SYNTHESIS OF MANGANESE (VI)

AND MANGANESE (III)

COMPOUNDS

BY :
YEYEN HASIM
(441418046)
 OBJECTIVES

Synthesizing manganese (VI) and

manganese (III) compounds
 PROCEDURE
Manganese (VI) Compound

Test tube 1
• Mix 10 mL 0.01M KMnO4with 5 mL 1 M H2SO4
• Add a little MnO2 then shake it
• Filter the solution
Test tube 2
• Mix 10 mL 0.01M KMnO4with 5 mL 2 M NaOH

• Add a little MnO2 then shake it

• Filter the solution
Manganese (III) Compounds
• Weigh 0.5 grams of MnSO4 then react with 2 mL
of
1 M H2SO4
• Add 10 drops of concentrated H2SO4
• Cool with cold water
• Add 5 drops of 0.1 M KMnO4
• Mix in 50 mL of distilled water
• Observe the changes that occur!
 DISCUSSION

the first experiment was conducted to make manganese (Vl). the

first step is to prepare 2 empty test tubes labeled 1 and 2. then put 4
ml of 0.01 M KMnO4 into two test tubes that have been labeled 1
and 2. after that add 2 ml of dilute H2SO4 solution into test tube 1
and 2 ml of dilute KOH into a test tube 2. the results obtained in
test tubes 1 and 2 of the solution both turned purple.
 Then a small amount of MnO2 was added to each test tube. in
test tubes 1 and 2 the solution remained purple. after filtering in the
test tube 1 the solution changes color to light purple while in the
test tube 2 the solution changes color to blackish green.
 in the manufacture of manganese (III) the first step is to weigh
0.5 g of MnSO4 then put it into a test tube and react with 2 ml of 1
M H2SO4 and the solution becomes clear.

After that, 10 drops of concentrated H2SO4 were added which

resulted in a cloudy solution and there were still insoluble MnSO4
granules.
 then the solution is cooled with cold water and added 5 drops of
0.1 M KMnSO4 and 50 ml of distilled water, the solution turns
brown.
 CONCLUSION

After carrying out the above practicum, it can be concluded that the
manufacture of manganese (VI) can occur using a base, which is marked by
a change in the color of the solution from purple to green. Compounds in
manganese (VI) containing permanganate ions are only stable in alkaline
conditions, this shows a positive reaction from manganese (VI). Meanwhile,
in the manufacture of manganese (III) it can be seen from the color changes
that occurred which were initially clear to dark brown which was a positive
reaction from the manufacture of manganese (III).
THANK YOU