International University, Vietnam National University - HCMC 1

CHEMISTRY LABORATORY

REPORT
EXPERIMENT 1: CHEMICAL REACTIONS

Group: ______________ Section: _____1_________ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1
2
3
4
5

Total score: _______/15__

Present well: + 1 point

Clear picture: + 1 point

Total = 15 points

The report must be typed and handed in together with the signed data sheet by the deadline
 International University, Vietnam National University - HCMC 2
CHEMISTRY LABORATORY

I. Introduction (1pt)
(Introduce what experiments you do in this report)

II. Experimental (1pt)

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. Reactions of Cu2+ (1 pt)

Reaction Observation Chemical Equation

0.5M CuSO4 (0.25 pts)

+ 2M NaOH

0.5M CuSO4 (0.25 pts)

+ 2M NH4OH

Comments: (0.5 pts)

2. Reactions of silver halides (2 pts)

Reaction Observation Chemical Equation

0.5M KCl (0.25 pts)

+ 0.1M AgNO3

0.5M KCl (0.25 pts)

+ 0.1M AgNO3

+ 2M NH4OH
0.5M KBr (0.25 pts)

+ 0.1M AgNO3

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0.5M KBr (0.25 pts)

+ 0.1M AgNO3

+ 2M NH4OH
0.5M KI (0.25 pts)

+ 0.1M AgNO3

0.5M KI (0.25 pts)

+ 0.1M AgNO3

+ 2M NH4OH
Comments: (0.5 pts)

3. Reactions of H2O2 (1 pt)

Reaction Observation Chemical Equation

0.1M KMnO4 (0.25 pts)

+ 2M H2SO4

+ H2O2
0.1M KI (0.25 pts)

+ 2M H2SO4

+ H2O2
H2O2 (0.25 pts)

+ MnO2

Comments: (0.25 pts)

4. Reactions of Nitrate (1 pt)

Reaction Observation Chemical Equation

1M NaNO3 (0.25 pts)

+ FeSO4

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+ concentrated H2SO4
1M NaNO2 (0.25 pts)

+ FeSO4

+ concentrated H2SO4
1M NaNO3 (0.25 pts)

+ FeSO4

+ concentrated

CH3COOH
Comments: (0.25 pts)

5. Reactions of KMnO4 (1 pt)

Reaction Observation Chemical Equation

0.5M Na2SO3 (0.25 pts)

+ 2M H2SO4

+ 0.1M KMnO4
0.5M Na2SO3 (0.25 pts)

+ 6N NaOH

+ 0.1M KMnO4
0.5M Na2SO3 (0.25 pts)

+ H2O

+ 0.1M KMnO4
Comments: (0.25 pts)

6. Reaction of Potassium Dichromate (K2Cr2O7) (0.5 pts)

Reaction Observation Chemical Equation

2M K2Cr2O7 (0.25 pts)

+ 6M H2SO4

+ C2H5OH
Comments: (0.25 pts)

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7. A. Reactions of Fe3+ (0.75 pts)

Reaction Observation Chemical Equation

0.5M FeCl3 (0.25 pts)

+ 2M KOH

0.5M FeCl3 (0.25 pts)

+ 2M NH4OH

Comments: (0.25 pts)

7. B. Reactions of Fe2+ (0.75 pts)

Reaction Observation Chemical Equation

0.5M FeSO4 (0.25 pts)
+ 2M KOH

0.5M FeSO4 (0.25 pts)

+ 2M NH4OH

Comments: (0.25 pts)

8. Reactions of Al3+ (1 pt)

Reaction Observation Chemical Equation

0.5M Al2(SO4)3 (0.25 pts)

+ 2M NaOH

0.5M Al2(SO4)3 (0.25 pts)

+ 2N NaOH

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CHEMISTRY LABORATORY

+ 2M HCl
0.5M Al2(SO4)3 (0.25 pts)

+ 2M NaOH

+ 2M NaOH
Comments: (0.25 pts)

9. Flame test (1 pt)

Solution Dominant flame Wavelength Frequency Photon energy

color (nm) (s1) (J)
LiCl
NaCl
KCl
CaCl2
BaCl2
Note: 0.15 pts for the calculation of each chemical

Comments: (0.25 pts)

IV. Conclusions (1 pt)

(conclude all your performance in this report)

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 International University, Vietnam National University - HCMC 7
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 2: pH AND BUFFERS

Group: _____________ Section: _______2_______ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1
2
3
4
5

Total score: ________/15__

Present well: + 1 point

Clear picture: + 1 point

Total = 15 points

The report must be typed and handed in together with the signed data sheet by the deadline
 International University, Vietnam National University - HCMC 8
CHEMISTRY LABORATORY

I. Introduction (1 pt)
(Introduce what experiments you do in this report)

II. Experimental (1 pt)

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. pH OF DEIONIZED WATER (2.5 pts)

Observed pH
Time
Explanation
(second) 1st 2nd
(Group___) (Group___)
0 (2 pts)
20
40
60
80
100
120
140
160

