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  • Hidrosin Plus Pleg X 12 STCK Lote 19258 FBQ122-PT0119 005

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    Brendapaez3
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    This document contains 3 chromatograms from an analysis of alginate of sodium using HPLC. The first chromatogram shows a blank sample. The second shows a diluent sample. The third shows a standard sample with a peak at 3.33 minutes for alginate of sodium. However, the analysis results for the standard sample again failed to meet criteria for symmetry, number of theoretical plates, resolution and signal to noise ratio.

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    HIDROSIN PLUS PLEG X 12 STCK LOTE 19258 FBQ122-PT0119 005

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    This document contains 3 chromatograms from an analysis of alginate of sodium using HPLC. The first chromatogram shows a blank sample. The second shows a diluent sample. The third shows a standard sample with a peak at 3.33 minutes for alginate of sodium. However, the analysis results for the standard sample again failed to meet criteria for symmetry, number of theoretical plates, resolution and signal to noise ratio.

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    © All Rights Reserved
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    7 views20 pages

    Hidrosin Plus Pleg X 12 STCK Lote 19258 FBQ122-PT0119 005

    Uploaded by

    Brendapaez3
    This document contains 3 chromatograms from an analysis of alginate of sodium using HPLC. The first chromatogram shows a blank sample. The second shows a diluent sample. The third shows a standard sample with a peak at 3.33 minutes for alginate of sodium. However, the analysis results for the standard sample again failed to meet criteria for symmetry, number of theoretical plates, resolution and signal to noise ratio.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 20

    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 12:38


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: BLANK
    Sample Name: FASE MOVIL Volume: 25.0 ul
    Sample Description:

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15

    0.10
    Absorbance (AU)

    0.05

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA

    Page Indicator 1 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 13:20


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: BLANK
    Sample Name: DILUENTE Volume: 25.0 ul
    Sample Description:

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15

    0.10
    Absorbance (AU)

    0.05

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA

    Page Indicator 2 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 14:01


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: STD1
    Sample Name: ESTANDAR SST Volume: 25.0 ul
    Sample Description:

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15
    3.31, ALGINATO DE SODIO
    0.10
    Absorbance (AU)

    0.05

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA


    No. RT Name Area BC

    1 3.31 ALGINATO DE SODIO 1674262 BV

    1674262

    Peak rejection level: 0


    RT Name k' Asym N Res
    (min) (USP) (USP)

    3.31 ALGINATO DE SODIO 329.67 1.45 593 ---

    RT Name Alpha S/N Noise


    (min) (uV)

    3.31 ALGINATO DE SODIO --- 0.91* 157641.67

    WARNING: Criterion for S/N Ratio not satisfied.


    Asymmetry warning outside the range of: 0.800 to 2.000
    No. of theoretical plates warning at less than: 500
    Resolution warning at less than: 2.000

    Page Indicator 3 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2
    Signal to noise ratio warning at less than: 3

    Page Indicator 4 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 15:23


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: STD1
    Sample Name: ESTANDAR Volume: 25.0 ul
    Sample Description:

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15
    3.33, ALGINATO DE SODIO
    0.10
    Absorbance (AU)

    0.05

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA


    No. RT Name Area BC

    1 3.33 ALGINATO DE SODIO 1647030 BB

    1647030

    Peak rejection level: 0


    RT Name k' Asym N Res
    (min) (USP) (USP)

    3.33 ALGINATO DE SODIO 332.33 1.28 587 ---

    RT Name Alpha S/N Noise


    (min) (uV)

    3.33 ALGINATO DE SODIO --- 0.89* 157641.67

    WARNING: Criterion for S/N Ratio not satisfied.


