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Adding 25ml of hot water The blue pop ice solution was Shake the solution for 15
to the purple pop ice transferred to a separating minutes and let it stand
powder funnel and 10 mL of butanol until the solvent layer
and 1 mL of 10% phosphoric separates
acid were added.
The purple pop ice solution Organic solvent collected
Shake the solution for 15
was transferred to a and evaporated to dryness
minutes and let it stand
separating funnel and 10 mL
until the solvent layer
of butanol and 1 mL of 10%
separates
phosphoric acid were added.
Organic solvent collected The residue is dripped with Residue drip 7 ml 4 drops
and evaporated to dryness 7 mL of Ammonium of Ammonium Hydroxide
Hydroxide (NH4OH) (NH4OH)