Professional Documents
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CONTENTS
6.0 MISCELLANEOUS 14
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REVISION STATUS
R0 83.12.20 --
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1.0 SCOPE
1.1 This basic study guide covers guidelines for setting up a chemical laboratory to
monitor the quality of water, fuel and effluents in power plants and water supply
projects. Testing facilities available in the vicinity of the operating plant and
cost-benefit analysis of having facilities in-house shall be considered while
making recommendations to client.
1.2 For chemical and industrial plants, process collaborator’s and client’s
requirements shall be considered. For utility generation plants within chemical
and industrial plants, guidelines as indicated in this document may be used with
suitable modifications.
1.3 This document does not include guidelines for laboratory furniture and
laboratory layout.
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6. Alfoc test kit for oxygen To test dissolved oxygen in feed water
12. De-ioniser with spare cartridges To produce ion free water for dilution
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16. Incubator. Temperature range- For BOD test and bacterial incubation
(-)10 to 500 C with ±0.50 C
uniformity
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(g) Refrigerator
(i) Membrane filtration holder for vacuum filtration and membrane filters
(j) Sieve shaker - Imparting both circular and vertical movement to the
sample being seived
Aperture 5.60 mm
4.00 mm
2.80 mm
2.00 mm
1.40 mm
1.00 mm
0.71 mm
0.50 mm
0.25 mm
0.149 mm
0.074 mm
Receiver
Sieve cover
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Aperture 16.0 mm
11.2 mm
8.0 mm
5.6 mm
Receiver
Sieve cover
2.5 Following miscellaneous items and glassware are required for analysis of water :
SL.NO. DESCRIPTION
1. Distillation flasks, round bottom, short neck
1000 ml capacity
2. Distillation splash heads, vertical quick fit type
3. Cone size to fit flask 24/29
Cone size to fit condenser 24/29
4. Condensers quick fit type - Liebig, Graham, Friedricks and condenser
adaptors
5. Adaptor receiver
6. Pipettes - 2 ml, 5 ml, 10 ml, 25 ml, 50 ml, 100 ml,
Bulbs class B BS 1583 1ml, 2 ml, 5ml, 10 ml,
Graduated pipette BS 700 Type 1 calibrated to deliver 0.1 ml,
Capillary pipette BS1428 Type 1 graduated for delivery
Pipette filler and dispenser
Safety pipette filler
7. Pipette filters
8. Burettes - 50 ml, 25 ml shell back class B, BS 846
10 ml (0.02 ml graduation)
Burettes - Automatic 25ml and 50 ml
Burettes - Micro-automatic 2ml and 5 ml
Burette support
Single burette holder
9. Nessler cylinders - 50ml, 100ml capacity
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SL.NO. DESCRIPTION
10. Stands for above 50ml capacity
100ml capacity
11. Measuring cylinders BS 604
10ml, 25ml, 50ml, 100ml, 250ml, 500ml, 1000ml
12. Distillation receivers 100ml with spout
13. Measuring cylinders-polythene with spout 1000ml
14. Volumetric flasks class B, BS 1792, with inter-changeable polypropylene
stoppers 25ml, 50ml, 100ml, 200ml, 250ml, 500ml, 1000ml, 2000ml
15. Beakers-pyrex low form with spout
-50ml, 100ml, 250ml, 600ml, 1000ml, 2000ml
Tall form - 400ml, 600ml
Conical - 125ml, 250ml
Beaker tongs
Beakers, Teflon 100 ml and 250 ml capacity
16. Polypropylene AZLON 1000ml, 2000ml
17. Buchner flasks - pyrex 500ml, 1000ml
18. BOD bottles
Reagent, narrow mouth stoppered polystop
125ml, 250ml, 500ml, 1000ml
Amber glass, narrow mouth, stoppered polystop
250ml, 500ml
1250 ml winchester pattern
Polypropylene narrow mouth, medium wall,
Autoclavable to 145°C
60ml, 125ml, 500ml, 1000ml, 2000ml
Polythene wash bottles 500ml
Polythene aspirator 40 lit, 9 lit
125ml dropping bottle with polythene stopper
Density bottles 50ml, 100ml capacity BS 733
Hartley funnels 7 cm dia AZLON
Gas washing bottles - Dreehsel's 500ml
Woolf bottles 500ml
Weighing bottles polypropylene 25 ml
19. Pear shaped separatory funnels: capacity 500 ml and 1000 ml
Cylindrical separatory funnels: capacity 500 ml and 1000 ml
Thistle Funnels
Porcelain funnel with fixed perforated filter plates
Funnel with fritted discs having different pore sizes
Funnels-
75mm, 200mm plain soda glass
250ml, 500ml, 1000ml separating cylindrical
Pyrex BS 2021
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SL.NO. DESCRIPTION
20. Imhoff cone 1000ml
Brush for imhoff cone
21. Wooden stand for above