Comments: (0.5 pts)

2. pH OF STRONG ACID (1.5 pts)

Measured pH
Theoretical
Solution Comments/ Explanation
pH 1st 2nd
(Group___) (Group____)
(1 pt)
10 mL of 0.1M HCl

Add 90 mL of distilled
water

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CHEMISTRY LABORATORY

Add 10 mL of
0.1M NaOH

Add 90 mL of
0.01M NaOH
Comments: (0.5 pts)

3. pH OF WEAK ACID (1.5 pts)

Measured pH
Solution 1st 2nd Ka Comments/ Explanation
(Group___) (Group____)
(1 pt)
0.1M acetic acid

0.01M acetic acid

0.001M acetic acid

Comments: (0.5 pts)

4. pH OF SALTS (1.5 pts)

Measured pH Explanation
Predicted
Solution 1 st
2nd
pH
(Group____) (Group____)
(1 pt)
0.1M NaCl

0.1M CH3COONa

0.1M NH4Cl

Comments: (0.5 pts)

5. pH OF BUFFERS (3 pts)

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CHEMISTRY LABORATORY

Volume (mL) Volume (mL) Measured pH

Calculated
Buffer 0.1M 0.1M Acid Base
pH 1st 2nd
CH3COOH CH3COONa
(Group__) (Group__)

A 10.0 40.0

B 40.0 10.0

C 25.0 25.0
Calculation pH: (0.5 pts)
Comments: (0.5 pts)

 Part I: Addition of 10 drops 0.1 M HCl

pH after Total volume HCl (drops)

pH from the
Buffer adding 10 to change pH by one unit Comments/ Explanation
start, pHo
drops HCl (pHo-1)

A (0.5 pts)

C
Comments: (0.5 pts)

`
 Part II: Addition of 10 drops 0.1 M NaOH

pH after Total volume NaOH

pH from the
Buffer adding 10 (drops) to change pH by Comments/ Explanation
start, pHo
drops NaOH one unit (pHo+1)

(0.5 pts)
A

C
Comments: (0.5 pts)

IV. Conclusions (1 pt)

(conclude all your performance in this report)

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 International University, Vietnam National University - HCMC 11
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 3: REDOX TITRATION

Group: _____________ Section: ______3________ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1
2
3
4
5

Total score:________/15__

Present well: + 1 point

Well reading buret (accuracy) + Clear picture: + 2 points

Total = 15 points

The report must be typed and handed in together with the signed data sheet by the deadline
 International University, Vietnam National University - HCMC 12
CHEMISTRY LABORATORY

I. Introduction (1 pt)
(Introduce what experiments you do in this report)

II. Experimental (1 pt)

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. TITRATION OF KMnO4 SOLUTION WITH STANDARD H2C2O4 SOLUTION (3 pts)

Calculation: (1.5 pts)

Normality of the standard H2C2O4 solution, N(H2C2O4) = ___________________

Volume of the standard H2C2O4 solution used, V(H2C2O4) = ___________________

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of KMnO4 (N)

1 -

2 -

Average Normality of KMnO4 = ____________ ( )

Comment: (1.5 pts)

2. TITRATION OF UNKNOWN CONCENTRATION H2C2O4 SOLUTION WITH STANDARD

KMnO4 SOLUTION (3 pts)

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Calculation: (1.5 pts)

Normality of the standard KMnO4 solution, N(KMnO4) = ___________________

Volume of the unknown H2C2O4 solution used, V(H2C2O4) = ___________________

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of H2C2O4 (N)

1 -

2 -

Average Normality of H2C2O4 =_______ ( )

Comment: (1.5 pts)

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CHEMISTRY LABORATORY

3. TITRATION OF UNKNOWN CONCENTRATION FeSO4 SOLUTION WITH STANDARD

KMnO4 SOLUTION (3 pts)

Calculation: (1.5 pts)

Normality of the standard KMnO4 solution, N(KMnO4) =___________________

Volume of the unknown FeSO4 solution used, V(FeSO4)= ___________________

Trial # Burette reading(mL) Volume of KMnO4 (mL) Normality of FeSO4(N)

1 -

2 -

Average Normality of FeSO4 =_______ ( )

Comment: (1.5 pts)

IV. Conclusions (1 pt)

(conclude all your performance in this report)

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 International University, Vietnam National University - HCMC 15
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 4: CHEMICAL EQUILIBRIUM

Group: _____________ Section: ______4________ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1
2
3
4
5

Total score: ________/15__

Present well: + 1 point

Clear picture: + 1 point

Total = 15 points

I. Introduction (1 pt)
(Introduce what experiments you do in this report)

The report must be typed and handed in together with the signed data sheet by the deadline
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CHEMISTRY LABORATORY

II. Experimental (1 pt)

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. ACID/BASE EQUILIBRIA (2 pts)

Equilibrium System: 2CrO42 + 2H+(aq)  Cr2O72 + H2O(l)

Description of Predicted Observation Explanation

conditions outcome

(0.5 pts)

