VN PHNG CNG NHN CHT LNG

Bureau of Accreditation (BoA)

YU CU B SUNG
CNG NHN CC PHNG TH NGHIM
LNH VC HA

Supplementary requirement for accreditation
in the field of chemical testing

M s/Code: AGL 03
Ln ban hnh/Issue number: 04.12
Ngy ban hnh/ Issue date: 06/2012



Yu cu b sung cng nhn cc phng th nghim lnh vc Ha
Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 1/34
Ni dung

Trang
Phn 1 Gii thiu 3
Mc ch 3
Phm vi 3
Chun mc cng nhn 3
Cu trc 3
Phn 2 Yu cu b sung cng nhn cc phng th nghim lnh vc
Ha
4
4.1 T chc 4
4.2 H thng qun l 4
4.5 Hp ng ph th nghim 5
4.12 Hnh ng phng nga 5
4.13 Kim sot h s 6
5.2 Nhn s 6
5.3 Tin nghi v iu kin mi trng 7
5.4 Phng php th v xc nhn gi tr s dng ca phng php 8
5.5 Kim sot thit b, ha cht 10
5.6 Lin kt chun o lng 11
5.7 Ly mu 12
5.8 Qun l mu 13
5.9 m bo cht lng kt qu th nghim 14
5.10 Bo co kt qu 15
Phn 3 Chu k hiu chun, kim tra thit b thng thng 17
Ph lc Hng dn hiu chun mt s thit b 28

Yu cu b sung cng nhn cc phng th nghim lnh vc Ha
Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 2/34
Supplementary requirement for accreditation
in the field of chemical testing

Content

Page
Section 1 Introduction 3
Purpose 3
Scope 3
Accreditation criteria 3
Structure 3
Section 2 Supplementary requirement for accreditation in the field of
chemical testing
4
4.1 Organization 4
4.2 Management system 4
4.5 Subcontracting of test 5
4.12 Preventive action 5
4.13 Control of record 6
5.2 Personnel 6
5.3 Accommodation and environmental conditions 7
5.4 Test methods and method validation 8
5.5 Equipment, Chemical 10
5.6 Measurement traceability 11
5.7 Sampling 12
5.8 Handling of test items 13
5.9 Assuring the quality of test and calibration results 14
5.10 Reporting the results 15
Section 3 Calibration, checking interval for commonly used chemical
testing equipment
17
Annex Guide to calibration equipment 28

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AGL 03 Ln ban hnh: 4.12 Trang: 3/34

PHN 1 GII THIU

MC CH
Tiu chun quc t ISO/IEC 17025 "Yu cu
chung v nng lc ca phng th nghim v hiu
chun" cp cc yu cu h thng qun l v cc
yu cu k thut cho cc phng th nghim p
dng. Cc yu cu trong tiu chun trn c xy
dng p dng cho tt c cc lnh vc th
nghim v hiu chun do vy Vn phng cng
nhn cht lng xy dng thm cc ti liu b
sung din gii cho tng lnh vc hiu chun
hoc th nghim c th cng nh cho cc k thut
th nghim, hiu chun.

PHM VI P DNG
Ti liu ny cp cc yu cu chi tit v c th
p dng cho cng nhn i vi cc phng th
nghim (PTN) thuc lnh vc ho.
Cc yu cu cng nhn cho cc PTN ho khng
ph thuc vo qui m ca PTN, s lng cc php
th nghim m PTN thc hin hoc s lng nhn
vin.

CHUN MC CNG NHN
Chun mc cng nhn phng th nghim lnh
vc ha bao gm:
- ISO/IEC 17025 : 2005 - "Yu cu chung
v nng lc ca cc phng th nghim v
hiu chun".
- Yu cu b sung cng nhn cho phng
th nghim lnh vc ho.

- Cc chnh sch ca BoA lin quan cng
nhn phng th nghim
- Cc vn bn php qui lin quan n hot
ng th nghim trong lnh vc ha.

Th tc cng nhn phng th nghim theo ti liu
APL 01
Ngoi ra cn c cc ti liu k thut h tr cc
PTN lin quan ti cc lnh vc k thut c th.
Mt s ti liu k thut c vin dn trong ti
liu ny. Cc ti liu k thut nhm a ra cc
hng dn do khng phi l cc yu cu
SECTION 1 INTRODUCTION

PURPOSE
International Standard ISO/IEC 17025 General
requirements for the competence of testing and
calibration laboratories included requirements of
management system and technical for laboratories.
These requirements are designed to apply to all
types of testing and calibration and therefore BoA
often need to be developed supplementary
requirements to interpreted with respect to the
type of calibration or testing concerned, and the
techniques involved


SCOPE
This document provides detailed and specified
requirements to accreditation for Chemical testing
laboratories.
Requirement for Chemical testing laboratory is
applicable to all of Chemical testing laboratories
regardless of the organization size, the number of
personnel or extent of the scope of testing

ACCREDITATION CRITERIA
Accreditation criteria for chemical testing
including:
- ISO/IEC 17025 : 2005 - General
requirements for the competence of
testing and calibration laboratories
- Supplementary requirements for
accreditation in the field of Chemical
testing
- BoA policies concerning accreditation for
laboratories
- Regulation concerning accreditation for
chemical testing

Accreditation assessment procedure for
laboratories is APL 01
Besides there are some technical documents to
assist laboratory concerning specified technical.
Technical documents have been reference in this
document. Technical documents assist for
laboratory so that it is not requirement for
Yu cu b sung cng nhn cc phng th nghim lnh vc Ha
Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 4/34
cng nhn tr khi chng c nu c th trong ti
liu ny.

CU TRC
Ti liu ny c 3 phn chnh:
Phn 1: Gii thiu
Phn 2: Cc yu cu b sung cng nhn cho
phng th nghim thuc lnh vc ha
Phn 3: Chu k hiu chun thit b

Ph lc 1: Hng dn hiu chun mt s thit b
Cc yu cu trong phn 2 ca ti liu ny c
trnh by theo th t ca cc yu cu trong tiu
chun ISO/IEC 17025, c th c mt s yu cu
trong tiu chun ISO/IEC 17025 s khng c yu
cu b sung.
Cc ni dung c k hiu iu mc trong du
ngoc ( ) l yu cu bt buc cn cc ni dung
c in ch nghing l cc hng dn, gii thch
thm lm r ngha ca cc yu cu.

accreditation unless mention in this document.


STRUCTURE
This document have 3 main section
Section 1: Introduction
Section 2: Supplementary requirements for
accreditation in the field of chemical testing
Section 3: Calibration interval for testing
equipment
Annex 1: Guide to calibration equipment
The requirements in section 2 have been presented
base on section of requirement in the standard
ISO/IEC 17025, there are some requirements in
ISO/IEC 17025 does not have supplementary
requirement.
All content mention in mark ( ) are mandatory
requirements and all content mention in italic are
guidelines, interpretation for more clear of the
requirement.
PHN 2 YU CU B SUNG CNG
NHN PTN LNH VC HA


4. CC YU CU QUN L

4.1. T chc
(1) Nhn vin PTN c trch nhim lin quan n
hot ng sn xut hoc bn hng, qung
co th phi c chnh sch r rng xc
nh cch thc m bo tnh khch quan ca
h i vi trch nhim th nghim.
(2) Trng hp PTN c thc hin th nghim
ti hin trng, ti PTN di ng phi c cc
th tc m bo qun l cho hot ng th
nghim .

4.2. H thng qun l
(1) Trong ti liu h thng qun l phi vin dn
ti ngi c thm quyn k c ph duyt,
phm vi cng nhn v chnh sch s dng
biu tng cng nhn ca BoA.


SECTION 2 SUPPLEMENTARY
REQUIREMENTS FOR ACCREDITATION
IN THE FIELD OF CHEMICAL TESTING

4. MANAGEMENT REQUIREMENTS

4.1. Organization
(1) For laboratory staff who may also have
production or marketing related
responsibilities, clear policies shall be
available to define how impartiality is
assured for their testing responsibilities
(2) For laboratory conduct tests at sites away
from its permanent facilities, or in mobile
facilities shall have procedures to manage
for those tests.

4.2. Management system
(1) Management system document shall
reference to signatory authorities, accredited
scope and policy for using BoA logo.



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AGL 03 Ln ban hnh: 4.12 Trang: 5/34
4.5. Hp ng ph v th nghim

(1) PTN phi tun th yu cu 5.10.6 ca tiu
chun ISO/IEC 17025:2005 v cc yu cu
bo co kt qu th nghim ca nh thu
ph.

(2) Trng hp PTN s dng nh thu ph cho
cc php th ng k cng nhn th phi s
dng nh thu ph c nng lc. Nh thu
ph c nng lc phi l mt PTN c BoA
cng nhn hoc mt phng th nghim c
cng nhn bi mt t chc cng nhn tham
gia tho c tha nhn ln nhau vi BoA.
Tt c cc kt qu do nh thu ph thc hin
phi c nu trong bo co th nghim ca
PTN.

(3) Trng hp PTN s dng nh thu ph
thc hin mt phn php th nh s dng
thit b th nghim th PTN cn nh gi v
m bo thit b p ng yu cu ca
phng php th v qui nh v kim sot
thit b ca PTN.

(4) PTN phi nh k xem xt tnh trng
cng nhn ca nh thu ph.

Cc thng tin v tnh trng v phm vi cng
nhn c th tm trn website
www.boa.gov.vn hoc lin h vi t chc
cng nhn. PTN c th s dng nh thu
ph cha c cng nhn cho cc ch tiu
th nghim m PTN khng ng k cng
nhn.

4.12. Hnh ng phng nga
Hnh ng phng nga l mt qu trnh ch
ng xc nh c hi ci tin ch khng
phi thc hin sa cha, khc phc nhng
vn pht sinh hoc phn nn.

4.5 Subcontracting of tests and calibrations

(1) Laboratory shall conformity with clause
5.10.6 of ISO/IEC 17025:2005 the results of
the subcontracted service are incorporated
into the laboratorys test reports.

