MANUAL OF WORKSITE OPERATIONS WI.

VOLUME 2 OF 12 - RECEIPT, STORAGE AND HANDLING

WORK INSTRUCTIONS (W.I.)

This section covers all the work instructions for worksite staff including operatives/operators,
drivers and contract workers, to carry out their work efficiently and without errors. Worksites are
allowed to make minor modifications (e.g. using colour code instead of word or colour code plus
word or providing translation to vernacular languages) to the instruction to further clarify the
work instruction. They need to put up only the relevant work Instruction at the work locations.

In all cases, they have to signify that the relevant work instructions have been duly authorised by
the Distribution Finance Manager as per this Manual.

ISSUE NO. 6 – MAY 2004

LATEST UPDATE: 1ST JULY 2005
MANUAL OF WORKSITE OPERATIONS WI.
VOLUME 2 OF 12 - RECEIPT, STORAGE AND HANDLING

WORK INSTRUCTIONS
CONTENTS

WORK INSTRUCTION W.I. NO.

Shore Tank Dipping & Product Density Sampling B.1

a) Tank Dipping & Tank Temperature
b) Product Density
Tank Release (After Discharge Before Ship Sails) B.2
Tanks Release Certificate - Main Product Only B.3
Hose Disconnection after Tanker Discharge B.4
Water Draining (Main Products) After Tanker Discharge B.5
Formula Shell Diesel Additive Decanting B.6
Warning - Formula Shell Diesel Additive - NEMO 7021 B.7
Warning - Formula Shell Super Unleaded, Super,
Regular/Unleaded 92 Additive - NEMO 9436 B.8
Additive Injection for Formula Shell Diesel B.9
Additive Injection for Formula Shell Super, Regular, ULG and U92 B.10
Calibration of Additive Injection System at Worksites with Avery Hardoll Meters B.11
Formula Shell NEMO 9436 Doping B.12
Doping Gasoil with Stadis 450 B.13
Subsidy Claim B.14

ISSUE NO. 6 – MAY 2004

LATEST UPDATE: 1ST JULY 2005
MANUAL OF WORKSITE OPERATIONS WI.
VOLUME 2 OF 12 - RECEIPT, STORAGE AND HANDLING

WI.B.1

WORK INSTRUCTION

SHORE TANK DIPPING & PRODUCT DENSITY SAMPLING

A) TANK DIPPING

1) DRAIN TANK UNTIL WATER FREE.

2) CLOSE AND LOCK ALL TANK VALVES.

3) RECORD IN DIP BOOK TANK BASE "ENRAF"/"WHESSOE" GAUGE READING

BY PRESSING TEST BUTTON 3 TIMES TO OBTAIN CONSISTENT READING.

4) WHERE "ENRAF" GAUGE IS USED: -

SWITCH "OFF" AND "ON" "ENRAF" GAUGE SWITCH LOCATED AT DIP HATCH
OF TANK TOP; OBTAIN CONSISTENT READING AND COMPARE IT WITH
TANK BASE "ENRAF" GAUGE READING. INFORM OPS SUPT. IF DIFFERENT.

5) APPLY WATER FINDING PASTE TO DIP WEIGHT AND ULLAGE PASTE TO DIP
TAPE (APPROXIMATE LEVEL OF PRODUCT INDICATED BY
"ENRAF"/"WHESSOE” READING).

6) TAKE DIP READINGS 2 OR MORE, UNTIL 2 CONSISTENT READINGS OF NO

MORE THAN + 2 MM DIFFERENCE IS OBTAINED. AVERAGE THE 2 READINGS
TO ETERMINE TANK'S PRODUCT AND WATER LEVELS. AFTER EACH
DIPPING, GRIP A PIECE OF CLOTH FIRMLY ON FRONT AND BACK OF DIP
TAPE THEN PULL DIP TAPE UP FROM TANK TO ALLOW PRODUCT STICKING
ON DIP TAPE TO FALL BACK INTO THE TANK THUS DRYING THE DIP TAPE.
WIND DIP TAPE BACK TO ATTACHMENT.

