International University, Vietnam National University - HCMC 1

GENERAL CHEMISTRY LABORATORY

REPORT
EXPERIMENT 3: REDOX TITRATION
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+ Hard copy: Submitted to Instructor/TAs
Deadline: At lab entry of Experiment 4

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Date: _________

Score: _________

Last updated: 07/05/2016 by Assoc. prof. Huynh Kim Lam & M.Sc. Le Nguyen Thien Phuc
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This report MUST BE TYPED and handed in together with the signed data sheet
 International University, Vietnam National University - HCMC 2
GENERAL CHEMISTRY LABORATORY

1. TITRATION OF KMnO4 SOLUTION WITH STANDARD H2C2O4 SOLUTION

Normality of the standard H2C2O4 solution, N(H2C2O4) = ______0.05N______

Volume of the standard H2C2O4 solution used, V(H2C2O4) = ___10mL_________

Trial
Burette reading (mL) Volume of KMnO4 (mL) Normality of KMnO4 (N)
#
1 16mL - 27.2mL 11.2 mL 0.044 N

2 27mL- 38.5mL 11.5mL 0.043 N

Average Normality of KMnO4 = ____0.044_____ ( N )

Comment:

2. TITRATION OF UNKNOWN CONCENTRATION H2C2O4 SOLUTION WITH

STANDARD KMnO4 SOLUTION

Normality of the standard KMnO4 solution, N(KMnO4) = ____unknown_____

Volume of the unknown H2C2O4 solution used, V(H2C2O4) = ___10mL___

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of H2C2O4 (N)

1 38.5mL-44mL 5.5mL 0.024 N

2 19.2mL-25mL 6.2mL 0.027 N

Average Normality of H2C2O4 =__0.025_____ ( N )

Comment:

Last updated: 07/05/2016 by Assoc. prof. Huynh Kim Lam & M.Sc. Le Nguyen Thien Phuc
*
This report MUST BE TYPED and handed in together with the signed data sheet
 International University, Vietnam National University - HCMC 3
GENERAL CHEMISTRY LABORATORY

Using unknown concentration H2C2O4 to titrate KMnO4 because

KMnO4 is changed the normality when we take it in the
unsuitable condition. When KMnO 4 reacts with H2C2O4 , the
color of KMnO4 disappear because KMnO4 does not exist after
reaction, as soon as all the H 2C2O4 react (endpoint), the KMnO4
in excess and the solution in flask now turn pink. We record the
volume of KMnO4 used and calculate the normality of KMnO 4
solution.

Last updated: 07/05/2016 by Assoc. prof. Huynh Kim Lam & M.Sc. Le Nguyen Thien Phuc
*
This report MUST BE TYPED and handed in together with the signed data sheet
 International University, Vietnam National University - HCMC 4
GENERAL CHEMISTRY LABORATORY

3. TITRATION OF UNKNOWN CONCENTRATION FeSO4SOLUTION WITH

STANDARD KMnO4 SOLUTION

Normality of the standard KMnO4 solution, N(KMnO4) =___unknown_____

Volume of the unknown FeSO4 solution used, V(FeSO4)= __10mL___

Trial # Burette reading(mL) Volume of KMnO4 (mL) Normality of FeSO4(N)

1 25.3mL-33mL 7.7mL 0.034 N

2 32.6mL-42mL 9.4mL 0.041 N

Average Normality of FeSO4 =___0.037____ ( N )

Comment:

Last updated: 07/05/2016 by Assoc. prof. Huynh Kim Lam & M.Sc. Le Nguyen Thien Phuc
*
This report MUST BE TYPED and handed in together with the signed data sheet