(2) Where laboratory use subcontractor for
accredited tests shall use a competent
subcontractor. Competent subcontractors are
accredited laboratories by BoA or by one of
BoAs mutual recognition partners. All of
test results by accredited subcontractor shall
be covered by an appropriate endorsed
report.



(3) Where laboratory use subcontractor for
partial of test such as use equipment of
laboratory shall evaluate and have evidence
that equipment fitness requirement for test
method and control equipment.


(4) The accreditation status of subcontractors
shall be regularly reviewed to ensure
currency.

Information on the accreditation status and
scope of accreditation may be found at
BoAs website www.boa.gov.vn or by
contacting accredited laboratory.
Laboratory may use unaccredited
laboratory for tests that outside scope of the
accredited laboratory.

4.12. Preventive action
Preventive action is a proactive process to
identify improvement opportunities, rather
than a reaction to the identification of
problems or complaints.

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AGL 03 Ln ban hnh: 4.12 Trang: 6/34
(1) Cc cng c qun l cht lng ton din
nh: phng cch tho lun theo nhm
(brainstorming), s nguyn nhn v kt
qu, biu kim sot, biu pareto ... cn
c s dng h tr thc hin phng
nga.
Phng th nghim cng nn c cch thc
khuyn khch v tip nhn cc ng gp
kin ci tin ca nhn vin

4.13. Kim sot h s

(1) Thi gian lu gi h s khng c di 3
nm tr khi c giao c hp ng hoc quy
nh php l.

(2) H s k thut (h s th nghim) cn bao
gm cc thng tin sau:
- nhn dng mu;
- xc nhn phng php th nghim;
- thi gian th nghim (thi gian bt u,
thi gian kt thc);
- chun, thit b th nghim;
- d liu quan trc gc, tnh ton kt qu
bao gm c du hiu, d liu c th
nhn bit, truy xut ti iu kin thc
hin th nghim;
- nhn vin thc hin th nghim;
- bng chng v kim tra, xc nhn vic
tnh ton v truyn d liu.
- cc thng tin c th qui nh trong
phng php th, cc vn bn hp ng
hoc cc qui nh do php lut yu cu.


5. CC YU CU K THUT

5.2. Nhn s

(1) Cn b kim sot k thut ca PTN phi c
t nht 2 nm kinh nghim lin tc trong lnh
vc th nghim c phn cng kim sot.

(2) Nhn vin mi cn c o to thc hnh
(1) Total quality management tools such as
brainstorming, flowcharting, Fishbone
diagram, Pareto chart etc shall be use to
assist for preventive actions.


Laboratory should be given to providing
staff with a formal mechanism for
contributing suggestions for improvement.

Control of records

(1) Unless otherwise prescribed by legislation or
contractual obligation, retention times will
not be less than three years.

(2) Technical records (test records) shall include
the following:
- The sample identification;
- The test document identification;
- Date of test (time start and finish);
- The identity of reference standard and
equipment use for the test;
- Original test observations and
calculations included data, sign that could
traceability to test condition;
- The identify of the person performing the
test;
- An indication that calculations and
manual data transfers have been checked;
- Any other information specified in the
test method, other contractual documents
or relevant statutory regulations.


5. TECHNICAL REQUIREMENTS

5.2. Personnel

(1) Technical manager who control technical
any scope of tests shall have at least 2 years
uninterrupted experiences on that scope.

(2) New staff shall be training to conduct tests
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AGL 03 Ln ban hnh: 4.12 Trang: 7/34
th nghim t nht 3 thng v cn c h s
th hin c kim tra vic thc hin th
nghim t c chnh xc theo yu cu
ca cc php th c th trc khi giao nhim
v th nghim chnh thc. Cc cn b mi
c giao nhim v th nghim c th cn
c cn b gim st t nht l 1 nm.

Kim tra vic thc hin th nghim c th p
dng hnh thc th nghim lp li, ti lp,
tham gia so snh lin phng, th nghim
trn mu chun, mu thm chun


Th lc ca nhn vin v nhn bit mu km
c th gp kh khn trong khi thc hin mt
vi php th. Nhn bit mu l mt trong
nhng yu cu m qun l PTN nn cn
nhc khi xc nh nhn vin thch hp
thc hin php th.

(3) Bt k th nghim no khng thc hin
PTN chnh (nh th nghim hin trng,
phng th nghim di ng, phng th
nghim tm thi) cng phi c kim sot
k thut y . PTN phi c ngi c thm
quyn k kt qu th nghim mi a im
th nghim.

(4) Nhn vin phi c thng bo, hng dn
cc thng tin lin quan v cc vn v
sinh an ton phng th nghim.

5.3. Tin nghi v iu kin mi trng

(1) PTN cn kim sot mi trng th nghim
m bo khng xy ra nhim bn mu.

(2) Khu vc t thit b, ha cht cn m bo
khng b nh hng ln nhau v m bo an
ton cho phng th nghim.

(3) Khi th nghim ti hin trng, v tr th
at least 3 months and shall have records that
new staff have been conduct the tests and
get accuracy base on requirement of test
methods before assign to become official
analyzer. New staff shall be supervising at
least 1 year.


Laboratory may use method such as
repeatabitability and reproducebility,
participate Proficiency testing/ inter
laboratory comparison, use certified
reference material (CRM) or spike sample
etc.
Eyesight of analyzer to determine color may
be getting difficult when conducts some tests.
Determine color is one of the requirement
that laboratory manager should consider
when define suitable analyzer to do.

(3) Any testing conducted away from the base
laboratory (such as in field
laboratories/permanent facilities, in a
mobile or temporally laboratories) shall also
be under adequate technical control. This
would normally require either the location of
an approved signatory at each facility

(4) Staff shall be announce, guide all of
information concerning laboratory hygiene
and safety.

5.3. Accommodation and environmental
conditions
(1) Laboratory shall control environmental
conditions to prevent sample contamination.

(2) Equipment area and chemical area shall be
ensure that not effect together and ensure to
safe for laboratory.

(3) When testing in the field, testing sites must
be chosen to minimize the effects of
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AGL 03 Ln ban hnh: 4.12 Trang: 8/34
nghim phi c la chn hn ch ti a
nh hng ca cc iu kin mi trng v
s nhim bn mu.

(4) Tt c cc iu kin mi trng nh hng
kt qu th nghim phi c theo di v
lu h s.

5.4 . Phng php th nghim v xc nhn gi
tr s dng phng php

(1) Phng th nghim phi c v p dng cc th
tc bng vn bn v vic la chn v xc
nhn gi tr s dng ca phng php. Th
tc bao gm chi tit cc bc tin hnh xc
nhn gi tr s dng, cc phng php thng
k c p dng tnh cc thng s nghin
cu. H s xc nhn gi tr s dng ca
phng php phi c lu gi v BoA s
yu cu c xem xt trc hoc trong cc
cuc nh gi.

(2) PTN p dng cc phng php th theo tiu
chun quc gia, quc t, hip hi khoa hc
c chp nhn rng ri trn th gii nh
TCVN, ASTM, APHA, AOACcn c h
s nh gi iu kin c bn - cc ngun lc
theo yu cu ca phng php th v vic
t c kt qu th nghim c chnh xc
nh phng php yu cu hoc nh mong
mun ca PTN. i vi cc phng php
th ban hnh m khng c d liu v
chnh xc th PTN phi xc nh d liu
chnh xc ca php th da trn d liu
nghin cu th nghim. Ton b cc phng
php phi c chun mc loi b nhng
kt qu nghi ng.

(3) Cc phng php th khng tiu chun nh
Phng php do PTN xy dng (phng
php th ni b), phng php theo hng
dn ca nh sn xut thit b cn c lp
thnh vn bn. Phng php th ni b cn
environmental conditions and sample
contamination.

(4) All relevant environmental conditions that
effect to test results shall be control and
recorded.

5.4. Test methods and method validation


(1) Laboratory shall have fully documented
procedures for choose and validation
method. That procedure shall be covering
detail of validation method step, statistical
method use to define examine factors.
Validation method records shall be kept and
BoA will be check before or onsite
assessment.



(2) As well as methods published by Vietnam
standard institute, international standard,
prestige technical association such as
TCVN, ASTM, APHA, AOAC ex.
laboratory shall have record to verified that
laboratory have enough capability to conduct
the test and evidence to get all of accuracy
factors that test method required or
laboratory required. Methods published do
not include accuracy data the laboratory
shall determine its own accurate factors
depend on verified data. All methods shall
include criteria for rejecting suspect results.



(3) Nonstandard method such as laboratory
developed methods, equipment producer
methodsshall be documented. Laboratory
developed methods shall be mention clear
materials/products have been test,
performance parameters, criteria for
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xc nh r i tng th, ch tiu th, gii
hn chp nhn ca kt qu, c lng
khng m bo.

(4) PTN phi thc hin nghin cu v xc nhn
gi tr s dng i vi phng php khng
tiu chun hoc cc phng php c sa i,
m rng phm vi so vi phng php tiu
chun. PTN phi lu h s lin quan n qu
trnh nghin cu, xc nhn gi tr s dng
bao gm nh gi iu kin c bn - cc
ngun lc thc hin phng php th v
chnh xc ca phng php.

(5) PTN c th xc nhn gi tr s dng ca
phng php bng cch s dng mu chun
hay cht chun c chng nhn hoc so
snh vi phng php tiu chun. Ty thuc
mc v mc ch s dng phng php
m PTN c th cn nhc la chn xc
nhn gi tr s dng ca phng php theo
cc thng s c cp di y:
- Tnh chn lc/tnh c hiu;
- Tnh tuyn tnh;
- nhy;
- chnh xc ( ng v chm);
- Gii hn pht hin v gii hn nh
lng;
- Khong nng ;
- Cc yu t nh hng;
- khng m bo o;
- Tnh lin kt chun.

