Epenmcnt:

Dote
K2o/AI8/1a Pane No

ExPERIMENT NO. -4

AIM-T Setevne the Concelration of dissolve8

the qve wates Sample
Gyaen ts
0sinq 1hndor N4o Na,0 40tion.
APPAROTS INVOLVED: Bosdte Prpeteleasinqlask,alassr
RERGANTS REGUIRED
PeToss in iside golstion (101.)
N40 Hyps 3slufion (Na,S,9,)
Starch 3slufien Grehy_peparel]
PRoCEDURE
2. 50 m wates Sample was taken in Todemesic Hask contact uith aiy w
ovcTdel a8 as ad psil+ble.
1m monqonese 3ulphate delstion rem te burette ans 1 mB
alkaline Tea7de rothe dthes bosette wa asSeN imeio kel
3he 5feppes wo inieie9 ansuas shaken 8evesal fime8.
The preaptte ug allouel t xttle t way and ine aqoin, The prscess
t p e e h k i ans settlinq w sepeae9 at least thseetfme
5. 1 Cenc. 8ulphufc agd aa addes. e stopper was înseste and

shaHen a gain
he yelo 3slsfion wo allaed t slans on5 mints.
0 m solutie wos At8xawn , ihidh wo htsates yinst te
STandard N40 30dym tiesulphate 3alstion U he cale ate 8olstion
be cemesfuint yello.

DELTA
 KaglAI8
Stodose e Starch

CHON CH0H CHOH

-O o H -O H
-0 OM C OH H H

OH H OH OH

Glocese
lelecoleg

o000nod
oO0000
Starch

ReactionsTnvelve
MnS0+2HoH MolOH),+ K,S04
an (oH)+ 2 MnOOH) Basic imonganese xde j
2rn O(oH) +H,S0% MaSo, +H,0 +p
KI +HSo, +Lo] So+ HOI
I + Na S0 aNalNa,0 (Se8fum tetiathionate )
Stasch+Ta Blue cels1 Complex

Aide Meksten
Na Ng+ H* NH+Na
N+NO,+ H*.
N+2H0
 Obsesvatiens
50 nl
Velue wdts an each ttration

ValneNho throsolphate woluien -

Tnnol busette Rnel busette Velume Cencendant

5.No. Jeang (ml) 8olotion
Teabing (ml)D
(v.) ()

45.5 45.5
445 44-5 44.5
3 44.5 445
44-5
. 445

Concedanit seadng 44-5

Calolahens
Nates Vsates = Npe X
Ve
N,x 50 m = x 44.5mt

N: 445 : 0.0225 N
0 SO
STsength deaske
Bdved oxy genE N»bq,st
O 0222Sx &x1o 00
1*8 ppm
 Experiment: Dale

Ko/As/R Poge No.

aFe dsops 3torch g9lsñen wag_aßdes ats lage , Doe to thke

nation Tasch-jerde tke celouo osnes Seep-blwe
The tratfon wag certinve t the salutfion became colaunleBp.

Resut Disselued Gxygen =F3 ppm.

Precaston$
.TeSelstion n the íosrde lask 3hl be shakencavefolly hle keeping
te thumb en t e .
dyausn j
2. he 38lstion dheulD be well 3haken bese each alauot is wth
atit,
pipette
3. The slotf+on inhe ToSine Mask theul! nst be jucked inte t
wTth e mg

DELTA