LAMPIRAN

A. Perhitungan
Percobaan 1
MassaAs.Salisilat = 2,5 gr

nAs.salisilat = 2,5/138.12
= 18.10 x 10-3 mol

BMAs.Salisilat = 138.12 gr/mol

VAs.Anhidrida = 6,25 ml
Massa jenis = 1.045 gr/ml

nAs.Anhidrida = 6,531/90

m=xV

= 0,0725 mol

= 1.045 x 6,25
= 6,531 gr

As.Asilisat

As.Anhidrida

Aspirin

As.Asetat

M 18.10 x 10-3 mol

0.0725 mol

R 18.10 x 10-3 mol

18.10 x 10-3 mol

18.10 x 10-3 mol 18.10 x 10-3 mol

0.0544 mol

18.10 x 10-3 mol 18.10 x 10-3 mol

BMAspirin = 180 gr/mol

MassaAspirin (teori) = n x BM
= 9.05 x 10-3 x 180
= 1.629 gr
MassaAspirin (Percobaan) = 1,47 gr

% Kesalahan =

135

85

135
= 37 %
% Yield = 85/135 x 100% = 62,96 %

x 100 %

nNaOH = M x V
= 0.1 M x 0.25 L
= 0.025 mol

naspirin x V1 = n NaOH x V2
naspirin x 50ml = 0.025 mol x 5.5ml
naspirin = 0.00275 mol

naspirin = massaaspirin/BM
0.00275 = massaaspirin/180
massaaspirin = 0.495 gr
KekuatanAspirin(percobaan) = 0.495/0.0648
= 7,6 grains

KekuatanAspirin(teori) = 5 grains
= 0.324gr
Aspirin(teori) : Aspirin(percobaan)
0.324gr : 0.495gr
1 : 1.52

(1 grains = 0.0648gr)

Percobaan 2
MassaAs.Salisilat = 2,5 gr

nAs.salisilat = 2,5/138.12
= 18.10 x 10-3 mol

BMAs.Salisilat = 138.12 gr/mol

VAs.Anhidrida = 9 ml
Massa jenis = 1.045 gr/ml

nAs.Anhidrida = 9,405/90

m=xV

= 0,1045 mol

= 1.045 x 9
= 9,405 gr

As.Asilisat

As.Anhidrida

Aspirin

As.Asetat

M 18.10 x 10-3 mol

0.1045 mol

R 18.10 x 10-3 mol

18.10 x 10-3 mol

18.10 x 10-3 mol 18.10 x 10-3 mol

0.086 mol

18.10 x 10-3 mol 18.10 x 10-3 mol

BMAspirin = 180 gr/mol

MassaAspirin (teori) = n x BM
= 18.10 x 10-3 x 180
= 1.944 gr
MassaAspirin (Percobaan) = 3.25 gr

% Kesalahann =

135

111

135
= 17,7 %

% Yield = 111/135 x 100% = 82,2 %

x 100 %

nNaOH = M x V
= 0.1 M x 0.25 L
= 0.025 mol

naspirin x V1 = n NaOH x V2
naspirin x 50ml = 0.025 mol x 6 ml
naspirin = 0.003 mol

naspirin = massaaspirin/BM
0.003= massaaspirin/180
massaaspirin = 0.54 gr
kekuatan Aspirin(percobaan) = 0.54/0.0648
= 8,3 grains

KekuatanAspirin(teori) = 5 grains
= 0.324gr
Aspirin(teori) : Aspirin(percobaan)
0.324gr : 0.683 gr
1 : 2,1

(1 grains = 0.0648gr)