    Asymmetry warning outside the range of: 0.800 to 2.000
    No. of theoretical plates warning at less than: 500
    Resolution warning at less than: 2.000

    Page Indicator 5 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2
    Signal to noise ratio warning at less than: 3

    Page Indicator 6 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 16:04


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: STD1
    Sample Name: ESTANDAR Volume: 25.0 ul
    Sample Description:

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15
    3.33, ALGINATO DE SODIO
    0.10
    Absorbance (AU)

    0.05

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA


    No. RT Name Area BC

    1 3.33 ALGINATO DE SODIO 1649837 BV

    1649837

    Peak rejection level: 0


    RT Name k' Asym N Res
    (min) (USP) (USP)

    3.33 ALGINATO DE SODIO 332.33 1.33 558 ---

    RT Name Alpha S/N Noise


    (min) (uV)

    3.33 ALGINATO DE SODIO --- 0.87* 157641.67

    WARNING: Criterion for S/N Ratio not satisfied.


    Asymmetry warning outside the range of: 0.800 to 2.000
    No. of theoretical plates warning at less than: 500
    Resolution warning at less than: 2.000

    Page Indicator 7 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2
    Signal to noise ratio warning at less than: 3

    Page Indicator 8 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 16:46


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: STD1
    Sample Name: ESTANDAR Volume: 25.0 ul
    Sample Description:

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15
    3.33, ALGINATO DE SODIO
    0.10
    Absorbance (AU)

    0.05

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA


    No. RT Name Area BC

    1 3.33 ALGINATO DE SODIO 1659144 BV

    1659144

    Peak rejection level: 0


    RT Name k' Asym N Res
    (min) (USP) (USP)

    3.33 ALGINATO DE SODIO 332.33 1.32 532 ---

    RT Name Alpha S/N Noise


    (min) (uV)

    3.33 ALGINATO DE SODIO --- 0.87* 157641.67

    WARNING: Criterion for S/N Ratio not satisfied.


    Asymmetry warning outside the range of: 0.800 to 2.000
    No. of theoretical plates warning at less than: 500
    Resolution warning at less than: 2.000

    Page Indicator 9 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2
    Signal to noise ratio warning at less than: 3

    Page Indicator 10 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 17:27


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: STD1
    Sample Name: ESTANDAR Volume: 25.0 ul
    Sample Description:

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15
    3.33, ALGINATO DE SODIO
    0.10
    Absorbance (AU)

    0.05

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA


    No. RT Name Area BC

    1 3.33 ALGINATO DE SODIO 1679006 BV

    1679006

    Peak rejection level: 0


    RT Name k' Asym N Res
    (min) (USP) (USP)

    3.33 ALGINATO DE SODIO 332.33 1.36 515 ---

    RT Name Alpha S/N Noise


    (min) (uV)

    3.33 ALGINATO DE SODIO --- 0.86* 157641.67

    WARNING: Criterion for S/N Ratio not satisfied.


    Asymmetry warning outside the range of: 0.800 to 2.000
    No. of theoretical plates warning at less than: 500
    Resolution warning at less than: 2.000

    Page Indicator 11 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2
    Signal to noise ratio warning at less than: 3

    Page Indicator 12 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 18:08


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: STD1
    Sample Name: ESTANDAR Volume: 25.0 ul
    Sample Description:

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15
    3.33, ALGINATO DE SODIO
    0.10
    Absorbance (AU)

    0.05

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA


    No. RT Name Area BC

    1 3.33 ALGINATO DE SODIO 1731512 BB

    1731512

    Peak rejection level: 0


    RT Name k' Asym N Res
    (min) (USP) (USP)

    3.33 ALGINATO DE SODIO 332.33 1.42 485* ---

    RT Name Alpha S/N Noise


    (min) (uV)

    3.33 ALGINATO DE SODIO --- 0.85* 157641.67

    WARNING: Criterion for No. of Theoretical Plates not satisfied.