B) TANK TEMPERATURES

1) FOR OIL DEPTH < 1.8 METERS, TAKE ONE MIDDLE LEVEL TEMPERATURE.

FOR OIL DEPTH 1.8 - 3.6 METERS, TAKE UPPER AND LOWER LEVELS
TEMPERATURES.

FOR OIL DEPTH > 3.6 METERS, TAKE UPPER, MIDDLE AND LOWER LEVELS
TEMPERATURES.

ISSUE NO. 6 – MAY 2004

LATEST UPDATE: 1ST JULY 2005
MANUAL OF WORKSITE OPERATIONS WI.
VOLUME 2 OF 12 - RECEIPT, STORAGE AND HANDLING

WI.B1

WORK INSTRUCTION
SHORE TANK DIPPING & PRODUCT DENSITY SAMPLING - (CONT'D)

B) TANK TEMPERATURES (CONT'D)

UPPER LEVEL IS 1/6 OF OIL DEPTH, MIDDLE IS 1/2 OF OIL DEPTH. LOWER IS
5/6 OF OIL DEPTH FOR > 3.6 METERS, AND 3/4 OF OIL DEPTH FOR 1.8 - 3.6
METERS OIL DEPTH.

2) DROP SAMPLING CAN TO REQUIRED DEPTH OF PRODUCT AND IMMERSE

CAN FOR AT LEAST 1 MINUTE (FOR LFO 2 MINUTES) BEFORE TAKING
SAMPLE. TAKE SAMPLE, AND IMMEDIATELY READ AND RECORD THE
READINGS. AVERAGE THE READINGS TO OBTAIN THE AVERAGE TANK
TEMPERATURE.

C) SAMPLE FOR DENSITY

1) NO. OF SAMPLES (AND DENSITIES OF SAMPLES) DEPENDS ON OIL DEPTH

AS PER B (1).

2) RINSE SAMPLING CAN AND RECEIVING SAMPLE TIN THOROUGHLY WITH

THE PRODUCT TO BE SAMPLED. RINSING AGENT TO BE BROUGHT DOWN
AND POURED INTO SAMPLE DRUM.

3) LOWER SAMPLE CAN GENTLY TO REQUIRED LEVELS AND DRAW

SAMPLES. STOP CORK MUST PLUG THE CAN AND JERKED OPEN WHEN THE
REQUIRED PRODUCT LEVEL IS REACHED.

4) TAKE EQUAL PROPORTIONS (UPPER, MIDDLE AND LOWER) OF SAMPLE

AND TRANSFER THEM TO THE SAMPLE TIN.

5) BRING THE SAMPLE TIN BACK TO OFFICE (LAB) FOR DENSITY TESTING.

ISSUE NO. 6 – MAY 2004

LATEST UPDATE: 1ST JULY 2005
MANUAL OF WORKSITE OPERATIONS WI.
VOLUME 2 OF 12 - RECEIPT, STORAGE AND HANDLING

WI.B.2

WORK INSTRUCTION

TANK RELEASE
AFTER DISCHARGE BEFORE SHIP SAILS

1. DUTY SUPERVISOR TO FLIP AND LOCK NOTICE TO "SETTLING" UPON COMPLETION

OF TANKER DISCHARGE.

2. DUTY SUPERVISOR WITNESSES WATER DRAINING BY HANDYMEN.

3. DUTY SUPERVISOR WITNESSES DRAWING OF COMPOSITE SAMPLES.

4. DUTY SUPERVISOR CARRIES OUT DENSITY AND FLASH POINT TESTS (FOR CLASS
II/III PRODUCTS ONLY) FROM COMPOSITE SAMPLE AND COMPARES MEASURED
DENSITY WITH CALCULATED DENSITY AND THAT THE FLASH POINT IS ABOVE
THE MINIMUM OF THE PRODUCT SPECIFICATION.

