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Silika - Dikonversi
Silika - Dikonversi
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
Sample Desc: Silika Comment:
Sample weight: 0.4271 g Sample Volume: 0.12525 cc Sample Density: 3.41 g/cc
Outgas Time: 3.0 hrs OutgasTemp: 300.0 C
Analysis gas: Nitrogen Bath Temp: 77.3 K
Press. Tolerance: 0.100/0.100 (ads/des) Equil time: 15/15 sec (ads/des) Equil timeout: 30/30 sec (ads/des)
Analysis Time: 86.4 min End of run: 2020/02/27 10:27:10 Instrument: Nova Station A
Cell ID: 96 Isotherm * Linear F/W version: 0.00
Ads Des
155.00
120.00
Volume @ STP (cc/g)
80.00
40.00
0.00
0.00 0.40 0.80 1.10
Quantachrome NovaWiiin - Data Acquiiisiiitiiion and Reductiiion for NOVA iiinstruments ©1994-2010, Quantachrome Instruments versiiion Report id:{1215528677:20200311 114826714} Page 1 of 29
11.0
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
Multi-Point BET Plot
A D BF
17.9000
16.0000
12.0000
1 / [ W((Po/P) - 1) ]
8.0000
4.0000
0.0000
0.000e+00 4.000e-02 8.000e-02 1.200e-01 1.600e-01 2.000e-01 2.400e-01 2.800e-01
V dV(r)
2.29e-01
4.26e-03
2.00e-01
3.72e-03
1.60e-01
2.98e-03
Cumulative Pore Volume (cc/g)
dV
1.20e-01 (r)
2.23e-03
(c
c/
Å/
g)
8.00e-02
1.49e-03
4.00e-02
7.44e-04
0.00e+00
0.00e+00
10.000 20.000 30.000 40.000 100.000 200.000 300.000 500.000
dV
0.0059
0.0056
0.0052
0.0048
0.0044
0.0040
0.0036
Pore Volume[cc/Å/g]
0.0032
0.0028
0.0024
0.0020
0.0016
0.0012
0.0008
0.0004
0.0000
Isotherm
Multi-Point BET
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
Langmuir
[(g/g)] [(g/g)]
4.41430e-02 5.9053e+00 1.97689e-01 1.0611e+01
7.86900e-02 7.6746e+00 2.22352e-01 1.0940e+01
1.11463e-01 8.8181e+00 2.60006e-01 1.1351e+01
1.31575e-01 9.3567e+00 2.82731e-01 1.1553e+01
1.58578e-01 9.9484e+00
LangMuir summary
Surface Area =159.172 m²/g
Quantachrome NovaWiiin - Data Acquiiisiiitiiion and Reductiiion for NOVA iiinstruments ©1994-2010, Quantachrome Instruments versiiion Report id:{1215528677:20200311 114826714} Page 10 of 29
11.0
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
DR method
[(g)] [(g)]
1.836399e+00 3.1926e-03 4.956406e-01 7.9572e-03
1.218994e+00 4.3792e-03 4.263554e-01 8.6811e-03
9.079598e-01 5.3986e-03 3.422445e-01 9.7830e-03
7.758555e-01 6.0060e-03 3.009911e-01 1.0452e-02
6.396114e-01 6.8080e-03
DR summary
Slope =-3.350e-01
Intercept =1.185e-02
Correlation factor =9.798e-01
Affinity coefficient (ß) =3.918e-01
Alpha-S method
P/PoVolume @ STP Liquid Vol. Alpha P/PoVolume @ STP Liquid Vol. Alpha
Alpha-s summary
Slope =46.353
-20.487
Alpha-S Intercept = Correlation coefficient = cc/g
1.000
Micropore volume =
-0.032 cc/g
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
Quantachrome NovaWiin - Data Acquiisiitiion and Reductiion for NOVA iinstruments ©1994-2010, Quantachrome Instruments versiion Report id:{1215528677:20200311 114826714} Page 13 of 29
11.0
Quantachrome NovaWin - Data Acquisition and Reduction
for NOVA instruments
©1994-2010, Quantachrome Instruments
version 11.0
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
Quantachrome NovaWiiin - Data Acquiiisiiitiiion and Reductiiion for NOVA iiinstruments ©1994-2010, Quantachrome Instruments versiiion Report id:{1215528677:20200311 114826714} Page 14 of 29
11.0
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
HK summary
Mode : 2.583 Å
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
SF summary
Mode : 4.430 Å
Analysis Report
Operator:nova Date:2020/02/27 Operator:nova Date:3/11/2020
Sample ID: Sample Filename: C:\QCdata\Physisorb\ 20200227_20200214-0854_1_AD.qps
MBET summary
Slope = 37.315
Intercept = 5.718e+00
Correlation coefficient, r = 0.997896
C constant= 7.526
Volume/Area summary
Surface Area Data