซิลิโคน ที่ช้ในแผง

26
permission
DEGLAZING TEST ( STRUCTURAL SILICONE SEALANT APPLICATION )
Elements to consider:
• Structural bite dimension
measurement.
• Glueline thikness dimension
measurement.
• Peel adhesion on all substrates.
• Sealant uniformity of cure and sealant
mix.
• Absence of bubbles or air entrapment
in the sealant.

WARRANTY TYPE ชนิ ดของใบร ับประกัน

TOP 20 HIGH RISE BUILDINGS - SEALANT BRAND
Reported by CTBUH _ Council of Tall Building and Urban Habitat
✓ 70% uses DOW sealant

SURFACE PREPARATION

CLEANERS AND PRIMERS: COMMON SUBSTRATES
Common Substrates Cleaning Solvent Primer (if needed) Approved for SG?
Aluminum
Mill Finished IPA Primer 1200 OS No
Analok IPA Primer 1200 OS Yes
Anodised IPA Primer 1200 OS Yes
Chromate IPA 1200 OS Yes
Powdercoated WS/MEK/Xylene/Toluene Primer C Yes
PvDF WS/MEK/Xylene/Toluene Primer C Yes
Steel
Carbon Steel IPA Primer 1200 OS No
Galvanized Mild Steel IPA Primer 1200 OS No
Painted Steel IPA Primer C No
Stainless Steel (Gr. 316) IPA Primer 1200 OS Yes
Glass
Clear IPA Primer 1200 OS Yes
Tinted IPA Primer 1200 OS Yes
Hard Coated - Low E IPA Primer 1200 OS Yes
Soft Coated - Low E IPA Primer 1200 OS Yes (Edge Deleted)
Fritted IPA Primer 1200 OS/Primer C Yes
Dow Restricted 31
STEEL COATING – DURABILITY

SURFACE PREPARATION
Dow Restricted 33
CLEANING CONSIDERATIONS: 2-CLOTH CLEANING
MAGNIFIED X-SECTION OF EXTRUSION FACE
DIRT & OIL WAX LAYER
https://www.researchgate.net/figure/SEM-
images-of-the-PVdF-polyurethane-interface-
exposed-by-ultra-low-angle-microtomy-
a_fig6_227196496
EXTRUSION
Ref :
https://www.flickr.com/photos/zeissmicro/2427890
0649
Dow Restricted DOW RESTRICTED 34

• The First Stage is performed with a clean, white, lint free cloth soaked
in a cleaning solvent.
• The Cloth is used to vigorously rub the paint surface.
• The solvent lifts the waxes, dirt and oil from the surface and suspends
them in solution.
Dow Restricted 35
• The traces of solvent and dirt are then removed with a second wipe
using a clean dry cloth
Dow Restricted 36
PRIMER APPLYING
3!
37
permission
PRIMER APPLYING
3!

PRIMER APPLYING
Layer of primer
การใช้รองพืน้ ทีถ่ กู ต้อง

permission

PRIMER APPLYING
Too much primering , creating too many layers which compromise
the adhesion with silicone
การใช้รองพืน้ ทีไ่ ม่ถกู ต้อง

Excessive primer application , reducing the adhesion performance
การใช้รองพืน้ ทีไ่ ม่ถกู ต้อง

Top 3 reasons for application failure*: Workmanship
Workmanship
Workmanship

BREAK 15 MINS
Month Year 43
SITE INSPECTION
• Assess sunny versus shady places Factors
• Look at the sidewalks if there is an overhang • Product selection
I. Do they look bad in the sun, good in the • Substrates
shade?
II. Take a cut in each place, squash it • Cohesion and Adhesion failure
III. Measure the physical material conditions, Substrate Preparation
width, shore ness, elongation, elastic • Sealant Movement capability
recovery • Substrate & Sealant material strength
• others external factor
• Product expired

ADHESION CHECK ON SITE
• Nondestructive test –
continuous - example
• Apply masking tape
• Use probing tools
• Depressing the sealant
along the bead and record
the sealant hardness /
adhesive / Cohesive
Failure / Elongation
• Mark in on the masking
tape
• Destructive test – 6
inches
• Video – DOW790 US
• Cut bond lines as close as
possible
• Cut along 6 inches
• Pull 90 degree
• It passes if cohesive
failure happens
• Check cut profile , rod,
cleanliness

DEGLAZING TEST ( STRUCTURAL SILICONE SEALANT APPLICATION )
Elements to consider:
• Structural bite dimension
measurement.
• Glueline thikness dimension
measurement. Peel adhesion
on all substrates.
• Sealant uniformity of cure and
sealant mix. Absence of
bubbles or air entrapment in
the sealant. มี

STORAGE CONDITIONS

SILICONE SEALANT PRODUCT STORAGE CONDITIONS
Quality Assurances: Storage & Shelf Life
Material Storage Temp ◦C Shelf Life (months)

DC 795 below 27 12
DC 995 below 30 18
DC 983 Base below 30 12
DC 983 C/A below 27 12
DC 121 below 30 12
DC 991 below 30 12
DC 791 below 30 12
DC 688 below 30 12
Panelfix 896 below 30 12
Primer 1200 OS* below 32 12

Primer C OS below 32 18
Primer P below 26 12

STRUCTURAL GLAZING AND INSULATING GLASS
APPLICATION AND QUALITY CONTROL – USED BY DATE ?