Initial solution

(0.5 pts)

+ Conc. HCl

(0.5 pts)

+ 6 N NaOH

Comment: (0.5 pts)

2. EQUILIBRIA OF ACID/BASE INDICATORS (2 pts)

Equilibrium System: H(MV)(aq) + H2O(l)  H3O+(aq) + MV(aq)

Addition Predicted Observation Explanation

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CHEMISTRY LABORATORY

outcome

(0.375 pts)

None (control)

(0.375 pts)

6 M HCl

(0.375 pts)

6 M NaOH

(0.375 pts)

6 M HCl

Comment: (0.5 pts)

3. COMPLEX ION FORMATION (2 pts)

Equilibrium System:Fe3+ + SCN [Fe(SCN)]2+

Addition Predicted Observation Explanation

outcome

None (0.25 pts)

(control)

(0.25 pts)
0.01M FeCl3

(0.25 pts)
6M NaOH

(0.25 pts)

Cold

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CHEMISTRY LABORATORY

(0.25 pts)
Hot

(0.25 pts)

0.1M AgNO3

Comment: (0.5 pts)

4. EQUILIBRIA OF PRECIPITATION REACTIONS (2 pts)

Equilibrium System:Ca2+(aq) + C2O42(aq)  CaC2O4(s)

Predicted
Addition Observation Explanation
outcome

Test tube 1: (0.375 pts)

0.1 M Na2C2O4

Test tube 2: (0.375 pts)

+ 0.1 M H2C2O4

Test tube 2: (0.375 pts)

+ 6 M HCl

Test tube 2: (0.375 pts)

+ 6 M NH4OH

Comment: (0.5 pts)

5. TEMPERATURE EFFECTS ON EQUILIBRIA (2 pts)

Equilibrium System:Co(H2O)6 2+(aq) + 4Cl(aq)  CoCl4 2(aq) + 6H2O(l)

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Description of Predicted
Observation Explanation
conditions outcome

Nothing changed (0.5 pts)

(control)

(0.5 pts)

Hot water bath

(0.5 pts)

Ice-water bath

Comment: (0.5 pts)

IV. Conclusions (1 pt)

(conclude all your performance in this report)

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 International University, Vietnam National University - HCMC 20
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 5: FACTORS AFFECTING
REACTION RATE

Group: _____________ Section: ______5________ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1
2
3
4
5

Total score: ________/15__

Present well: + 1 point

Clear picture: + 1 point

Total = 15 points

The report must be typed and handed in together with the signed data sheet by the deadline
 International University, Vietnam National University - HCMC 21
CHEMISTRY LABORATORY

I. Introduction (1 pt)
(Introduce what experiments you do in this report)

II. Experimental (1 pt)

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. EFFECT OF CONCENTRATION ON REACTION TIME (5 pts)

Reaction 1:

__________________________________________________

Reaction 2:

__________________________________________________

Calculate the initial concentrations of I- and S2O82- ions:

Mixture # 5:

(1 pt)

[I-] =

[S2O82-] =

Mixture Iodide ion Peroxydisulfate Time in seconds

1 0.08 0.04

2 0.068 0.04

3 0.056 0.04

4 0.044 0.04

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CHEMISTRY LABORATORY

5 0.032 0.04

6 0.02 0.04

Mixture Iodide ion Peroxydisulfate Time in seconds

7 0.08 0.034

8 0.08 0.028

9 0.08 0.022

10 0.08 0.016

11 0.08 0.01

Plotting the concentration of iodide ion versus time: [Note: X – axis: time; Y – axis:
concentrations].

- Mixtures # 1-6: Graph (1 pt)

The order of reaction with respect to iodide ion? (0.5 pts)

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CHEMISTRY LABORATORY

Comments: (0.5 pts)

- Mixtures # 1, 7, 8, 9, 10, and 11: Graph (1 pt)

The order of reaction with respect to peroxydisulfate ion? (0.5 pts)

Comments: (0.5 pts)

2. EFFECT OF TEMPERATURE ON THE REACTION RATE (2 pts)

Reaction System:

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CHEMISTRY LABORATORY

Description of Predicted Observation Reaction Explanation

conditions outcome time

(0.5 pts)

Room
temperature

(0.5 pts)

500C

900C (0.5 pts)

Comment: (1pt)

3. EFFECT OF A CATALYST ON THE REACTION RATE (3 pts)

Reaction System:

Trial Description of Predicted Observation Explanation

conditions outcome (Reaction rate)

1 + MnCl2 (0.25 pts)

2 + MnO2 (0.25 pts)

3 + NaCl (0.25 pts)

4 + CaCl2 (0.25 pts)

5 + Zn (0.25 pts)

6 + KNO3 (0.25 pts)

7 + Fe(NO3)3 (0.25 pts)

The order of catalyst activity: (0.5 pts)

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Comments: (0.75 pts)

IV. Conclusions (1 pt)

(conclude all your performance in this report)

The report must be typed and handed in together with the signed data sheet by the deadline