    WARNING: Criterion for S/N Ratio not satisfied.
    Asymmetry warning outside the range of: 0.800 to 2.000
    No. of theoretical plates warning at less than: 500

    Page Indicator 13 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2
    Resolution warning at less than: 2.000
    Signal to noise ratio warning at less than: 3

    Page Indicator 14 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 18:49


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: UNK
    Sample Name: MT1 LOTE 19258 Volume: 25.0 ul
    Sample Description: HIDROZINCPLUS

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15

    0.10
    Absorbance (AU)

    0.05
    3.36, ALGINATO DE SODIO

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA


    No. RT Name Area BC

    1 3.36 ALGINATO DE SODIO 616514 BB

    616514

    Peak rejection level: 0


    RT Name k' Asym N Res
    (min) (USP) (USP)

    3.36 ALGINATO DE SODIO 335.00 1.67 383* ---

    RT Name Alpha S/N Noise


    (min) (uV)

    3.36 ALGINATO DE SODIO --- 0.27* 157641.67

    WARNING: Criterion for No. of Theoretical Plates not satisfied.


    WARNING: Criterion for S/N Ratio not satisfied.
    Asymmetry warning outside the range of: 0.800 to 2.000
    No. of theoretical plates warning at less than: 500

    Page Indicator 15 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2
    Resolution warning at less than: 2.000
    Signal to noise ratio warning at less than: 3

    Page Indicator 16 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 19:30


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: UNK
    Sample Name: MT2 LOTE 19258 Volume: 25.0 ul
    Sample Description: HIDROZINCPLUS

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15

    0.10
    Absorbance (AU)

    0.05
    3.39, ALGINATO DE SODIO

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA


    No. RT Name Area BC

    1 3.39 ALGINATO DE SODIO 640183 BV

    640183

    Peak rejection level: 0


    RT Name k' Asym N Res
    (min) (USP) (USP)

    3.39 ALGINATO DE SODIO 337.67 --- 364* ---

    RT Name Alpha S/N Noise


    (min) (uV)

    3.39 ALGINATO DE SODIO --- 0.28* 157641.67

    WARNING: Criterion for No. of Theoretical Plates not satisfied.


    WARNING: Criterion for S/N Ratio not satisfied.
    Asymmetry warning outside the range of: 0.800 to 2.000
    No. of theoretical plates warning at less than: 500

    Page Indicator 17 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2
    Resolution warning at less than: 2.000
    Signal to noise ratio warning at less than: 3

    Page Indicator 18 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2

    LABORATORIO FARBROQUIM S.A.S

    Analyzed Date and Time: 05/01/19 20:12


    Processing Method: ALGINATO DE SODIO ENE/05/19
    System(acquisition): HPLC MP-13 Vial Type: UNK
    Sample Name: MT3 LOTE 19258 Volume: 25.0 ul
    Sample Description: HIDROZINCPLUS

    N-Meth 0
    Inhib Inhib
    0.15 Sens 15

    0.10
    Absorbance (AU)

    0.05
    3.36, ALGINATO DE SODIO

    0.00

    -0.05

    -0.10

    -0.15

    -0.20

    0 1 2 3 4 5 6 7 8 9 10 11
    Retention Time (min)

    Developed by: ANGELA GARCIA Analizo: SOFÍA CORREA


    No. RT Name Area BC

    1 3.36 ALGINATO DE SODIO 707474 BV

    707474

    Peak rejection level: 0


    RT Name k' Asym N Res
    (min) (USP) (USP)

    3.36 ALGINATO DE SODIO 335.00 1.83 373* ---

    RT Name Alpha S/N Noise


    (min) (uV)

    3.36 ALGINATO DE SODIO --- 0.31* 157641.67

    WARNING: Criterion for No. of Theoretical Plates not satisfied.


    WARNING: Criterion for S/N Ratio not satisfied.
    Asymmetry warning outside the range of: 0.800 to 2.000
    No. of theoretical plates warning at less than: 500

    Page Indicator 19 / 20
    D-7000 HSM: ENERO 2019 Series: 0007 System: Sys 2
    Resolution warning at less than: 2.000
    Signal to noise ratio warning at less than: 3

    Page Indicator 20 / 20

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