TEST BEFORE USE ? ( WS )
Skin over time & Elastomeric test
• Spread sealant bead 1mm on the
plastic sheet
• Tap sealant with finger every few
minute.
• Sealant should not be adhered to
the finger after 3 hours, if not
material should not be used
• After 24 hours, the sealant should
be able to remove out from the
sheet

UNCURED SEALANT

Q&A
• what can we inspect from the
sealant application on site
• bubble from the backer rod
• surface temperature
• material usage calculation
• fresh concrete
• bubble occurring
• stain on glass
• joint unfilled 100%
• material test on site

1. what can we inspect from the 1. Physical check, shore hardness, color,
sealant application on site hardening, powdering ?
2. bubble from the backer rod
3. surface temperature
4. material usage calculation
5. fresh concrete
6. bubble occurring
7. stain on glass
8. joint unfilled 100%
9. material test on site

SEALANT HARDENING

BACKER ROD OUTGAS
1. what can we inspect from the

• Do not poke backer rod with
sharp objects
5. fresh concrete
6. bubble occurring
7. stain on glass

BACKER ROD OUTGAS

3. surface temperature 3. Temperature at surface of glass /
4. material usage calculation aluminum should not exceed 50”c ( when
5. fresh concrete surrounding temp is around on 43’c )
6. bubble occurring
7. stain on glass

sealant application on site 10x10 mm, 500 ml = 5 meters ...
( not include 10% waste. )
4. material usage calculation 10x10 mm, 600 ml = 6 meters ...
5. fresh concrete ( not include 10% waste. )
6. bubble occurring
7. stain on glass
8. joint unfilled 100% 20 x10 mm, 500 ml = 2.5 meters ...
( not include 10% waste. )

5. fresh concrete
6. bubble occurring
7. stain on glass

5. fresh concrete
6. Micro bubble occurring
7. stain on glass

• Working time of Cleaning Solvent is after 10
5. fresh concrete
mins but not exceed than 4 hours, can check
6. bubble occurring with using finger to rub the surface
7. Working time of primer & cleaner
8. stain on glass
• Working time of Primer is within 15 mins but not
exceed 1 hour

5. fresh concrete
6. bubble occurring
7. stain on glass

5. fresh concrete
6. bubble occurring
7. stain on glass

5. fresh concrete
6. bubble occurring
7. stain on glass

DOWSIL™ 650 PPC
Dow Restricted 65
คุณสมบัตขิ องผลิตภัณฑ์ DOWSIL™ 650 Protective Peelable
Coating | Dow Inc.
Recommended thickness for glass substrate

ความหนาของ coating ที่แนะนา
Month Year 66
WHY USE A PEELABLE PROTECTION FOR GLAZING SYSTEM & PANELS
Designed to provide Protection Skin for valuable façade system and

panels during storage, transport and throughout on-site installations
✓ Minimizes dirt, scratches, corrosion,

debris, damages
✓ Reduce cleaning with surface
protection.
✓ Reduce need to repair, replace
expensive panels
✓ Save time & money.
Month Year 68
Month Year 69
DOWSIL™ 650 PROTECTIVE PEELABLE COATING
DURABILITY AND PERFORMANCE AFTER OUTDOOR EXPOSURE
Natural weathering Outdoor Exposure Aging Test under UV Chamber

(UVA 340nm), 45C UV test
Day 1 6400 hours 8600 hours

GLASS NANO COATED TESTING WITH DS 650
650 can be applied on Nano coating (Hydrophobic Technology) without hurting the glass surface and not adversely affecting
the water beading capability of the nano coating.
Comparison of Beading Effect on glass surface Comparison of Beading Effect on glass surface
applied with 650 and without 650 – UV Condition applied with 650 and without 650 – RT Condition
DOW CONFIDENTIAL - Do not share without permission August 2019 71

DOWSIL™ 650 PROTECTIVE PEELABLE COATING
COMPATIBLE SYSTEM WITH DOWSIL™ SEALANTS.

Extension lab testing to ensure compatibility (ASTM C1084)
DOWSIL™ FIRE-RATED
SEALANTS
• SMOKESEAL 800 SL
• FIRESTOP 700 SILICONE
SEALANT

DOWSIL™ SMOKE SEAL 800SL | FIRE RESISTANCE TESTING
▪ Bite: 6 to 50 mm, thickness: 2 mm;

Bite: 6 to 150 mm, thickness 6-10 mm
▪ Single joints only
▪ Backing material: MW and PU/PE
▪ Tested without metal bracket (also covers
with bracket)
▪ Tested with PE (also cover PU) backer rod
▪ Up to EI 240 depending on configuration
Photo taken during test Reference Project : OCBC project

Indonesia

DOWSIL™ FIRESTOP 700 SILICONE SEALANT | CHARACTERISTICS & APPLICATION
▪ A low-modulus, one-part, neutral-curing silicone