5. DUTY SUPERVISOR DECIDES TO RELEASE SHIP.

6. OPERATIONS SUPERINTENDENT SIGNS TANK RELEASE CERTIFICATE AND

RELEASES TANK FOR ISSUING AND LOCKS NOTICE TO "ISSUING".

ISSUE NO. 6 – MAY 2004

LATEST UPDATE: 1ST JULY 2005
 WI. B.3
WI.B.3

TANK RELEASE CERTIFICATE - MAIN PRODUCT ONLY.

Measured
Date Tank Product After Density Flash Calculated Expected Water Colour Density OCT Checked
Authorised
No. Shipment @15 Deg C Point Weighted Flashpoint Drained Comparision Waiver By To
(Composite) Deg. C Avearge Deg C (Differences Ref. Release
( A) Density Range ( A) - (B) (OFF- by.
@15DegC SPEC).
(B)

i) Composite Sample to be drawn as per Work Instruction.

ii) To be completed by duty Supervisor.
iii) To be authorised by Ops. Supt. Or Worksite Manager prior to releasing tank for issues.
iv) Density Acceptable limits, MOGAS, DPK & Gas-Oil is +/- 0.002 and Fuel Oil is +/- 0.004.
v) To seek for Waiver from OCT for Product Density differences exceeding acceptable Limits. Refer WOM Vol. 2 of 12, section B.1.6.4.
 WI. B. 4

WORK INSTRUCTION

HOSE DISCONNECTION AFTER TANKER DISCHARGE

(MAIN PRODUCTS & FUEL OIL)

1. ENSURE COMPLETE STRIPPING OF CARGO TANK, INDICATED BY AIR BLOWING

OUT FROM DRAIN COCK.

2. CLOSE CARGO LINE VALVE.

3. ENSURE DRIP TRAY UNDER HOSE / SHORE CARGO LINE CONNECTION.

IF WATER FREE, CLEAN AND CLOSE THE DRAIN COCK.

OPEN DRAIN VALVE TO RELEASE PRESSURE IN HOSE OR REQUEST SHIP'S CREW

TO RELEASE IT AT THEIR END.

4. IF SHIP'S MANIFOLD LEVEL IS LOWER THAN JETTY, SHIP TO DRAIN BACK

REMAINING QUANTITY INSIDE HOSE INTO SHIP'S TANK, SLIGHTLY OPEN HOSE
FLANGE CONNECTION TO RELEASE VACUUM.

IF SHIP'S MANIFOLD IS HIGHER THAN JETTY, SLOWLY CRACK OPEN HOSE/FLANGE

CONNECTION TO ALLOW REMAINING OIL (IF ANY) TO BE COLLECTED INTO
DRIP TRAY.

5. CONTAIN OIL FROM DRIP TRAY IN "WASTE-OIL" DRUM.

IF RECOVERY SYSTEM IS AVAILABLE, PUMP BACK OIL COLLECTED (EXCEPT JET

A-1) IN THE DRIP TRAY BY OPERATING THE RECOVERY SYSTEM. FOR JET-A1,
HOSE CONTENT COLLECTED IN THE TRAY SHOULD BE RECOVERED VIA MANUAL
METHOD INTO CLEAN DRUM FOR DOWNGRADING TO KEROSINE.

6. DISCONNECT HOSE AND INSTALL BACK BLANK FLANGE AT BOTH HOSE ENDS.
USE ALL BOLTS.
 WI. B. 5
WORK INSTRUCTIONS
WATER DRAINING (MAIN PRODUCTS) AFTER TANKER DISCHARGE

A. WATER DRAIN TANK AVAILABLE

1. AFTER TANKER DISCHARGE, CLOSE TANK INLET & OUTLET VALVE AND PADLOCK
TO PREVENT ACCIDENTAL ISSUING AND RECEIPT.

ALLOW TWO HOURS SETTLING TIME FOR VERTICAL TANKS AND 1 HOUR FOR
HORIZONTAL TANKS.

2. CRACK OPEN TANK DRAINING VALVE NEAREST TO TANK LEAVING SPRING

LOADED VALVE ON DRAIN LINE CLOSE. (SPRING LOADED VALVE IS SITUATED
JUST AFTER TANK DRAINING VALVE).