(6) BoA c th cng nhn cc phng php th
nhanh, phng php th theo b Kit ca nh
cung cp khi PTN c h s v xc nhn
tnh ng n phng php cho cc i
tng th. PTN phi c kh nng khng nh
phng php trong trng hp c tranh ci.

(7) PTN ng k cng nhn vi phm vi cng
nhn khng hn hp (cc nhm cht cn
phn tch, v d thuc tr su hp cht clo)
rejecting suspect results, uncertainty of
measurement.

(4) Laboratory shall validate method for all
nonstandard method or modify method,
extend scope of standard method. Laboratory
shall be studies recorded validate method
including evaluate laboratory capabilities to
perform method and studies accuracy
factors.



(5) Method may be validated by using certified
reference materials or comparison with other
established methods. Depend on
requirement and purpose of using method,
laboratory could consider for choosing
validate factors. The following parameters
require consideration:

- Selectivity;
- Linearity of response;
- Sensitivity;
- Accuracy (trueness and precision);
- Limit of detection and limit of
quantitation;
- Range;
- Robustness/ruggedness;
- Measurement uncertainty;
- Traceability.

(6) BoA accredits for quick tests, producers KIT
tests, Laboratory shall recorded all of
validate data for all materials/products and
laboratory shall have capability to confirm
method if get dispute.


(7) A laboratory seeking accreditation for a
more open scope of accreditation (where
groups of analyses, for example, organ
chlorine pesticides) shall have fully
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phi c y cc th tc c vn bn
ha gm cc qui nh nh: vic la chn
phng php, xy dng phng php, xc
nhn gi tr s dng ca phng php, c
cc chun chnh ph hp v c bng chng
v hot ng o to nhn vin. H s cc
th tc ny c xem xt nh mt phn ca
mi cuc nh gi.


(8) PTN ng k cng nhn php th phm vi
m nh thc phm cn thc hin xc nhn
gi tr s dng trn t nht 5 nn mu i
din cho bn cht ca mu thc phm (giu
protein, bo, hydratcacbon, nc).

Phng th nghim c th tham kho ISO 78-
2 Hng dn trnh by phng php
phn tch ha hc i vi cch trnh by
cc phng php th

5.5. Kim sot thit b, ha cht

Thit b

(1) PTN thc hin hiu chun kim tra v bo
tr thit b ni b cn c:
- Phng php hiu chun, bo tr, kim
tra c lp thnh vn bn;
- Ton b d liu th hin vic thc hin
cc hot ng hiu chun, kim tra, bo
tr v ngi thc hin phi c lu h
s;

(2) i vi PTN thc hin hiu chun ni b,
khi cn thit BoA c th thc hin nh gi
o lng v nh gi k thut m bo
rng PTN tun th cc yu cu tng ng
ca ISO/IEC 17025 cho phng hiu chun.

Ha cht

(3) PTN phi c th tc kim sot vic tip
nhn, kim tra, s dng, bo qun v thanh
l cc ha cht, thuc th.
documented procedure, covering such
elements as: method selection, method
development, and method validation,
acquisition of appropriate reference
standards or reference materials and staff
training. Records of the application of these
procedures will be reviewed as part of each
assessment.

(8) Laboratory want to conduct parameter with
extend scope such as food shall validate
method at least in 5 matrix representative for
nature of food (high protein, oil, hydrate
carbon, water).

ISO 78-2 Chemistry layouts for
standards Part 2: Method of chemical
analysis also provides useful guidance.


5.5. Equipment, chemical

Equipment

(1) Laboratory conduct calibration, check and
maintenance by its shelf shall:
- Documented procedure for calibration,
check and maintenance;
- Keep record of full results (including raw
data) for each calibration, check and
maintenance;


(2) BoA may conduct measurement audit and
technical assessment for Laboratory that
carry out in-house calibration to ensure the
laboratory comply with requirement in
ISO/IEC 17025 for calibration.

Chemical

(3) Laboratory shall documented procedure for
control chemical including: receive, check,
use, keep in good condition and liquidate.

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AGL 03 Ln ban hnh: 4.12 Trang: 11/34

(4) Nhn gc trn bao b ha cht, thuc th
phi c th hin bng ngn ng m nhn
vin c th c v hiu c v phi c
thng tin v tiu chun k thut ca ha
cht, thuc th nh:
- Tn ha cht
- Cc thnh phn v nng
- Hn s dng
- Cnh bo (nu c)

(5) Cc ha cht, thuc th hoc dung dch
chun PTN pha ch cn c h s th hin
vic thc hin pha ha cht, thuc th hoc
dung dch chun. Trn mi chai ha cht,
thuc th hoc dung dch chun pha ch cn
c nhn vi ni dung sau:
- Tn ha cht
- Nng
- Ngy pha
- Ngi pha
- Hn s dng
- Cnh bo (nu cn thit)

5.6. Lin kt chun o lng

(1) Cc thit b th nghim v hiu chun c
nh hng ng k n kt qu th nghim
(k c cc thit b s dng kim sot iu
kin mi trng c tc ng quan trng, nu
cn) phi c hiu chun bi cc t chc
hiu chun theo qui nh Chnh sch v lin
kt chun APL 02 ca BoA.

(2) Thit b c hiu chun bng cch s dng
cc cht chun, cht chun c chng
nhn hoc cc cht chun pha ch thng
qua vic so snh vi nhng cht chun gc
th phi m bo:

- Cc cht chun kh nng hiu
chun nhng hng mc lin quan ca
thit b trn nhng phm vi o m thit b
(4) Original label of chemical shall be expressed
in language that staff could be read and
understand and enough specific information
of chemical such as:


- Name of chemical;
- Component and concentration;
- Expiry date;
- Warning (if any) ...

(5) Laboratory preparing chemical, solution or
stock solution shall keep records of
preparing chemical, solution or stock
solution process. In chemical, solution or
stock solution bottles shall have label
included information as:
- Name;
- Concentration;
- Date prepare;
- Name of person prepare;
- Expiry date;
- Warning (if any).

5.6. Measurement traceability

(1) Test equipment that has a significant effect
on the reported result (including, where
relevant, instruments used for monitoring
critical environmental conditions) shall be c
calibrated by organization base on
requirement of BoA mention in
Traceability measurement APL 02.

(2) When the laboratory undertakes calibration
of equipment using certified reference
material of reference materials developed
through comparison with certified reference
materials it shall be able to demonstrate that
it has:
- Sufficient reference materials to calibrate
the relevant items of equipment over the
desired measurement ranges;
- Full records of the identity and source of
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Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 12/34
c yu cu;
- C h s nhn dng v ngun gc mi
cht chun;
- C y cc vn bn v nhng gi tr
qui chiu c xc nh (v khng
m bo o lin quan) ca mi cht
chun bao gm cc chi tit v tnh hiu
lc;
- C thc hin phng nga cn thit bit
c s khc nhau gia dng mu ca
cht chun vi dng mu th nghim
thc t ti phng th nghim, hoc xc
nh v tnh ton nhng nh hng ca
cc dng mu th.

(3) Cht chun phi c cc thng tin sau:
- c tnh ( khng m bo o, nu l
cht chun chng nhn);
- K thut xc nh cc c tnh;
- Thi hn chng nhn c hiu lc (nu
thch hp);
- Thi hn s dng ca cht chun;
- Cc iu kin lu gi;
- Ngy m cht chun s dng ln u.


ISO Guide 31 c cc qui nh chi tit v ni
dung chng ch cc cht chun.

5.7. Ly mu
Tiu chun ISO/IEC 17025 p dng cho
PTN bao gm c hot ng ly mu. Hot
ng ly mu ca cc PTN rt khc nhau.
Hot ng ny c th c cc b phn
khc trong cng t chc vi PTN thc hin
hoc mt t chc hon ton c lp thc
hin. BoA khuyn khch PTN ng k cng
nhn c hot ng ly mu.

Trng hp PTN khng thc hin ly mu
c th hng dn cho n v, ngi ly mu
v cch thc ly mu v bo qun mu
m bo tnh hiu qu ca hot ng th
nghim

each reference material;
- Full document of the assigned property
values (and associated measurement
uncertainty) of each reference material
including details of the mode of
validation;
- Taken any necessary precautions to
match the matrices of the reference
materials to those encountered in the
laboratorys test samples, or determined
and accounted for the effects of any non-
matching of matrices.


(3) Reference materials shall be obtained at
least the following information:
- Property values (and associated
uncertainties, if a certified reference
material);
- Technique(s) by which the property
values were established;
- Date of certification;
- Period for which certification if valid;
- Storage conditions.
- Open dated
ISO Guide 31 contains more detail on the content
of certificates for reference materials.

5.6. Sampling
Scope of International standard ISO/IEC
17025 includes sampling activities.
Sampling activities of laboratories are
difference. Sampling activities may demand
a different part of the laboratory
organization or an independent
organization. BoA encourages laboratory to
seek accreditation for sampling activities.

Laboratory may introduce or training for
organization or sampling officer to sampling
and keep in good condition for sample for
ensuring the effectiveness of sampling
activities.

(1) When the laboratory has no control over
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AGL 03 Ln ban hnh: 4.12 Trang: 13/34
(1) Nu PTN khng thc hin ly mu th bo
co kt qu th nghim cn ghi r kt qu
ch ng vi mu th. H s tip nhn mu
cn ghi r cc thng tin lin quan n mu
th nh: loi mu, ngy tip nhn, tnh trng
mu, lng mu, iu kin bo qun (nu
c).

(2) Nu hot ng ly mu do b phn khc
thc hin nhng bo co kt qu th nghim
c tuyn b p dng cho c sn phm, l
hng th PTN phi b tr BoA tin hnh
nh gi hot ng ng ly mu bao gm:

- Th tc ly mu c lp thnh vn bn
(c th l cc tiu chun quc gia hoc
quc t). Nu s dng cc phng php
ni b th cn xc nhn gi tr s dng
ca phng php m bo vic ly
mu p ng c mc ch ra.