22. Desiccator - vacuum 20 cm dia
Desiccator - non-vacuum 20 cm dia
23. Watch glasses - Pyrex and Teflon - 4 cm, 7.5 cm, 12.5 cm
24. Test tubes
(a)100mm x 12mm rimless, soda glass
(b)125mm x 16mm rimless, Pyrex
Test tube rack
25. Gas distribution tubes - porosity No.1
26. Glass rod - 5mm soda glass
27. Stirring rods 229 x 6.5 mm
28. Glass tubing
Id 4mm, 6mm, 8mm soda glass
29. Thermometers - general purpose BS 1704
5 to 1050 C
0 to 3600 C
30. Evaporating basins
Safety tong for casseroles
1 Pyrex flat bottomed 80mm dia, nickel round bottomed 60mm dia and
Porcelain 90mm dia
31. Crucible porcelain with fritted glass, capacity- 15 and 30 ml., pore size
from 4 to 220 microns
Walter crucible holder
Crucible tongs
Crucibles - silica glazed translucent
25ml capacity crucibles
Covers for Crucibles - Gooch - Porcelain with perforated
Crucible - nickel 25ml capacity
Platinum - 10ml capacity
32. Rubber crucible cones in 34mm large end 31mm
33. Filter paper - Whatman or equivalent grade No.1, 41 No.42, 15 cm dia
34. Glass wool
Glass fibre pads - Whatman grade, GFC or equivalent 2.5 cm, 7 cm dia
35. Retort stands - cast iron, double and single
36. Rods, mild steel - 50cm, 75cm length
37. Stands - pipette - horizontal and vertical
38. Test tube racks - 12 holes
39. Burette holders - double
40. Boss heads
41. Clamps
42. Funnel holder - double
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SL.NO. DESCRIPTION
43. Iron-wire triangles with clay tube coverings
Tripods - triangular
44. Bunsen burner - gas type
45. Gauzes - asbestos centre
46. Magnetic stirring bars 12mm, 25mm, 37mm PTFE coated
47. Stirring bar retriever
48. Rubber tubing - gas N8
Normal wall N3, N6.5, N8
PVC tubing colourless
5mm, 6.5mm, 10mm bore
49. Rubber teats - assorted sizes
50. Rubber stoppers - assorted pack
51. Corks assorted
52. Cork rings id - 80mm
53. Cork borers - set of six 4 to 10mm
54. Cork borer sharpener
55. Spatula nickel spoon one and 12 cm and 18 cm Chattaway 15.2 cm
56. Brushes-assorted for beaker, bottle and burette
57. Pinch cocks
Clips - mohr No.1, No.3
58. Pestle and mortar 12.5 cm dia, agate and porcelain
59. Tongs crucible 20 cm beaker
Furnace 38 cm
60. Gloves - latex
Gloves- asbestos guantlet disposable
61. Glass cutting knife
62. Glass cutting file
63. Hydrometers. Range 0.80 to 0.85, 0.85 to 0.90, 0.90 to 0.95, 0.95 to 1.0
and 1.0 to 2.0
64. Goggles - safety/contrast
65. Sealing tissue - parafilm 16.5 cm
66. Silicone vacuum grease
67. Stopclock
68. Tool kit
69. Paper towels - kim wipes or similar
70. Scissors
71. Gas-lighter-battery operated
72. Marking pens and refills
73. Labells - Dymo tape set
74. Laboratory coats
75. Plastic buckets 11 litre capacity
76. First aid kit-for up to 50 people
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SL.NO. DESCRIPTION
77. Eye wash bottles
78. Boiling chip
79. Litmus paper
80. Glass joints- Ball socket joints, O-ring joints, Taper inner and outer joints,
Reducing and enlarging adapters
81. Jerrycan bottles (polythene) - 10 & 20 lit capacity
82. Petri dishes
83. Trays-enamel and fibreglass
84. Visor
85. Ring support for levelling bottle
86. Flask-vacuum - 1000 ml capacity
87. Flask-Kjeldahl - capacity 500 and 800 ml
88. Aspirator with splashgon
89. Scoops for sample collection
3.1 COAL
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3.2 OIL
3.3 GAS
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3.5.1 Coal
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3.5.2 Oil
3.5.3 Gas
(a) Wind anemometer to measure wind speed using three (3) cup rotator with
sensor of optical/ultrasonic interruptor, specifying maximum wind speed
and accuracy
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(b) Wind direction sensor to indicate wind direction with an accuracy of ±50
under ambient conditions
(c) Barometric pressure sensor for gas turbine performance analysis - piezo
electric sensing element/capacitive sensing element in aluminium casing -
range 600 to 1100 mB ( 0 to 4242 metres above MSL) with accuracy ±
0.1% of overall reading
6.0 MISCELLANEOUS
The laboratory shall be well-lit and ventilated. Eye-wash fountains and safety
showers shall be provided at suitable locations inside or near the laboratory.
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APPENDIX - 1
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APPENDIX - 1 (CONTD.)
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APPENDIX - 1 (CONTD.)
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