➢ Excellent adhesion to most porous and non-porous surfaces
➢ Joint movement capability (±50%) according to EN ISO 11600
▪ Application
➢ Working time: 15 minutes
➢ TFT: 1.5hours
▪ Certified for
➢ Fire rated horizontal and vertical linear joints in walls
(EN1366-4 and BS476-22)

DOWSIL™ FIRESTOP 700 SILICONE SEALANT | FIRE RESISTANCE TESTING
▪ Horizontal and vertical linear joints in wall (150 mm) applications
▪ Bite ranging from 10 to 50 mm, thickness from 10 to 25 mm
▪ Single and double joints
▪ Backing material: MW and PU/PE
▪ Up to EI 240 min depending on the configuration

CONCLUSIONS

DETAILS PREVAIL
Performance (E, I) influenced by:
Construction parameters:
• Wall material and thickness
• Backing material (MW or PE/PU rod)
• Support elements for backing
• Compression and thickness of MW
Joint parameters: Replacement/substitution/extension of the details is subject to

review and authorization:
• Joint bite and thickness typically less onerous should be allowed
• Joint orientation (vertical or horizontal)
• Single or double joints Please contact your local Dow Technical Specialist to review your
project and our certification range
• Movement or static
Penetration parameters:
• Diameter
• Separation (grouped/shattered)
• Sheathing material
• position (corner/middle)

THANK YOU
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thỏa thuận được ký kết bởi các đại diện được ủy quyền của Dow và của quý công ty. Bất kỳ dẫn obligations, and is subject to change without notice to you. The creation of binding obligations will occur
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SILICONE SEALANT

APPLICATION TRAINING - SITE TEAM

DOW CONFIDENTIAL - Do not share without permission

DOW CONFIDENTIAL - Do not share without permission 2

• Organic, which consist of a carbon- • Inorganic, which consist of a noncarbon-

DOW CONFIDENTIAL - Do not share without permission 9

DOW CONFIDENTIAL - Do not share without permission 10

DOW CONFIDENTIAL - Do not share without permission 11

Silicone has a lot of excellent features! But not perfect…

DOW CONFIDENTIAL - Do not share without

DOW CONFIDENTIAL - Do not share without

DOW CONFIDENTIAL - Do not share without permission

From Outside From Inside

DOW CONFIDENTIAL - Do not share

DOW CONFIDENTIAL - Do not share without permission 16

DOW CONFIDENTIAL - Do not share without permission 17

DS 121 Structure Two 25 Site SSG

DS 982 Structure Two 25 IGU seal

▪ 2-part Structural Glazing Silicone

DOW CONFIDENTIAL - Do not share without permission 19

DOW CONFIDENTIAL - Do not share without permission 20

PMS = Quality Check and Systematic Approach for Quality Seal

DOW CONFIDENTIAL - Do not share without permission 21

DOW CONFIDENTIAL - Do not share without permission 22

Bad Design Bad Sealant

DOW CONFIDENTIAL - Do not share without permission 24

• Adhesion Test With

DOW CONFIDENTIAL - Do not share without permission 25

Snap Time Test การทดสอบการแห้งตัวของ ซิลิโคน

Snake Test การยิงทดสอบเป็ นรูปงู

Mix Ratio Test การทดสอบการผสม

Deglazing Tests การแกะแผงเพื่อตรวจสอบ :ซิลิโคน ที่ช้ในแผง

DOW CONFIDENTIAL - Do not share without

DOW CONFIDENTIAL - Do not share without

DOW CONFIDENTIAL - Do not share without permission 28

Reported by CTBUH _ Council of Tall Building and Urban Habitat

✓ 70% uses DOW sealant

DOW CONFIDENTIAL - Do not share without permission 29

DOW CONFIDENTIAL - Do not share without permission 30

DOW CONFIDENTIAL - Do not share without permission 32

MAGNIFIED X-SECTION OF EXTRUSION FACE

DIRT & OIL WAX LAYER

Dow Restricted DOW RESTRICTED 34

DOW CONFIDENTIAL - Do not share without permission 38

การใช้รองพืน้ ทีถ่ กู ต้อง

DOW CONFIDENTIAL - Do not share without

DOW CONFIDENTIAL - Do not share without permission 39

การใช้รองพืน้ ทีไ่ ม่ถกู ต้อง

DOW CONFIDENTIAL - Do not share without permission 40

การใช้รองพืน้ ทีไ่ ม่ถกู ต้อง

DOW CONFIDENTIAL - Do not share without permission 41

DOW CONFIDENTIAL - Do not share without permission 42

DOW CONFIDENTIAL - Do not share without permission 44

DOW CONFIDENTIAL - Do not share without permission 45

DOW CONFIDENTIAL - Do not share without

DOW CONFIDENTIAL - Do not share without permission 47

Material Storage Temp ◦C Shelf Life (months)

Panelfix 896 below 30 12

Primer 1200 OS* below 32 12

DOW CONFIDENTIAL - Do not share without permission 48

DOW CONFIDENTIAL - Do not share without

DOW CONFIDENTIAL - Do not share without permission 50

DOW CONFIDENTIAL - Do not share without permission 51