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Exfraction (saS/s2L)
Mass Tresf
Ne Sepa fa fien Precess es oam Sep
Zone melting
te
Sep ete
Cryegenic Sep",
Mem brane Sep Ce X
Drying
Drying Siilar te evape raien bd t diff.is ihe
exTent o bent Cguudl toved
Th puupeke oevapora Tion 1s To ihcrease The oueh
He Subs Tan ce whureas dryivng asTu
purpose
Fuuovig the mecisTure ( crfonl poi
guila)
Bew ddry s h one witl o oigTsure
E y lbrabe v Ra goveraing
Basul on uubh un Baseo ch he ral
tronsferob 1 sptcies
Tootgh esia ant malenal
2hd
adoltie o phase
a Sep by a
Strea
Fecd
AdAcd STrea 2
pha
S p bg Lig a
batrer
Feed Strea
boirer
Steam 2
act ihort Catrier
Olure dutivq solid partieles hal as
Fead
Feecd
bate preus
advevbrut
(traps strea 1)
li nlir. ey
as
selid salt c t o t
Crystall se t
tach otar.
beth alnost epposil ef
Ipertat Tems AC c- c*
Degee eSpertatirnbe
h e C- sel"
cone o Saunlio
eguile one
Ths is qpuvalut Te
the drVTL
forte fer Cnystallisatie
force
Always tiyber Rale Driviug
Resistanee
Hes e hydrmli
Mas e aukylrat R
Mact eb selvent
Sel Couch Haus o Selveut
Mats e Salt
OR
Maus o 9eliutien
H fact
tot tiug
valuu given fecs
ou
Whil wig tu
Saie tu
wu coarry t
Supertafuraliey Ratio ()
Relat Superatirat.cu (y) sc
S 2.4
2 O4
Tki C 24 k so 34 leg s
3.4S
2 u 3.04
3.45 2-b
06
- Crahl Yeld
Bad Haterial balauce Co frSfed)
luput+Geuaatieu = Dlhut + acciydlatieyt eonsuplien
we, ,iwtal
wrtee, wes of sclvetin cel7 Liguor.
W fiual nas Se lvet 1 lapor.
y icld ot erystals
R Ratie mel. t ohyiali t. nel. iut ot anlydrs
Salt
t nas eb
E Ratie c a s oselv. vepetatad
Selv. e te iitial sol
O.126 2
RU GD7
T-GG(R-1)
eAsded (Grtitalernd
C 41 by T balan o rosleod
C
w, SIo k H,C
Per 1000 k So/
Iitial 40 k selutin lo00 ka
SIo selvent
lSSS?se1 H o
S
1o0
a18.92
So lute 408.12 k l
Dif.
Dif italfi
21-08 k
inibal 490
- wWoys fo obtauuSupersatuation
Fo Evaperalion
- ooliua
-Evaporelion k cooliug both (adickote 2unp)
peipitatiom by odding ouother subsfance
Salbing
hse ls
Also chpsfallses CO be elhuufied along
22 Loke i industrial tystallso
- Fruze Cystallsaticy
iustead ob thu solet
.tstls s e l r u t gst ferued,
.Depeuding on te proces Hu Selvent Crys tals n a beft inal
produce ot tu oncantrattd nution alse be final proks
Bot cau le the producs.
'Prodcek CoHc iapLor
Soleut separmtid ( ltd)
ucle mng
tlure s an ksue, as fena
lotres ckyslals fern
But the uat trahsfer.
shck to alls asnd terioral
"Seraped Suacehaat
Tucs, to vercoe
blacey wsi ch scrape o t any eryslals
rcheger, lue are
along tl
Loall. T Llaoles are no
vt
Hha sCick t. t
r tiub.
involved. l nart
so
a
are
e
inmiscible ebr9erunb
In , int
to enue easy sepotaion.
tht o Rx" occu & inumiscib
e
Seawir + n-butane desalinati on)
Look hore into his
Freeze Grindung
Tis ic invelved ih size rductou ob plastes, Frbbr, trax
nl freatid textis.
te duform etur ttan
tkan break
T tu tduty o such matiriaL is
ahotmal femperlres
On freezing, cralal lattice shrnks
wwchos copic Cracks levelop
Crack Propoqaluo
tnystals of
ice
1E is a Chyogenic uthod Separntie
Teupehab iqvelved o'c
- Foam
Separation (-Alsle Sep
Eadserpt re bullle eparticn,ts aderblk
crdar t create bbblas r t adol Sfaclauls or pass a ga,
foam
a
Lallan struete tere a no. ot buldols an o u clo
Coas chiol
tunIh Seu jctie, 7 auella s very fun ttuu juncion
Ttce ad ajehily ot Liguid flocr oCceus hurt
hirt
Cg qolad)
Surteretat
Cprekmbay M) t
Sep at tha Ptrue ey Sep t
Aclrantage o fedum seP odiffxuct. kis u be cawst
very hih at lo cHc
e Sturace actr o t Cost funti.
dupends
Coaidered.