3. MAKE SURE WATER DRAIN TANK BOTTOM VALVE AND SAMPLING DRAIN LINE
VALVE IS SECURELY SHUT, (THE SAMPLE DRAIN VALVE IS NORMALLY
LOCATED IN THE CENTRE OF THE DRAINING LINE ABOVE SPLLAGE DRAIN)
BEFORE OPENING VALVE LEADING TO WATER DRAINING TANK.

4. FLUSH DRAIN LINE QUANTITY INTO WATER DRAINING TANK BY CRACKING OPEN
SPRING LOADED VALVE AND INLET VALVE TO WATER DRAINING TANK.
(DRAIN LINE QUANTITY IS STATED ON DRAIN LINE OR AT TANK DRAIN
VALVE).

5. MAKE SURE QUANTITY FLUSHED DOES NOT EXCEED DRAIN TANK CAPACITY
(TANK CAPACITY SHOULD BE CLEARLY STATED ON WATER DRAINING TANK)
AND OVERFLOW.

6. RELEASE SPRING LOADED VALVE TO STOP FLOW TO WATER DRAIN TANK.

7. USING A BEAKER OR 1-LITER CONTAINER (MAKE SURE CONTAINER IS BONDED TO

TANK FOR ELECTRICAL CONTINUITY) DRAW SAMPLE FROM DRAIN LINE.

8. IF FREE WATER IS FOUND, CLOSE WATER DRAINING TANK INLET VALVE

AND ALLOW TO SETTLE FOR ABOUT 15 MINS. DRAIN FREE WATER
INTO DRAIN BY CRACKING OPEN BOTTOM DRAIN TANK VALVE TO
DRAIN OFF FREE WATER IF ANY. THEN CLOSE BOTTOM VALVE
(SAMPLE SHOULD BE POURED BACK INTO WATER DRAINING TANK).

9. REPEAT STEPS 3 TO 9 UNTILL FREE OR SUSPENDED WATER IS REMOVED.

10. WHEN WATER IS COMPLETELY REMOVED OPEN WATER DRAINING TANK OUTLET
VALVE AND PUMP OIL BACK INTO STORAGE TANK.

11. FINALLY CHECK ALL VALVES STARTING FROM TANK INLET TO QUICK FLUSH
WATER DRAINING TANK AND ENSURE VALVES ARE TIGHTLY CLOSED THEN
PADLOCK.

12. RECORD IN RECORD BOOK AND DAILY RECORD CHECKLIST APPENDIX B.2 B
QUANTITY DRAINED.

B. WATER DRAIN TANK NOT AVAILABLE

FOLOW ABOVE PROCEDURE, INSTEAD OF DRAINING INTO WATER DRAIN TANK WATER
CAN BE DRAINED INTO DRUMS. WORKSITE TO ENSURE THESE CONTAMINATED PRODUCT
MUST BE BOOKED INTO STOCK. WORKSITE MANAGER CAN AUTHORISED DISPOSAL AFTER
CONSULTING OLA/OCT.
 WI.B.6

WORK INSTRUCTION

FORMULA SHELL DIESEL ADDITIVE DECANTING

1. ADDITIVE CONTAINED I N UNDERGROUND TANK.

2. GANTRY OPERATOR DIPS TANK EACH DAY AND RECORDS THE DIPS DIP BOOK.

3. OPS. SUPT. REVIEWS THE DIP BOOK DAILY.

4. DO NOT ALLOW TANK LEVEL TO FALL BELOW 200 LITRES.OPS.SUPT. ESTIMATES

REQUIREMENT AND INFORMS GANTRY OPERATOR TO CARRY OUT DECANTING
OPERATIONS.