- Bo co kt qu th nghim phi vin
dn n phng php ly mu

5.8. Qun l mu th nghim

(1) Cc dng c cha mu phi ph hp yu cu
ca phng php ly mu hoc phng php
th v phi kim tra v m bo khng nh
hng n cht lng mu th (khng b r
r, khng thm nc, bin cht hoc nhim
bntrong qu trnh vn chuyn v lu
gi). Nu phng php ly mu v/hoc
phng php th yu cu iu kin bo qun
mu cn c m bo th phi ghi r iu
kin bo qun vo h s ly mu.

(2) Vic nhn dng cc nhn mc phi m bo
r rng, khng h hng, c nhn din
trong sut qu trnh th nghim v d c.
Khng chp nhn vic dn nhn mc ch trn
np.

sampling the test results report shall mention
results only for received sample. The sample
receiving record shall mention detail
following information concerning sample:
sample type, date of receipt, condition of
receipt, sample volume, maintaining
condition (if any).

(2) Where sampling activities conducted by
other part of laboratory but test report has been
stated that the test results for product lot/batch, the
assessment of sampling activities shall be included
as an element of the laboratory assessment as:

- The laboratory shall have documented
sampling procedures (may be national or
international standards). If in house
methods are used, their validity for the
intended purpose shall be demonstrated
by appropriate data.

- The sampling procedure shall be cited on
the test report.

5.8 Handling of test items

(1) Sample container shall be comply with
requirement of sampling procedures or test
procedures and may be necessary to test
container to ensure not effect to sample
(leak-proof, hydrophilic, contamination ex.
During transport and storage). Any
temperature or other environmental
tolerances specified in the method shall be
cited in sampling record.


(2) Identification labels shall be secure, legible
and identify during conducting test.
Labeling on caps or lids alone is not
acceptable.


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AGL 03 Ln ban hnh: 4.12 Trang: 14/34
(3) Nhn vin phng th nghim phi kim tra
trng thi ca mu khi tip nhn. Nu trng
thi khng m bo hoc nu mu khng
nhng khch hng vn yu cu th nghim
m PTN ng cn ghi r tnh trng mu
vo h s tip nhn v c xc nhn ca
khch hng.

(4) Ngoi tr cc trng hp c bit PTN phi
lu gi cc mu th nghim cho n khi c
c tt c cc kt qu, hoc lu gi lu hn
nu cn thit. Mu lu phi c bao gi
trong vt ng thch hp v lu gi iu
kin bo qun ca mu th.

5.9. m bo cht lng kt qu th nghim

(1) PTN phi c th tc kim sot cht lng
cc php th nghim khng thc hin
thng xuyn v nu r cch thc m bo
kt qu th nghim nu mun c cng
nhn hoc duy tr cng nhn nhng phi m
bo tn sut thc hin kim sot t nht 4
ln/nm.

(2) PTN phi thc hin kim sot cht lng kt
qu th nghim thng xuyn vi tn sut
ty thuc vo phng php th, tn sut v
k thut th nghim nhng phi m bo t
nht 1 nm/ln cho tt c cc ch tiu c
cng nhn. H s thc hin vic kim sot
ny phi c lu y v sn sng trnh
by trong qu trnh nh gi.

(3) Cc d liu kim sot cht lng kt qu th
nghim cn c lu h s sao cho c th
nh gi xu hng ca cc kt qu v thc
hin bin php thch hp kp thi (v d:
biu kim sot cht lng/control chart).


(4) Chng trnh kim sot mc tin cy ca
kt qu th nghim phi bao gm cc ni
(3) Laboratory staff shall check condition of
sample when received. When sample
condition does not ensure or not enough
volume against method, this fact shall be
acknowledged on reports and client shall
confirmed by writing on the record.


(4) Except special case, laboratory shall keep
sample at least until get test results or longer
if any. Sample shall be kept in suitable
container and condition.



5.9. Assuring the quality of test results

(1) Laboratory wishing to maintain
accreditation for tests performed less
frequently shall have a documented
procedure to describe how they assure the
results generated by infrequently performed
tests and at least performed tests 4 times per
year.

(2) Laboratory shall perform assuring the
quality of test results with suitable frequency
depend on method, perform test frequency
and technique to do the tests but at least
once per year for all accredited tests.
Quality control data shall be fully
documented and ready to show when
assessment.

(3) Quality control data shall be fully
documented in such a way that they are
readily accessible for evaluation of trends in
analysis, and these trends shall be monitored
with appropriate action being taken when
necessary (example: control chart).

(4) The program for monitoring the reliability
of test results shall include: natural and
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AGL 03 Ln ban hnh: 4.12 Trang: 15/34
dung: i tng th, hnh thc thc hin,
ngi thc hin, ngi nh gi kt qu.
PTN phi c cc tiu ch nh gi kt
qu.

(5) PTN la chn nh cung cp chng trnh th
nghim thnh tho/ so snh lin phng (PT)
v tham gia nh k theo qui nh trong th
tc th nghim thnh tho/so snh lin
phng APL 03.

(6) Nu PTN tham gia PT cho cc php th
c cng nhn m kt qu khng t th
phi thc hin hnh ng khc phc v np
bo co hnh ng khc phc, bng chng
ti BoA. Trng hp bo co hnh ng
khc phc ca PTN khng c BoA chp
nhn th BoA s tin hnh nh gi b sung
hoc tm thi nh ch cng nhn cho cc
php th

(7) PTN phi tham gia cc chng trnh th
nghim thnh tho/ so snh lin phng do
BoA t chc nu ph hp vi phm vi m
PTN c cng nhn.

Trng hp chng trnh th nghim thnh
tho/so snh lin phng nm ngoi phm vi
m PTN c cng nhn nhng nu ph
hp vi nng lc ca PTN th PTN c th
ng k tham gia .

5.10. Bo co kt qu

(1) PTN c cng nhn phi s dng logo ca
BoA trong bo co kt qu th nghim thuc
phm vi c cng nhn. Vic s dng logo
ca BoA phi tun th qui nh v s dng
du ca BoA.

(2) Bin bn th nghim phi c xc nhn bi
nhng ngi c thm quyn k c BoA
tha nhn.

range of the tests, method, testing staff,
evaluate results staff. Laboratory shall have
criteria for accept or rejecting suspect
results.

(5) Laboratory shall selection PT provider and
participate regularly base on requirement of
APL 03 PT procedure of BoA.



(6) Laboratory shall take corrective action when
have outliers results for accredited tests after
participated PT program. The corrective
action report and evidence shall be sent to
BoA. BoA may conduct assessment
(follow up visit) or suspend accreditation
of that tests if does not accept the evidence
of corrective action.


(7) Accredited laboratories shall participate PT
programs concerning to accredited scope,
which program is organized and carried out
by BoA or BoA is contact point.

When PT program outside of laboratory
accredited scope but corresponding with
laboratory capability, laboratory could
register to participate.


5.10. Reporting the results

(1) Accredited laboratory shall use BoA
logo to reports for accredited tests.
Laboratory shall comply with Guidance for
use of accreditation logo and symbol of
BoA.

(2) Test report shall be examined by BoA
approved signatory.


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AGL 03 Ln ban hnh: 4.12 Trang: 16/34
(3) Trong bo co th nghim nu c cc php
th cha c cng nhn th PTN phi ch
thch vo bo co xc nh r php th
cha c cng nhn.
PTN c th ch thch: cc php th nh
du * l cc php th cha c cng nhn.


(4) Trong bo co th nghim nu c cc php
th ca mt PTN c cng nhn khc
(nh thu ph) th cn ch r ch tiu no
c thc hin bi nh thu ph, tn nh
thu ph.

(5) Nu kt qu th nghim nm phm vi gn
gii hn ph hp hay khng ph hp theo
qui nh k thut ca sn phm, i tng
th cn tnh khng m bo o v PTN
phi bo co khng m bo o cng kt
qu th nghim.
(3) Where results of tests not covered by the
scope of accreditation are included on test
reports, laboratory shall have notation which
tests are out of accredited scope.
Laboratory may notation: tests have
been defined by * are not including in
accredited scope.

(4) Tests report may have results of sub-
contractored work from an accredited
laboratory shall define the test results and
name of sub-contractor.


(5) If the results of a test fall into the range
where neither compliance nor non-
compliance can be proved, taking into
account the estimated uncertainty of the
measurement, then the result and its
associated measurement uncertainty shall be
reported.

























PHN 3 CHU K HIU CHUN, KIM PART 3 CALIBRATION AND CHECK
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Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 17/34
TRA THIT B THNG THNG

Ni dung phn 3 ny nu chi tit cc yu cu hiu
chun v kim tra thit b thng thng s dng
trong cc PTN lnh vc Ha.


Bng chu k hiu chun v kim tra thng thng
cho cc thit b lnh vc th nghim ha c nu
trong phn 3 ca ti liu ny. Cc chu k nu
trong bng l chu k ln nht cho mi thit b da
vo:
- Thit b cht lng tt, kh nng hot
ng n nh, c lp t v tr thch
hp v s dng hp l;
- Nhn vin am hiu, thnh tho thc
hin nhng kim tra thit b ni b;
- Tt c cc hot ng kim tra khng
nh thit b hot ng tt.

PTN phi rt ngn khong thi gian gia cc ln
hiu chun v/ hoc kim tra khi thit b hot ng
trong iu kin t l tng hn. Nu c bt k
nghi ng no v s h hng ca thit b th PTN
cn thc hin hiu chun li ngay lp tc v sau
gim chu k cho ti khi thy rng thit b t
c n nh.

Gim khong thi gian gia cc ln hiu chun
v/ hoc kim tra cng c th c yu cu trong
cc ng dng th nghim c th hoc vi cc cu
hnh thit b c th.