Wandr fors
Walls a
1ue.
- Suclion prsue ol
alo bê uelorel wig aienc /atpic
Sou latnic rus o
Sutachanbs).
.Fer feaun breaseng e a-feam.
We haUe tu toducthnty deuring prees.Wheen Hre 6 a
Sizeabe olffereuce e siply Sepamt H fean ad Ten
ur-Tur precess
Foam stabibtyu nd a slalle
abeut s-epatatim .
foaun before ca Tteik
facters chnical hatue & CouC ob eotupohsns
ecraunie Substances gve stable fhnm)
upernlut of opereilicn.fwt iuCRas t
Teup. en feaun breakiq uTIoccur.
Bubb& Size A biggar laalla Can break tajkr
Pe 73 S3 bar
is l tu supcrcitcal
te Solrent tat toe use
In this ptrocess
pha. Seliolhermal
esd to do furtiur
extracton ( seporat
SLE & LUE, ue
i6.
t Selvent Hat odselos
precess tget
pure Specte fro
ii i
at kigh presure
4 t Supercritenl selvent, like Co it fanms lo a
eduu th preisiure
Luix phase btutif we
e Hessure.
by urely ohanging Colna br.t
f Coues changes aletg e
.
f we
cousider diei llatien,
it s ixed tt fus
hot get ahy pe Specie,
te do the pure speeie by Siply
Le Can get
Bat,iSCFS/sc FE
aApulating the phessur
C192 Pfena
Zone Melting. liguid zo
Sebiol ILLILI
Teelid
Zone Healur
anel toe
qet a purlg lovel ot
I f tue do 4-passes epectadly
im 1D pturilias prLeu.
Huismuhod fe prasolute
Cehuauiau 6hugk pcunlg
Pfaun td
have differeut charnchrst
Sep ik bettr if selid liquid phass
Ts glaus (hih i sapertecud Ligpid) leh '
eg e Tny o
tdcew t Cwom.
guiel phue.
Zons slting
Zohs invelres a fonaly ot Teclnigpus thal has dueloped
DRt cfOhu phart thraek anotur
t Coutept 6 koviy
ain Targal i puriicalion .
2o hug
ug& spacing
Stiting in 2one
pese
is nermally enotugh)
Ne. 2ons passes
(S-6 2ou
sholole
Fsr max. puriicalion sheld e nored sloty, anple
sthined and
unghs ong, ult stould be
ore zonl
ma
should be hmade Com tainersbe borosilicali
Can qans,
yes
fazed silta gradey lut1
htfals/pelyprs er
A m a cohe oupanilg
Ccne
MultcomponenT Distllation
Distllati it a sep precess bas«d cn velatitl oitference.
Ve laicty fCip- pres i s Synbelblhtlfy
Relain elatl i t y = (if a e , tn ho 3eparation Tako phce
tonduser
Conlmiors dust. couumn
11
Can thus achiee
reux
vap stream asfeady state
Fexd
Cli)
Dest.
oun reboilur
Reide botou)
Raoults Low
Dalton's Laus PAaP
Tetal
A
. T solue matkan.ahally
LWe CQn wn& Mass balance eg
overall was elahee
r ersy plalz /frny otent mas balan
For vty topo nut|als ane e
e Ca unt Bury belanc
bvenll euthalpy blanct
end t be
Ne subscript es itk
T couponint
iuho o h o r t Velnth
is of
T u dictanc cur from 4 Lie a hostrt
Felatir velalGty
b e l l separnlie
fh Curvt is farur hun is higher
If belt sparakaau Syuten, I)
ie, Syste
Bruary &Maltcomponint Sys fe
A*B. Ou ti be h o r e
la Binarg SysTem, Tro Conpehun
Itspectv et whel part of colus t e
velati than ottar olali k
cOLvHder the orn velatu compohtrt is huore
tuugbheu
ele Buulkcampen Coupohsnt caubeadjasid te le
t
Kault's B& Daltes
Uing dotan'C give perfect
Sat
k data oleny
P tetrd
Condunsaticn
DistUaten E Reptald boiling
Bubble poit
D e r poi
Ne N
k Xi compevn
GGives B. PE
pfatl 2 atm
Autetu Crut B
2617.SS -49.78
uxas Is 8366
- S%. SI
29/.32
h-huplan I3737
IS-1426 3/20.21 -l3.43
h-oclaw
P B
A- THC
m g
haut 7-46
174S.174S.
put
2 2
216 af
eptan 6.616 4
747.27 g7 o.1932
oclas
79
3 27.348 o.4307
R 114
p 819
K 0 3S 1.86S
0.717C
h 0424 03473
h . O14
For iterahen olt uuo 7C
hor22377 hup ,7 47
Papt 0.417 a
.For tu De poiut Cale
(lstally fead i veprur phast)
N. Ne
L k
1
ha 9547
P. 0.4167 T
.96S
=0.7AS
D.3473
-Dist lation Coluwn Deaigh
We fint uud t. keifhe hd prdleuet,