5. GANTRY OPERATOR CARRIES OUT DECANTING.

- DETETMINE THE NUMBER OF DRUMS TO BE DECANTED

- OPEN TANK VALVES
- USE NOT FILL TANK TO BEYOND SAFE LEVEL
- ATTACHED BONDING TO THE DRUM TO BE DECANTED
- CONNECT DECANTING HOSE. ENSURE NO LEAKS
- START ADDITIVE PUMP AND COMMENCE DECANTING
- DISCONNECT DECANTING HOSE FOR PROPER STOWAGE
- DISCONNECT BONDING
- STACK ADDITIVE DRUMS IN DESIGNATED AREA OF DRUM
- RECORD THE NUMBER OF DRUMS DECANTED IN THE DIP BOOK

6. FOLLOW "WARNING " SIGN INSTRUCTIONS AT ALL TIMES.

 WI. B. 7

WORK INSTRUCTION

WARNING - FORMULA DIESEL ADDITIVE - NEMO 7021

A. SAFE HANDLING

WHEN HANDLING ADDITIVE FULL FACEPIECE RESPIRATOR WITH ORGANIC

VAPOUR CANISTER AND BUILT-IN PARTICULATE FILTER (NPF 400) AND NEOPRENE
OF NITRILE RUBBER GLOVES MUST BE USED AT ALL TIMES.

B. IN CASE OF: -

1. INGESTION

OBTAIN MEDICAL ATTENTION IMMEDIATELY.

2. SKIN CONTACT

REMOVE ANY CONTAMINATED CLOTHING.

WASH CONTAMINATED SKIN WITH SOAP AND WATER.
IF WASH IRRITATION PERSISTS, OBTAIN MEDICAL ATTENTIO N.

3. INHALATION

REMOVE AFFECTED PERSON TO FRESH AIR.

IF BREATHING STOPPED, APPLY FIRST AID AND OBTAIN MEDICAL
ATTENTION IMMEDIATELY.
 WI. B.8

WORK INSTRUCTION

WARNING - FORMULA SHELL SUPER UNLEADED, SUPER,

REGULAR/UNLEADED 92 ADDITIVE - NEMO 9436

A. SAFE HANDLING

WHEN HANDLING ADDITIVE, FULL FACEPIECE RESPIRATOR WITH ORGANIC

VAPOUR CANISTER AND BUILT-IN PARTICULATE FILTER (NPF 400) AND NEOPRENE
OR NITRILE RUBBER GLOVES MUST BE USED AT ALL TIMES.

B. IN CASE OF: -

1. INGESTION

DO NOT INDUCE VOMITING.

OBTAIN MEDICAL ATTENTION IMMEDIATELY.
DO NOT GIVE ANYTHING BY MOUTH TO AN UNCONSCIOUS PERSON.

2. SKIN CONTACT

REMOVE ANY CONTAMINATED CLOTHING.

WASH CONTAMINATED SKIN WITH SOAP AND WATER.
IF SKIN IRRITATION PERSISTS, OBTAIN MEDICAL, ATTENTION.

3. INHALATION

REMOVE AFFECTED PERSON TO FRESH AIR.

IF BREATHING HAS STOPPED, GIVE ARTIFICIAL RESPIRATION.
OBTAIN MEDICAL ATTENTION IMMEDIATELY.

4. EYE CONTACT

IMMEDIATELY FLUSH EYE WITH PLENTY OF FRESH WATER FOR 10

MINUTES. REFER FOR MEDICAL ATTENTION.
 ADDITIVE INJECTION FOR FORMULA SHELL DIESOLINE (FSD)
WI.B.9
1. FILLING AT GANTRY

OPS. SUPT./ DRIVER

FILLING GANTRY
BULK SUPV.
Determine additive tank to be used for the day. Proceed to Bay__Meter__ 1. Automated
‘ON’ isolating switch (in the office) Ready to fill per procedures.
‘ON’ power supply (in the office) Ensure amber light ‘ON’ at additive tank whilst
Handover the LAT (Loading Advice Ticket). filling up ( for ‘GAS’ equipped W/site).
Instruct driver to fill ex Bay__Meter__.
1A NON is when ‘amber’ light at additive
CONFORMANCE tank is not lighted.