PTN c th ko di chu k hiu chun da trn
cc thng s nh theo di d liu hiu chun,
kim tra chng minh s n nh ca thit b,
tn sut s dng, chnh xc yu cu hoc PTN
c nhn vin nng lc tin hnh kim tra ni
b hoc tham gia t kt qu tt trong cc chng
trnh th nghim thnh tho.

PTN c th gim chi ph hiu chun bng cch
trin khai hot ng hiu chun ni b.
INTERVALS OF GENERAL EQUIPMENTS

The content of part 3 shows detailed requirements
for calibration and check intervals of general
instruments/equipments that used in chemical
testing laboratory.

The table includes the information on calibration
and check intervals for general equipment of
chemical testing laboratory was showed in part 3
of this document. The intervals are maximum
intervals for each ones and are based on:
- Good quality, stable operation ability,
installation at suitable location and
reasonableness utilization of equipments;
- Understanding and proficiency staffs to
check themselves equipments;
- All of checks were carried out to confirm
the good operation ability of equipments.

Shorter intervals between calibrations and/or
checks may be required when the equipment
operates under less than ideal conditions. If any
suspicion of damage arises, the equipment must be
recalibrated immediately and thereafter at reduced
intervals until it is shown that stability has not
been impaired.

Furthermore, reduced intervals between
calibrations and/or checks may also be required in
particular testing applications or with particular
equipment configurations.

Longer intervals between calibrations could be
based on parameters such as calibration and check
data to prove stability, frequency of use, accuracy
required of equipments or expertise ability of staff
to perform in-house checks or successful
participation in proficiency testing programs.

The laboratory can calibrate equipment
themselves in order to reduce of calibration fee.

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Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 18/34

Vic hiu chun thit b PTN v cc chng trnh
kim tra phi gm c:
- bn giao cc thit b mi (gm: hiu
chun ban u v kim tra sau khi lp
t);
- kim tra hot ng (kim tra trong khi s
dng vi cc chun chnh v cht chun);
- kim tra nh k (kim tra gia k nhng
tng i ton din, c th bao gm hiu
chun mt phn thit b)
- bo dng theo k hoch ni b hoc ca
nh cung cp c chuyn mn;
- ti hiu chun li ton b

Equipment calibration and checking program shall
cover:
- handover of new equipment (including
initial calibration and checks after
installation);
- operational checking (checking during
use with reference items or materials);
- periodic checking (interim but more
extensive checking, possibly including
partial calibration);
- scheduled maintenance by in-house or
specialist contractors;
- Complete recalibration.
CHU K HIU CHUN, KIM TRA THIT
B TH NGHIM THNG THNG

Cc yu cu di y v chu k ti a PTN c th
la chn thc hin hiu chun v kim tra cc
thit b th nghim thng thng trong PTN. Cc
khong thi gian c a ra cho tng loi thit b
l khong thi gian ti a v ph thuc vo yu
cu v chnh xc v cch s dng cc thit b.

Thng thng vic hiu chun c thc hin bi
cc phng hiu chun c nng lc v theo qui nh
ca c quan cng nhn (BoA). PTN sau khi nhn
giy hiu chun s tin hnh nh gi thit b c
ph hp vi mc ch s dng ti PTN. Nu
phng th nghim mun t thc hin cc php
hiu chun thi phi chng minh rng phng c
nng lc thc hin cng vic ny theo nh quy
nh iu 5.6.2.1 ca ISO/IEC 17025.

Cc php kim tra thng c cc k thut vin
ca phng th nghim thc hin hoc cc n v
cung cp dch v cho PTN.

CALIBRATION AND CHECK INTERVALS
FOR GENERAL EQUIPMENTS

The requirements described below are maximum
intervals that laboratories can select for calibration
and check of general equipments. The intervals
are maximum intervals for each ones and are
based on accuracy and equipment use purpose.


Usually calibration has been conducted by
capabilities laboratory base on requirement of
BoA. Laboratory shall evaluate the calibration
results when received calibration certificate to
ensure the calibration results fitness purposes.
When laboratory would like to conduct calibration
themselves, they shall demonstrate that laboratory
have enough capabilities to perform conformity
with requirement of 5.6.2.1 of ISO/IEC 17025.

Checking equipment should be performing by
technician or services organization.





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Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 19/34
Thit b
Chu k hiu
chun (nm)
Chu k kim
tra (thng)
Phng php v khuyn ngh
Equipment
Calibration
period (year)
Check period
(month)
Method and recommendation
CN
BALANCES
3
(vi iu kin
kim tra nh
k nghim
ngt theo qui
nh ct bn)

3
(shall conduct
check period
as next
column)








Hiu chun c thc hin bi phng hiu chun theo qui
nh APL 02 BoA hoc PTN t hiu chun nhng phi
p ng cc yu cu ca mt phng hiu chun theo
ISO/IEC 17025 cho hot ng hiu chun cn.
Conducted by accredited laboratory against APL 02-BoA
or inhouse calibrate if comformity with requirement of
ISO/IEC 17025 for calibration.
Hng ngy
Daily
Kim tra hng ngy c th bng mt trong cc cch:
- Kim tra lp li.
- Kim tra 1 im thng s dng.
Daily check should choose one way as:
- Repeatability check
- One point check
1 Kim tra nh k cho 1 di o thng s dng
One range check
6 Kim tra nh k cc di o
All range check
1 Hng ngy
Daily
Kim tra hng ngy c th bng mt trong cc cch:
- Kim tra lp li.
- Kim tra 1 im thng s dng.
Daily check should choose one way as:
- Repeatability check
- One point check
3 Kim tra nh k cc di o
All range check
QU CN/ MASSES
Chun - Ton b bng
thp khng g hoc hp
kim Ni-Cr
Reference - of integral
stainless steel or nickel
chromium alloy
3
sau l
/then
6

Hiu chun c thc hin bi phng hiu chun theo qui
nh APL 02 BoA hoc PTN t hiu chun nhng phi
p ng cc yu cu ca mt phng hiu chun theo
ISO/IEC 17025 cho hot ng hiu chun cn

Conducted by accredited laboratory against APL 02-BoA
or inhouse calibrate if comformity with requirement of
ISO/IEC 17025 for calibration. Cng tc - thp khng g
hoc hp kim Ni-Cr
Working - stainless steel
or nickel chromium alloy
3


Cng tc hp kim khc
Working - other alloy
1
DNG C THY TINH/ GLASSWARE
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Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 20/34
Thit b
Chu k hiu
chun (nm)
Chu k kim
tra (thng)
Phng php v khuyn ngh
Equipment
Calibration
period (year)
Check period
(month)
Method and recommendation
Pipet, buret, bnh nh
mc
Pipetters, burettes,
volumetric flasks
Ban u (tu
thuc mc
ch s dng)
Initial
( subject to
nature of
intended use)
12
Dng c thu tinh cp A cn c s dng khi th nghim
yu cu mc chnh xc cao
Kim tra chm, ng mc dung tch thng dng
bng cn phn tch thch hp
(kim tra i din cho tng l/chng loi)
Grade A glassware distillation receivers should be used
where a high degree of accuracy is required.
Check precision and accuracy of volume delivered at
settings in use by suitable balance
(check represent for batch/type)
Buret, pipet t ng
dng pit tng
piston operated
including: pipetter,
dispensers, diluters,
displacement burettes
Ban u (tu
thuc mc
ch s dng)
Initial
( subject to
nature of
intended use)
6
Dng c thu tinh cp A cn c s dng khi th nghim
yu cu mc chnh xc cao
Kim tra chm, ng mc dung tch thng dng
bng cn phn tch thch hp.
Grade A glassware distillation receivers should be used
where a high degree of accuracy is required.
Check precision and accuracy of volume delivered at
settings in use by suitable balance
(check represent for batch/type)
NHIT K/ THERMOMETERS
Chun u, in tr
Platin
Refefence, platunum
resistance

-40
0
C n/to 250
0
C 5 6 Kim tra ti im bng
Check at ice point
<-40
0
C v/and >250
0
C 2 trc khi s
dng
Before use
Kim tra in tr ti im bng
Check resistance at ice point
Chun cng tc, in tr
Platin
Refefence, platunum
resistance

-40
0
C n/to 250
0
C 5 6 Kim tra ti im bng
Check at ice point
<-40
0
C v/and >250
0
C 2 6 Kim tra in tr ti im bng
Check resistance at ice point
Chun u, nhit k thy
tinh
Reference, lidquid-in-
glass (where kept as a
reference)
10

trc khi s
dng
Before use
Kim tra ti im bng
Check at ice point
Chun cng tc, nhit k
thy tinh
Reference, lidquid-in-
glass (where kept as a
reference)
5

6 Kim tra ti im bng
Check at ice point or against a reference thermometer at 1
point in range.
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AGL 03 Ln ban hnh: 4.12 Trang: 21/34
Thit b
Chu k hiu
chun (nm)
Chu k kim
tra (thng)
Phng php v khuyn ngh
Equipment
Calibration
period (year)
Check period
(month)
Method and recommendation
Cu o nhit AC - chun
u v cng tc
AC temperature bridge
reference and working
5
Cu o nhit DC
Measurement instrument
DC bridge type
1
(chun u/
reference)
2
(cng tc/
Working)


Chun u - H thng
ch th nhit c hoc
khng c u d nhit,
dng cm tay, bn, t
ghi, mt hoc nhiu knh
Hand-held, bench type
and temperature loggers
1 6 Kim tra ti im bng
Check at ice point
Cng tc - H thng ch
th nhit c hoc
khng c u d nhit,
dng cm tay, bn, t
ghi, mt hoc nhiu knh
Hand-held, bench type
and temperature loggers
2 6 Hiu chun phi thc hin 1 nm/ln nu khng c chun
u
Calibrate every 12 months if the facility does not have a
reference device

