D-7000 HSM: ENERO 2020 Series: 0030 System: OFFLINE

LABORATORIO FARBROQUIM S.A.S

Analyzed Date and Time: 18/01/20 10:08
Processing Method: HALOPERIDOL ENE/18/20
System(acquisition): HPLC MP-07 Vial Type: BLANK
Sample Name: FASE MOVIL- DILUENTE Volume: 20,0 ul
Sample Description:
500 N-Meth 0
Inhib Inhib
Sens 5
400
Intensity (mV)

300

200

100

0 1 2 3 4 5 6 7 8
Retention Time (min)
Developed by: ANGELA GARCIA Analizado por: ISMAEL MAYORGA

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D-7000 HSM: ENERO 2020 Series: 0030 System: OFFLINE

LABORATORIO FARBROQUIM S.A.S

Analyzed Date and Time: 18/01/20 17:14
Processing Method: HALOPERIDOL ENE/18/20
System(acquisition): HPLC MP-07 Vial Type: STD1
Sample Name: ESTANDAR SST Volume: 20,0 ul
Sample Description:
500 N-Meth 0
Inhib Inhib
Sens 5

3,14, HALOPERIDOL
400
Intensity (mV)

300

200

100

0 1 2 3 4 5 6 7 8
Retention Time (min)

No. RT Name Area BC

1 3,14 HALOPERIDOL 3186019 BB

3186019

Peak rejection level: 0

RT Name k' Asym N Res
(min) (USP) (USP)

3,14 HALOPERIDOL 313,00 1,38 1041 ---

RT Name Alpha S/N Noise

(min) (uV)

3,14 HALOPERIDOL --- 521,32 808,00

Asymmetry warning outside the range of: 0,800 to 2,000

No. of theoretical plates warning at less than: 500
Resolution warning at less than: 2,000
Signal to noise ratio warning at less than: 3
Developed by: ANGELA GARCIA Analizado por: ISMAEL MAYORGA

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D-7000 HSM: ENERO 2020 Series: 0030 System: OFFLINE

LABORATORIO FARBROQUIM S.A.S

Analyzed Date and Time: 18/01/20 17:23
Processing Method: HALOPERIDOL ENE/18/20
System(acquisition): HPLC MP-07 Vial Type: STD1
Sample Name: ESTANDAR Volume: 20,0 ul
Sample Description:
500 N-Meth 0
Inhib Inhib
Sens 5

3,19, HALOPERIDOL
400
Intensity (mV)

300

200

100

0 1 2 3 4 5 6 7 8
Retention Time (min)

No. RT Name Area BC

1 3,19 HALOPERIDOL 3194390 BB

3194390

Peak rejection level: 0

RT Name k' Asym N Res
(min) (USP) (USP)

3,19 HALOPERIDOL 318,33 1,38 994 ---

RT Name Alpha S/N Noise

(min) (uV)

3,19 HALOPERIDOL --- 504,82 808,00

Asymmetry warning outside the range of: 0,800 to 2,000

No. of theoretical plates warning at less than: 500
Resolution warning at less than: 2,000
Signal to noise ratio warning at less than: 3
Developed by: ANGELA GARCIA Analizado por: ISMAEL MAYORGA

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D-7000 HSM: ENERO 2020 Series: 0030 System: OFFLINE

LABORATORIO FARBROQUIM S.A.S

Analyzed Date and Time: 18/01/20 17:32
Processing Method: HALOPERIDOL ENE/18/20
System(acquisition): HPLC MP-07 Vial Type: STD1
Sample Name: ESTANDAR Volume: 20,0 ul
Sample Description:
500 N-Meth 0
Inhib Inhib
Sens 5

3,12, HALOPERIDOL
400
Intensity (mV)

300

200

100

0 1 2 3 4 5 6 7 8
Retention Time (min)

No. RT Name Area BC

1 3,12 HALOPERIDOL 3162110 BB

3162110

Peak rejection level: 0

RT Name k' Asym N Res
(min) (USP) (USP)

3,12 HALOPERIDOL 310,67 1,36 1050 ---

RT Name Alpha S/N Noise

(min) (uV)

3,12 HALOPERIDOL --- 522,93 808,00

Asymmetry warning outside the range of: 0,800 to 2,000

No. of theoretical plates warning at less than: 500
Resolution warning at less than: 2,000
Signal to noise ratio warning at less than: 3
Developed by: ANGELA GARCIA Analizado por: ISMAEL MAYORGA

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D-7000 HSM: ENERO 2020 Series: 0030 System: OFFLINE

LABORATORIO FARBROQUIM S.A.S

Analyzed Date and Time: 18/01/20 17:41
Processing Method: HALOPERIDOL ENE/18/20
System(acquisition): HPLC MP-07 Vial Type: STD1
Sample Name: ESTANDAR Volume: 20,0 ul
Sample Description:
500 N-Meth 0
Inhib Inhib
Sens 5

3,18, HALOPERIDOL
400
Intensity (mV)

300

200

100

0 1 2 3 4 5 6 7 8
Retention Time (min)

No. RT Name Area BC

1 3,18 HALOPERIDOL 3192866 BB

3192866

Peak rejection level: 0

RT Name k' Asym N Res
(min) (USP) (USP)

3,18 HALOPERIDOL 317,00 1,38 990 ---

RT Name Alpha S/N Noise

(min) (uV)

3,18 HALOPERIDOL --- 505,15 808,00

Asymmetry warning outside the range of: 0,800 to 2,000

No. of theoretical plates warning at less than: 500
Resolution warning at less than: 2,000
Signal to noise ratio warning at less than: 3
Developed by: ANGELA GARCIA Analizado por: ISMAEL MAYORGA

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D-7000 HSM: ENERO 2020 Series: 0030 System: OFFLINE

LABORATORIO FARBROQUIM S.A.S

Analyzed Date and Time: 18/01/20 17:50
Processing Method: HALOPERIDOL ENE/18/20
System(acquisition): HPLC MP-07 Vial Type: STD1
Sample Name: ESTANDAR Volume: 20,0 ul
Sample Description:
500 N-Meth 0
Inhib Inhib
Sens 5

3,12, HALOPERIDOL
400
Intensity (mV)

300

200

100

0 1 2 3 4 5 6 7 8
Retention Time (min)

No. RT Name Area BC

1 3,12 HALOPERIDOL 3140292 BB

3140292

Peak rejection level: 0

RT Name k' Asym N Res
(min) (USP) (USP)

3,12 HALOPERIDOL 310,67 1,37 1038 ---

RT Name Alpha S/N Noise

(min) (uV)

3,12 HALOPERIDOL --- 516,56 808,00

Asymmetry warning outside the range of: 0,800 to 2,000

No. of theoretical plates warning at less than: 500
Resolution warning at less than: 2,000
Signal to noise ratio warning at less than: 3
Developed by: ANGELA GARCIA Analizado por: ISMAEL MAYORGA

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