For ‘GAS’ Worksites

For other Worksites is when warning light at gantry starts to blink.
Immediately stop operations
Inform Delivery Service Supervisor / Supervisor.
Wait for further instructions.

2. STOCK CONTROL
OPS. SUPT./ DEPOT OPS. SUPT./ STOCK
BULK SUPV. OPERATOR BULK SUPV. CLERK
Instruct Depot Operator to do daily tank dip. Dip tank daily.
Instruct Depot Operator to top up tank with Record tank dip in dip book. When topping up is required, To issue required quantity of
calculated quantity of additive (SAP XXXX). When instructed, top up the additive storage tank. inform stock clerk additive (in drums).
Additive stock level in tank is not allowed to Use protective apparel and follow warning signs. To update stock card.
fall 200 lit. To indent if required.

1. PUMPING/DECANTING ADDITIVE INTO UNDERGROUND STORAGE TANKS

OPS. SUPT./ DEPOT Put in the nozzle into the drum to pump out additive into
BULK SUPV. OPERATOR underground storage tank.
After completion:
Get the correct number of drums in the godown. Out back nozzle in the original position and place.
Instruct Depot Operator to take the correct
Roll it to the additive underground storage tank. Turn the ‘knob’ back into its original position and place.
number of additives in drums ex godown,
Attach bonding wire to the drum to be decanted and Roll the drum into the empty drum yard.
Switch ‘OFF’ the system switch (in the office).
connect hose. For STSB worksites, use drums for packed diesel or
Switch ‘ON’ the drumming switch (in the office).
Turn the ‘knob’ (near the storage tank) ‘OFF’ by containing sludge or toxic paint waste.
After completion : ‘ON’ the system switch.
turning it to the right. For SMTSB worksites, drums are sold to TKO.
‘OFF’ the drumming switch.
 WI. B.10

ADDITIVE INJECTION FOR FORMULA

SHELL SUPER (PMS) & REGULAR (RMS), ULG & U92

STOCK CONTROL

OPS. SUPT./ STOCK CLERK

BULK SUPV.

Based on ship’s arrival, calculate volume of additive Upon receiving request from Ops. Supt. / Bulk Supv.:
(Qty SAP XXXX) to fill the additive tank. Issue number of additive (in drums) required.
Update stock card.
Inform Stock Clerk on the number of drums Indent if required.
required.

OPS. SUPT./ DEPOT OPERATOR

BULK SUPV.

Instruct Depot Operator to:
Take additive drums to additive tank area,
Fill additive into storage tank.
Store empty drums at empty drums yard.
Advise Stock Clerk to book-in empty drums
into Stock Card.
Take correct number of additive drums from
warehouse to additive tank area.
Attach bonding wire to drum to be decanted.
Fill additive into additive tank in yard and stack them
properly.
After completion, store empty drums in designated
area of drum yard.
Use protective apparel and follow warning signs.

DOPING

OPS. SUPT./ DEPOT OPERATOR

BULK SUPV.

Instruct Depot Operator to start doping product
when ship starts discharging product,
When ship starts discharging product and after
instruction by Ops. Supt./Bulk Supv.:
Open Valve 1 - Outlet valve of additive tank.
Open Valve 2 - Valve after sight glass of
additive pump to the cargo line.
Open Valve 3 - Valve to the cargo line.
‘ON’ the injection pump.
While pumping, observe the plastic tube & the
graduated scale on the additive side & keep
Ops. Supt./Bulk Supv. Informed.
‘OFF’ the injection pump when the required has
been injected.
Close all the three valves.
Inform Ops. Supt./Bulk Supv.
2. Use protective apparel and follow warning signs.
 WI.B.11

WORK INSTRUCTION

CALIBRATION OF ADDITIVE INJECTION SYSTEM AT WORKSITES WITH AVERY

HARDDOLL METERS

1. CLOSE THE OUTLET VALVE LEADING TO GANTRY.

2. OPEN SUCTION VALVE OF UNDERGROUND TANK.

3. CLOSE MEASURING CAN'S OUTLET VALVE.

4. START ADDITIVE PUMP AND TRANSFER ADDITIVE FROM UNDERGROUND TANK

INTO THE CALIBRATED MEASURING CAN AND OBSERVE FILLING.