Kim tra so vi chun nhit s dng. Trng hp s
dng nhiu hn 1 im nhit th chn im yu cu kht
khe nht. Kim tra im bng nu khng c chun u
(dng t ghi khng s dng mt nhit k t ghi khc cng
loi khim tra)
Check against a reference device at the temperature of use.
If used at more than one temperature, choose the most
critical temperature. Check at ice point if the facility does
not have a reference device. (For data loggers the
reference device cannot be another data logger of the same
type).
1 6
Hng ngoi
Infra - red
1 6 Kim tra ti im bng
Check at ice point
L NUNG
FURNACES
Ban u
Initial

3 Kim tra nhit vi u d nhit thch hp
Monitor temperature with appropriate sensor
12 Kim tra lp li, chnh lch nhit gia cc khu vc
trong t
Check temperature variation within the working zone
T MI TRNG
ENVIRONMENTAL
CONDITIONING
CHAMBERS
3 Khi s dng
On use
IEC 60068-1,IEC 60068-2-38,IEC 60068-2-39
Kim tra ti im nhit s dng
Check at working temperature
THIT B CN KIM SOT NHIT / TEMPERATURE CONTROLLED ENCLOSURES
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AGL 03 Ln ban hnh: 4.12 Trang: 22/34
Thit b
Chu k hiu
chun (nm)
Chu k kim
tra (thng)
Phng php v khuyn ngh
Equipment
Calibration
period (year)
Check period
(month)
Method and recommendation
T lo ha
Ageing
5 Hng ngy
Daily
Kim sot nhit bng du d thch hp
Monitor temperature with appropriate sensor
T BOD
BOD
1 khi s dng
On use
Kim tra nhit lc bt u, nhit ti a v ti thiu
ca t phi c kim sot trong qu trnh th nghim.
Check the temperature at the start of the test. The maximum
and minimum temperature of the laden chamber must be
monitored for the test period.
T sy
Drying
Ban u
Initial

khi s dng
On use
Kim sot nhit bng du d thch hp
Monitor temperature with appropriate sensor
12 Kim tra lp li, chnh lch nhit gia cc khu vc
trong t
Check temperature variation within the working zone
T lnh
Refrigerators
Hng ngy
Daily

Khi nhit t lnh cn c kim sot th thc hin kim
sot nhit qui nh bng nhit k (u d nhit hoc
nhit k thy tinh)
Where critical, the temperature of the working space must
be monitored by an appropriate temperature sensor
throughout use.
T sy chn khng
Vaccum
12 Kim tra lp li, chnh lch nhit v p sut gia cc
khu vc trong t
Check temperature variation and pressure in the working
space.
CP NHIT IN/ PYROMETER
chun u
Reference
3 BS 1041 phn 5. Hiu chun bi c quan c thm quyn
Calibration by an approved testing authority
in t
electronic
1
cng tc
working
6 kim tra bng chun u
Check against reference pyrometer
NHT K/ VISCOMETERS

ng xi phng (ng hnh
ch U)
U tube

Chun
Reference
ban u,
10
Initial
then 120
S dng nht chun
ASTM 2162
Against reference oils.
Cng tc
Working
ban u
2
Initial
then 24
S dng nht m bo cht lng so vi chun hoc s
dng nht chun
ASTM 2162/D445; IP 71
Using quality oils against reference tubes or using
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AGL 03 Ln ban hnh: 4.12 Trang: 23/34
Thit b
Chu k hiu
chun (nm)
Chu k kim
tra (thng)
Phng php v khuyn ngh
Equipment
Calibration
period (year)
Check period
(month)
Method and recommendation
reference oils
Cc loi khc
Other

Brookfield ban u
Initial
S dng nht chun
Against reference oils.
24
1 S dng nht m bo cht lng (v d: ca nh sn xut)
Against quality (i.e. manufacturers) oils.
Ferranti ban u
Initial
S dng nht chun
Against reference oils.
3
Zahn ban u Initial S dng nht chun
Against reference oils.
12
T TRNG K / HYDROMETERS
Chun
Reference
5
Loi thy tinh - Cng tc
Working - glass
12 Kim tra so vi t trng k chun hoc chun b mi dung
dch bit t trng ASTM-E126
Check against reference hydrometer or in newly prepared
solutions of known density.
Loi kim loi - Cng tc
Working - metal
6 ISO 649.1,.2, ISO 650
Khi s dng
On use .
Kim tra trt ca thc
Check that scale has not slipped
THIT B T TRNG/
DENSITY METERS
Ban u
Khi nhit
th nghim
thay i hoc
sau khi lau
cell
Initial and
whenever test
temperature
is changed or
cell cleaned
ASTM D 4052 or ASTM D5002


Hng ngy
Daily
S dng vt liu tinh khit bit t trng v n nh
With pure substance of known density and stability
Hng tun
Weekly
Khng kh hoc nc ct 2 ln
Air and double-distilled water
M K/ HYGROMETER
m k Assmann & Sling
Assmann & Sling
psychrometers
10
6 So snh vi cp nhit in ti nhit phng vi bc kh
Compare thermometers at room temperature with wick dry.
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AGL 03 Ln ban hnh: 4.12 Trang: 24/34
Thit b
Chu k hiu
chun (nm)
Chu k kim
tra (thng)
Phng php v khuyn ngh
Equipment
Calibration
period (year)
Check period
(month)
Method and recommendation
m k t ghi
Thermohygrographs
Hng tun
Weekly
Kim tra vi m k c hiu chun thch hp
Check against a calibrated psychrometer, if capacitance
type
Nhit-m k loi in t
Electronic types
1 So vi m k chun
Check against a calibrated thermometer at ambient
temperature.
KH P K/ BAROMETER
Fortin ban u
Initial then

60 Kim tra ti 1 im
One point check with transfer instrument.
Aneroid 1
P K/ MANOMETERS
Chun, chun cng tc
(dung dch thu ngn)
Reference and Working,
liquid (Mercury based)
10 36 Kim tra sch ca du
Check the cleanliness of the fluid
Chun, chun cng tc
(dung dch khc)
Reference and Working,
liquid (other than
Mercury)
3 18 Kim tra sch ca du
Check the cleanliness of the fluid
in t
Electronic
1
THIT B O P SUT/ PRESSURE EQUIPMENT
Cc p k kim tra
hiu chun p k cng
nghip
Test gauges used for
calibration of industrial
gauses
1
Cc p k cng nghip
khng ph thuc ti
trng va p
Industrial gauges not
subject to shock loading
1
Cc p k cng nghip
ph thuc ti trng va
p
Industrial gauges subject
to shock loading
6 month
Cc b chuyn i p
sut
Pressure transducers
1
Cc b hiu chun
Calibrators
1
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AGL 03 Ln ban hnh: 4.12 Trang: 25/34
Thit b
Chu k hiu
chun (nm)
Chu k kim
tra (thng)
Phng php v khuyn ngh
Equipment
Calibration
period (year)
Check period
(month)
Method and recommendation
MY LY TM
CENTRIFUGES
2 1 Trng hp khi s dng c yu cu k thut v tc
S dng my o tc kim tra
Tachometer (mechanical stroboscope or light cell type, or
by other approved means) where operating speed is
specified.
U THI KH
AIR FLOW NOZZLES
ban u
Initial
12 Kim tra ng knh ng
Check throat diameter.
THC CP/
CALLIPERS
2
THC DY, THC/ TAPE MEASURES, RULES
Thc dy
Tape measures
Ban u BS 4035
24 n/to 60 Kim tra chiu di ti a, ph thuc vo yu cu s dng
v chnh xc
Check at maximum length, depending on use and accuracy
required
Thc thp/Steel rules Ban u BS 4372
CC THIT B O IN/ ELECTRICAL INSTRUMENT
ng h vn nng ch th
s
Digital multimeters
1 6 So snh vi cc ng h c di o thng thng
Calibrate over all ranges and parameters of use.
Calibration must include linearity.
Compare with meters of similar resolution
ng h o vn nng
dng Analog
Analog meters
2 6 So snh vi cc ng h c di o thng thng
Calibrate over all ranges and parameters of use.
Calibration must include linearity.
Compare with meters of similar resolution
Data loggers 1 1 Kim tra im 0 v im cc i
Check at zero and the maximum point.
O LU LNG / FLOWMETERS
Lu lng k kiu phao
(chun u)
Rotameters (Reference)
Tc cao > 1 L/pht
High flow > 1 L/min
Tc chm < 1 L/pht
Low flow < 1 L/min

24
ASTM D 3195
ng h lu lng kiu bng x phng
Soap bubble flow meter or any type of reference flowmeter
Lu lng k kiu phao
(chun cng tc)
Rotameters (Working)
mi ln s
dng
Each time on
use
ng h lu lng kiu bng x phng
Soap bubble flow meter or any type of reference flowmeter
Lu lng k kiu ng
Orifice plates
ban u
Initial
BS 1042 phn 1 hiu chun bi c quan c thm quyn
Calibration by an approved testing authority.
6 Kim tra bng ngoi quan xem c b nt, mng i, bn
Visual inspection for damage, wear or contamination
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AGL 03 Ln ban hnh: 4.12 Trang: 26/34
Thit b
Chu k hiu
chun (nm)
Chu k kim
tra (thng)
Phng php v khuyn ngh
Equipment
Calibration
period (year)
Check period
(month)
Method and recommendation
ng h nc
Wet test meters
24 ASTM D 1071
ng h lu lng
Electronic soap film
like

1 3 thng
nu kt qu
trong phm vi
3 % v thi
hn c th
n 6 thng
Monthly for 3
months then,
if
measurements
are within
3% of
the expected
result, the
interval
can be
lengthened to
6 months.
Theo dng h lu lng chun th cc di s dng
Against primary flow meter over the range of use
(including high flow rates where used).
VI K
MICROMETERS
5
1 Kim tra im 0 v 1 im trong di o thng dng
Check zero and one point against gauge block. Inspect
anvils.
MY O KHC X
REFRACTOMETERS
6

