CHEM LAB

Friday, 17 February 2023 6:16 pm

Distillation- Process sa purification or separation of components sa liquid mixture. SUBLIMATION

TYPES OF DISTILLATION • However, some substances exhibit appreciable vapor pressure below their
melting points. These substances change directly from the solid phase to
Simple distillation, Steam distillation, Fractional distillation the gas phase without forming an intermediate liquid phase by a process
called sublimation or volatilization.
Boiling point of the liquid • Ang solid into gaseous phase through sublimator
The temperature at which the vapor pressure equals the atmospheric pressure is referred to
as
Simple distillation
Ginagamit ni siya nga process for removing tung mga non volatile impurities or mga
immisicble liquids by at least gap nila 25 degrees celcius
•
Round- glass joint flask
Distillation adapter
Thermometer
Water-jacketed condenser
Collector flask • USING PETRI DISH
Clips • Prepare a clean and dry petri dish and separately weigh the base and the lid.
Clamps • Weigh about 1 gram of dry crude naphthalene and place on the base of the dish
Clamp holders and cover with the lid.
• Place a wire gauze atop a hotplate and place the covered dish with the crude
Procedures sample.
• First, the clamp and clamp holder are fixed to a support stand (or lab frame) at the lab • Place a beaker full of ice top sa lid
desk or fume hood. • Next, weigh the lid containing the sublimates and determine the mass of the
• the round-bottom flask is placed on the hot plate, sublimate and the rate of recovery.
• while the thermometer is placed such that its bulb is below the lower level of the lateral Separation of Iodine and Mixture
line of the distillation connector so that it is in the vapor stream of the distillation. • Next, weigh the lid containing the sublimates and determine the mass of the
• The condenser should then be inclined to allow the condensed vapor to drop into the sublimate and the rate of recovery.
receiving flask.
the rubber
• tubing is connected to a water-jacketed condenser to provide the water (inlet from
water supply, lower end, and outlet to sink, upper end). The receiving container should
be placed in an ice-water bath.
REMEMBER

• Place boiling chips first tas 50 ml rum

• Density

-Relative error
Ss

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