5. SLOWLY SHUT OFF THE SUCTION VALVE OF UNDERGROUND TANK WHEN

ADDITIVE REACHES THE DESIRED QUANTITY IN THE MEASURING CAN.

6. OPEN MEASURING CAN OUTLET VALVE.

7. OPEN OUTLET VALVE LEADING TO GANTRY.

8. SHUT OFF VALVE FROM RELIEF VALVE TO THE UNDERGROUND TANK AND OPEN
THE VALVE FROM THE RELIEF VALVE TO THE CALIBRATION CAN DURING
FILLING OF BULK LORRY.

9. MONITOR INJECTION OF ADDITIVE THROUGH METER INTO LORRY

COMPARTMENT.

10. THE DIFFERENCE BETWEEN THE ADDITIVE QUANTITY READINGS AT THE

BEGINNING AND END OF LORRY FILLING IS THEN CALCULATED AND THE DOPING
RATE WORKED OUT.

11. STOP ADDITIVE PUMP.

12. AFTER COMPLETION OF CALIBRATION, ENSURE THE VALVE LEADING FROM

RELIEF VALVE BACK TO THE UNDERGROUND TANK IS OPENED AND THE VALVE
FROM THE RELIEF VALVE TO THE CALIBRATION CAN IS CLOSED BACK FOR
NORMAL ADDITIVE DOPING.

13. RECORD ABOVE CHECKS USING APPENDIX C.14.

 WI. B. 12

WORK INSTRUCTION
FORMULA SHELL GASOLINE NEMO 9436 DOPING

1. CALCULATE THE QUANTITY OF NEMO 9436 BASED ON VA QUANTITY AT

OBSERVED TEMPERATURE.

2. MEASURE THE BALANCE OF A DRUM'S ADDITIVE BY TRANSFERRING THE EXCESS

IN THAT DRUM TO ANOTHER NEMO 9436 PART DRUM USING A HAND PUMP. USE A
DRUM DIPSTICK TO DETERMINE THE QUANTITY.

3. POSITION DRUM TO THE INLINE BLENDING WORKSTATION.

4. ATTACH BONDING TO DRUM TO BE DECANTED.

5. ESTIMATE DURATION OF MOGAS DISCHARGE.

6. COMMENCE IN-LINE BLENDING SOON AFTER DISCHARGE HAS STARTED.SPREAD

OVER THE BLENDING EVENLY OVER PERIOD OF DISCHARGE.

7. EMPTY DRUMS MAY BE USED FOR STORING SLUDGE, WASTE OIL/USED OILS OR
TOXIC PAINT WASTE, OR FOR FILLING PACKED MOGAS AND SOLD.
HOWEVER, PRECAUTIONS MUST BE TAKEN TO ENSURE CORRECT
LABELLING IS DONE BEFORE DRUM IS FILLED WITH PRODUCT.

8. FOLLOW "WARNING" SIGN INSTRUCTIONS DISPLAYED AT ALL TIMES

 WI. B.13
Page 1 of 2

WORK INSTRUCTION

DOPING GAS OIL WITH STADIS 450

Objective : To increase product (Gas oil) electrical conductivity (reduce risk factor from
‘Increased’ to ‘Standard’ as documented in OP.98.42179 document)

Scope : All Gas Oil product shipments received by worksites.

These additional steps are to be taken immediately after the procedure written in 1.3.13 of Manual of
Worksite Operations (WOM) Volume 2 of 12

5. Make a volumetric composite sample of the individual tank’s composite sample that will be
discharged at the site.

6. Measure the product electrical conductivity using an approved conductivity meter (Maihak/Emcee
meter). Ensure the meter is clean from any contamination before conducting the measurement.
Method of using these meters can be found in SAOM (Appendix 02.03.06.1 and 02.03.06.1).