Kim tra bng bromonaphthalene hoc cht chun khc
bit trc cc ch s khc x
Check against bromonaphthalene or other reference
compound of known refractive index.
khi s dng
Each time on
use
Kim tra bng nc ct
Check by distil water
SNG/ SIEVES Ban u
Initial
Compliance certificate to AS 1152, BS 410.
12 Ph thuc vo yu cu v chnh xc, tn sut kim tra t
hay nhiu c th ph thuc vo cc b chun hoc cc vt
liu chun ph hp.
Depending on the accuracy required, more or less frequent
checks may be required against a reference set or a
suitable reference material.
Khi s dng
Each time on
use
Kim tra ngoi quan vt mi mn v lin kt
Visual check for wear and binding.
MY O IN TH/ POTENTIOMETERS
Chun u/ Reference 5 BS 1041 phn 5. Hiu chun bi c quan c thm quyn
Calibration by an approved testing authority

Chun cng tc/ working 12 kim tra bng chun u
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AGL 03 Ln ban hnh: 4.12 Trang: 27/34
Thit b
Chu k hiu
chun (nm)
Chu k kim
tra (thng)
Phng php v khuyn ngh
Equipment
Calibration
period (year)
Check period
(month)
Method and recommendation
NG H O THI
GIAN
TIMING DEVICES
6 Kim tra so vi ng h truyn thi gian ca Vin o
lng Vit Nam qua internet.
Test accurally against a speaking clock. Two
measurements separated by an appropriate interval.
CC THIT B HA
L: AAS, GC, HPLC,
ICP
PHYSIOCHEMISTRY
EQUIMENT: AAS, GC,
HPLC, ICP
Ban u
Initial
Hiu chun ban u bng mu chun c chng nhn
(Certified Reference Material - CRM) c th tham kho
theo qui nh ca nh sn xut thit b, phng php th.
Calibration by Certified Reference Material CRM against
test method or equipment manufacturer requirements
nh k (theo
qui nh
phng php
th, nh sn
xut thit b)
periodic
(against test
method,
equipment
manufacturer)
Hiu chun bng mu chun (Reference Material - RM) c
th tham kho theo qui nh ca nh sn xut thit b,
phng php th.

Calibration by Reference Material RM against test
method or equipment manufacturer requirements


Trc khi s
dng (theo
qui nh
phng php
th, nh sn
xut thit b)
Each time on
use
(against test
method,
equipment
manufacturer)
Theo qui nh ca nh sn xut thit b v/hoc phng
php th.

Against test method or equipment manufacturer
requirements


nh k (theo
qui nh
phng php
th, nh sn
xut thit b)
periodic
(against test
method,
equipment
manufacturer)
Bo tr/kim tra ton b h thng theo qui nh ca nh sn
xut.

Maintenance system/ check system against manufacturer
requirements





PH LC: HNG DN HIU CHUN
MT S THIT B
Cc hng mc c th ca mt s thit b c kit
k di y cng vi hng dn hiu chun
ANNEX: GUIDE TO CALIBRATION OF
EQUIPMENT
Some specific equipment below with guide to in-
house calibration, maintenance.
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AGL 03 Ln ban hnh: 4.12 Trang: 28/34
ni b, vn hnh v bo dng.

NHIT LNG K
Xc nh ng lng nc bng axt benzoic
theo chu k 6 thng.

THIT B O DN
o dn ti mt im kim tra ang s dng v
kim tra ton b thang chia mi nm. Theo ASTM
D 1125 hoc theo hng dn s dng ca nh sn
xut.

THIT B O LNG OXI HA TAN
o dn ti im 0 v mt im ang s dng
bng mt trong cc phng php sau:
- Kim tra vi nc bo ho
- Kim tra vi nc bo ha xi
- Kim tra vi chun Winkler

Kim tra im 0 c th thc hin bng cch o
DO ca dung dch chun b sn bng cch cn 1g
sunphit natri v mt cht tinh th clorit coban
trong 1 lt nc. Thc hin o hiu chun s
c DO v phi m bo khng ln hn 0,2 mg/L.


THIT B O pH
Kim tra trc mi ln o dng t nht 2 dung
dch m chun ng vi pH tng ng vi khong
pH ca mu th nghim. 6 thng 1 ln kim tra
3 m chun. H s th hin vic kim tra cn
c lu. Tham kho ti liu APHA 4500-H v
BS 1647. in cc cng phi c kim tra t nht
l hng tun, hoc tn sut ln hn. Tham kho
theo hng dn s dng ca nh sn xut.


THIT B O C
o dn ti mt im tng ng vi c ca
mu th, v hiu chun y mi nm. Theo
APHA 2130B. (cht chun c th mua hoc PTN


CALORIMETERS
Determine water equivalents using certified
benzoic acid at six monthly intervals.

CONDUCTIVITY METERS
Conduct a one-point check on use and check the
complete scale each year. Reference to ASTM
D1125 or manufacturer guidelines.


DISSOLVED OXYGEN METERS
On use, conduct a zero check and a one-point
check by one of the following check procedures:
- Check against water saturated air;
- Check against oxygen saturated water
- Check against the value obtained by the
Winkler titration.
A zero check can be carried out by measuring the
dissolved oxygen (DO) for a prepared solution
containing 1g sodium sulfite and a few crystals of
cobalt chloride in 1 L of water. If the meter is
properly calibrated the DO reading should be less
than 0,2 mg/L.

pH METERS
Calibrate the pH before using at least two buffer
solutions suitable with measure range. One per
six months using three buffer solutions. Records
must be kept of all calibrations and checks,
including the temperature of all buffer and sample
solutions measured. Method 4500-H+; BS 1647,
and references therein. The electrode system
should be check weekly or more. References to
recommended by the instrument manufacturer.

TURBIDIMETERS
Conduct a one-point check appropriate to the
anticipated turbidity of the sample being
measured, and a complete calibration each year.
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AGL 03 Ln ban hnh: 4.12 Trang: 29/34
t to. Kim tra li cht chun ca nh cung cp
hng nm bng chun formazin).



THIT B PHN TCH T NG
Ton b h thng cn c kim tra/hiu chun
(tham kho hng dn ca nh sn xut) mi ln
s dng v km theo vic kim sot cht lng
bng cht chun, hiu chun ng nn v mu
trng. Cn c k hoch lm mu lp v kim tra
thu hi bng mu thm. Trong trng hp phn
tch mt chui mu, phi p dng bin php thch
hp bo m thit b vn hnh tt trong sut thi
gian phn tch mu.

Th tc kim sot cht lng cn kim tra c
tnh hiu qu ca bt k phn ng trong qu trnh
th nghim v d ct kh cadmium s dng cho
phn tch nitrate.

Ni chung cc thit b phi c bo tr theo qui
nh ca nh sn xut. Nu c yu cu kim sot
nhit (v d b iu nhit) phi c theo di
bng thit b hiu chun (nhit k hoc cp
nhit in cng tc). Cc b phn ca thit b cn
c kim tra nh k v ch ra cch kim sot
cht lng khi c vn khng ph hp.


THIT B O PH
a s cc php phn tch nh lng trong phng
th nghim ha c s dng thit b o quang ph
hoc so mu. Do phng th nghim cn thc
hin thng xuyn v ghi nhn h s v kim tra
v hiu chun cho cc thit b quang ph t ng
hoc so mu. ng cong hiu chun c th s
dng trong mt khong thi gian nhng phi c
kim sot bng mu trng v mu chun cho mi
ln th nghim v phi c thit lp li mt
thng mt ln.


Refer APHA 2130B. (Reference standards may be
purchased or made up in the laboratory. Check
manufacturer supplied standards annually against
formazin standards.)

AUTOANALYSERS
The total system must be checked/ calibrated on
use (ref recommended by the instrument
manufacturer) and monitored during each run with
quality control measures such as reference
materials, calibration/drift checks and blanks. The
scheduled use of duplicates and recovery checks
by spiked samples is also recommended when a
bath of sample being measured to ensure status of
equipment.

Quality control procedures need to verify the
efficiency of any chemical reactions which are
part of the method (eg. cadmium reduction
column used for nitrate analysis).

In general the equipment must be maintained in
accordance with manufacturers specifications.
Temperature controlled enclosures (such as water
baths) must be monitored with calibrated
equipment (working thermometers or
thermocouples). Individual components should be
checked routinely and whenever quality control
measures indicate a problem.

SPECTROPHOTOMETERS
A great number of the quantitative analyses
performed in a chemical testing facility involve
some form of spectrophotometric or colorimetric
measurement. It is essential that a facility carry
out regular, recorded calibration checks on all
spectrophotometers or automated devices
employing spectrophotometers or colorimeters.
The calibration curve may be use for a period time
but shall be use blank and QC samples for each
measured. A new calibration curve must be
prepared at least every month.

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AGL 03 Ln ban hnh: 4.12 Trang: 30/34
Thit b phi c kim tra/hiu chun nh k v
phi bao gm c vic kim tra s chnh xc ca
bc sng, hp th, tnh tuyn tnh, lp li,
phn gii, nh sng phn tn, tnh trng n v
ph hp t bo quang in. Vic kim tra/hiu
chun phi thc hin ph hp vi hng dn ca
nh sn xut v/hoc cc s liu, ti liu lit k
trong khong ph hp vi cc th tc th nghim
v iu kin mi trng s dng thit b (nhng t
nht ba thng mt ln).

Tt c thit b phi c kim tra bng cc cht
chun ph hp. Mu trng v t nht 2 im trn
ng cong hiu chun cng phi c kim tra.
Vic hiu chun ny phi gip theo di c tnh
trng ca h thng thit b qua cc ln kim tra
pht hin bt k s khc bit no ca h thng.

Mt s phng php phn tch s dng cc thit b
di y c cp cch kim tra v s dng thit
b gm c:

a) T ngoi/ kh kin:

ASTM E131 Thut ng lin quan n php ghi
quang ph phn t.