7. Record the electrical conductivity reading in the “Bulk Cargo Receipt Log” page 3 of 9 for the
composite sample.

8. If the sample’s electrical conductivity is less than or equal to 70pS/m, do the following:

a) Prepare Stadis 450 additive for doping:

n Estimated of 3 liters per 1000MT to increase product electrical conductivity by 200pS/m
n Maximum of 3 mg of Stadis 450 per Liter Gas Oil
n Dope the Gas Oil product based on calculated electrical conductivity to be at least 100pS/m

b) Dope the storage tank with Stadis 450 by

i. If design permits, dope Stadis 450 through the product pipeline.

n Set up the doping equipment into product line.
n The slower the doping rate (stretched throughout the product discharging time) the
better the mixing result will be.

OR

i. Dope Stadis 450 into storage tank

n Fill Stadis 450 into an approved container with approved rope attached.
n Gently lower the container (until it reaches the product level) into the storage tank.
n Remove product from container (avoid splash loading).
n If product will be pumped into more than 1 tank, ensure each tank is doped with Stadis
450 accordingly; based on estimated amount each tank will receive and from which ship
cargo tank will it receive from.

5. Continue tanker discharge procedure as stated in 1.3.14 of WOM Volume 2 of 12

6. During the first delivery of the new Gas Oil stock,

7. Sample product at gantry during the coldest time of normal operation (i.e. morning/night)
8. Measure product electrical conductivity of product using either Maihak/Emcee meter.
Record the measurement reading into the tank dip book (remark column).
9. If the electrical conductivity falls below or at 50pS/m, dope the affected product at the
storage tank with Stadis 450 (as per procedure above).
10. Record the Stadis 450 doping amount into the tank dip book (remark column).
11. Note such depletion and adjust doping amount accordingly during the next Gas Oil
shipment.

WI. B.13
Page 2 of 2
7. If the affected Gas Oil stock remained in the storage tank for more than a month, the electrical
conductivity of the product should be tested once a month:
8. Sample product at gantry during the coldest time of normal operation (i.e. morning/night)
9. Measure product electrical conductivity of product using either Maihak/Emcee meter.
Record the measurement reading into the tank dip book (remark column).
10. If the electrical conductivity falls below or at 50pS/m, dope the affected product at the
storage tank with Stadis 450 (as per procedure above).
11. Record the Stadis 450 doping amount into the tank dip book (remark column).
12. Note such depletion and adjust doping amount accordingly during the next Gas Oil
shipment.
 WI. B.14

WORK INSTRUCTION

SUBSIDY CLAIM

1. The due date for submission of subsidy claim to local Customs for any month is on or
before the 15th of the following month.

2. Fax or letters of Customs subsidy rates and duty rates for all products are obtained from
Head Office Stocks Accounting Dept for current month.

3. MPSS is signed off after month-end closing and sent off to Head Office Stocks
Accounting Dept After the end-month closing, worksite compiles the “Lampiran
A”. Worksite gets confirmation via e-mail from Head Office Stocks Accounting
Dept for all commercial customers (PDA7) on the agreed amount to claim for each
worksite.

4. The “Lampiran A” is sent to the local Customs together with supporting copies of
delivery documents (e.g. invoices, delivery tickets), MPSS, sales summary,
subsidy/duty rates, K1 form, gatepass report and MDTCA subsidy permits. The
supporting documents required by each area’s local Customs may vary.

5. Retail stations qualify for full subsidy subject to quotas. Where quotas are exceeded,
duty penalties may be imposed on the retail stations.

6. Subsidy permits are issued by MDTCA to land transport commercial customers and
fisheries.

7. A copy of the “Lampiran A” is e-mailed to Head Office Stocks Accounting Dept.

8. Head Office Stocks Accounting Dept issues credit notes to qualifying commercial
customers.

9. Worksite engages with local Customs on discrepancies arising from the subsidy claim.

10. Worksite follows up with local Customs on the despatch of the subsidy claims by local
Customs to Customs Head Office.

11. Subsidy claim records should be kept for 6 years by worksite.