ASTM E169 Thc hnh k thut chung v
phn tch nh lng bng quang
ph t ngoi

ASTM E275 Thc hnh m t v o bng
quang ph k t ngoi, kh kin
v hng ngoi gn

ASTM E925 Thc hnh hiu chun theo nh
k quang ph k c di ph di
hp khng ln hn 2nm.



ASTM E958 Thc hnh o di rng quang ph
ca quang ph k t ngoi - kh
kin.


b) Hng ngoi:
Equipment shall be checked/calibrated frequency
and shall include checks on wavelength accuracy,
absorbance, linearity, stray light and matching of
cells. These checks/calibrations must be carried
out in accordance with the manufacturers
instructions and/or the codes of practice listed
below at intervals appropriate to the test
procedures and the physical environment within
which the instrumentation is used (but at least
every three months).

All instruments must be checked on use against
appropriate reference materials. A blank and at
least two points on the calibration curve must also
be checked. These calibrations should be
compared over time to detect any system
deterioration.

Relevant standards for the checking and use of
spectrophotometers include:


a) Ultraviolet/ Visible:

ASTM E131 Standard terminology relating to
molecular spectroscopy.

ASTM E169 Standard practices for general
techniques of ultraviolet-visible
quantitative analysis.

ASTM E275 Standard practices for describing
and measuring performance of
ultraviolet and visible
spectrophotometers.
ASTM E925 Standard practice for monitoring
the calibration of ultraviolet -
visible spectrophotometers
whose spectral slit width does
not exceed 2nm.

ASTM E958 Standard practice for measuring
practical spectral band-width of
ultraviolet-visible
spectrophotometers.

b) Infrated:
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ASTM E168 Thc hnh k thut chung v
phn tch nh lng bng quang
ph hng ngoi

ASTM E932 Thc hnh m t v o bng
quang ph k hng ngoi tn x.



THIT B QUANG PH

c tnh thit b phi c kim sot khi s dng
bng cc cht chun. th hiu chun phi c
chun b s dng mu trng v bng t nht t 03
n 05 dung dch chun bao ph c khong
nng c th c trong mu phn tch.


Kim tra ng tuyn tnh phi c thc hin;
tuy nhin c hm tuyn tnh cn chun b 1
im trng v 5 im nng ng dung dch chun.
i vi hp th nguyn t, ng tuyn tnh phi
c dng da vo da trn tn hiu o ( hp
th). Cc b phn ca thit b v thit b ph tr
phi c bo dng v kim tra nh k theo cc
th tc c vn bn ha m bo c tnh
thit b quang hc. (iu ny c th thc hin bi
cc k thut vin bn ngoi). Cc tiu chun lin
quan kim tra v s dng quang ph k bao
gm:

a) Hp th nguyn t:
ASTM E 1184 Thc hnh phn tch hp th
nguyn t l graphit.

APHA 3111 Phn tch kim loi bng quang
ph hp th nguyn t ngn la.

APHA 3112 Phn tch kim loi bng quang
ph hp th nguyn t bay hi
lnh.

APHA 3113 Phn tch kim loi bng quang
ph hp th nguyn t nhit in.

APHA 3114 Phn tch asen v selen bng

ASTM E168 Standard practices for general
techniques of infrared
quantitative analysis.

ASTM E932 Standard practice for describing
and measuring performance of
dispersive infrared
spectrophotometers.

SPECTROMETERS

Instrument performance must be routinely
monitored during use with reference materials.
Calibration graphs must be prepared using a blank
and three to five solutions of standards covering
the expected concentration range of analyte in the
sample.

This may be adequate for a linear graph; however,
for a polynomial fit the graph should be prepared
with a blank plus five to six solutions of standards.
For atomic absorption, linearity checks must be
done in the absorbance mode. Spectrometer
components and supporting equipment must also
be adequately maintained and checked
periodically in accordance with documented
procedures to ensure optimal instrument
performance. (This may need to be done by
external technicians.) Relevant standards for the
checking and use of spectrometers include:

a) Atomic absorption:

ASTM E1184 Standard practice for
electrothermal (graphite furnace)
atomic absorption analysis.
APHA 3111 Metals by flame atomic
absorption spectrometry.

APHA 3112 Metals by cold-vapour atomic
absorption spectrometry.


APHA 3113 Metals by electrothermal atomic
absorption spectrometry.

APHA 3114 Arsenic and selenium by hydride
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Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 32/34
quang ph hp th nguyn t /
pht sinh hyrua.

b) Pht x nguyn t v hunh quang tia X:

AS 2563 Bc sng phn tn quang ph
hunh quang tia X Xc nh
chm.

AS 2883 Phn tch kim loi phng php
thit lp, hiu chun v chun ha
pht x nguyn t s dng h
quang/tia la in.


ASTM E135 Thut ng lin quan n ha phn
tch kim loi, qung v vt liu lin
quan.

c) Plasma lin hp cm ng:

APHA 3120 Phn tch kim loi bng quang
ph pht x plasma

d) Cng hng t ht nhn:

ASTM E386 Thc hnh trnh by d liu lin
quan n quang ph cng hng
t ht nhn phn gii cao.

SC K

a) Sc k kh
Cc thng s c trng ca thit b phi c
kim tra/hiu chun nh k bng cc cht chun.
Cc thnh phn ca h thng (my tch phn, nhit
l ct, chng trnh nhit , tc dng kh,
detector) cng phi c kim tra theo chu k, v
cc h s kim tra phi c lu gi.

b) Sc k lng, bao gm sc k lng hiu
nng cao (HPLC) v sc k ion


Ton b h thng phi c kim tra/hiu chun
bng cc chun chnh. S gim kh nng pht hin
c th c pht hin bng vic so snh cc kt
qu theo thi gian khi th bng cht chun. Cc
thnh phn ca h thng phi c kim tra nh
generation/atomic absorption
spectrometry.

b) Atomic emission and x-ray fluorescence:

AS 2563 Wavelength dispersive X-ray
fluorescence spectrometers -
Determination of precision.

AS 2883 Analysis of metals - Procedures
for the setting up, calibration and
standardization of atomic
emission spectrometers using
arc/spark discharge.

ASTM E135 Standard terminology relating to
analytical chemistry for metals,
ores and related materials.

c) Inductively coupled plasma (ICP):

APHA 3120 Metals by plasma emission
spectroscopy.

d) Inductively coupled plasma:

ASTM E386 Standard practice for data
presentation relating to high
resolution NMR spectroscopy.


CHROMATOGRAPHS

a) Gas chromatographs (GC)
Instrument performance must be routinely
monitored during use with reference materials.
System components (eg. integrators, ovens,
electronic amplifiers and detectors) must also be
checked periodically, and records kept.


b) Liquid chromatography including high
performance (or high pressure) liquid
chromatographs (HPLC) and ion
chromatography:
The total system must be monitored during use
with reference standards. Loss of efficiency may
be detected by chronological comparison of
reference material measurements. System
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Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 33/34
k v ni dng c lu gi h s kim tra.


Cc tiu chun lin quan n vic kim tra v s
dng thit b sc k gm:

ASTM D1945 Cc Phng php phn tch kh
t nhin bng sc k kh.


ASTM D4626 Thc hnh tnh ton cc h s
p ng trong sc k kh.

ASTM E260 Thc hnh sc k kh ct nhi.


ASTM E355 Thc hnh cc hng mc ca sc
k kh v nhng vn lin quan.


ASTM E516 Thc hnh kim tra detector dn
nhit dng trong sc k kh.


ASTM E594 Thc hnh kim tra detector ion
ha ngn la dng trong sc k
kh.


ASTM E682 Thc hnh cc hng mc ca sc
k lng v nhng vn lin
quan.

ASTM E685 Thc hnh th nghim detector
UV/VIS bc sng c nh dng
trong sc k lng.

ASTM E697 Thc hnh s dng cng kt in
t ECD trong sc k kh.



ASTM E840 Thc hnh s dng detector trc
quang ngn la FPD trong sc k
kh.

ASTM E1151 Thc hnh cc loi sc k ion v
nhng vn lin quan.

ISO 10301 Cht lng nc - Xc nh cc
hyrocacbon halogen d bay hi
components (eg. pumping system and detectors)
must be subject to periodic checks and details
must be recorded.

Relevant standards for the checking and use of
chromatographic instrumentation include:

ASTM D1945 Test methods for analysis of
natural gas by gas
chromatography.

ASTM D4626 Standard practice for calculation
of GC response factors.

ASTM E260 Standard practice for packed
column gas chromatography.

ASTM E355 Standard practice for gas
chromatography terms and
relationships.

ASTM E516 Standard practice for testing
thermal conductivity detectors
used in gas chromatography.

ASTM E594 Standard practice for testing
flame ionization detectors used
in gas or supercritical fluid
chromatography.

ASTM E682 Standard practice for liquid
chromatography terms and
relationships.

ASTM E685 Practice for testing fixed-
wavelength photometric
detectors used in liquid
chromatography.

ASTM E697 Standard practice for use of
electron-capture detectors in gas
chromatography.

ASTM E840 Standard practice for using
flame photometric detectors in
gas chromatography.

ASTM E1151 Standard practice for ion
chromatography terms and
relationships.

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Supplementary requirements for accreditation in the field of Chemical testing


AGL 03 Ln ban hnh: 4.12 Trang: 34/34
bng sc k kh.


BS 5443 Khuyn co v mt s tiu
chun cho cc phng php phn
tch ha hc bng sc k kh.


Phn tch kch thc ht:

c tnh thit b phi c kim sot nh k khi
s dng vi cc cht chun.

ASTM F660 Thc hnh so snh kch thc ht
trong vic s dng cc loi my
m ht khc nhau.
ISO 10301 Water quality Determination
of highly volatile halogenated
hydrocarbons - gas
Chromatographic methods.

BS 5443 Recommendations for a standard
layout for methods of chemical
analysis by gas chromatography

Particle size analysis

Instrument performance should be routinely
monitored, during use, with reference materials.

ASTM F660 Standard practice for comparing
particle size in the use of
alternative types of particle
counters.