Professional Documents
Culture Documents
Every effort has been made to ensure that the information contained in this manual is accurate; however no liability is accepted
for errors. Should an error be discovered please inform the company in writing, giving full details. Any experimental results given
are for guidance only and are not guaranteed as exact answers that can be obtained for a given apparatus; due to the complex
variables applicable to most experiments.
EdLabQuip GmbH
Peiner Str. 157E, 30519 Hannover, Germany
www.edlabquip.com
sales@edlabquip.com
Tel: +49 511 56 37 98 7
TD 005 Temperature Measurement Bench
CONTENTS
4. Results .………………………………………………………………… 30
5. Sample Graphs …………………………………………………………. 37
ADDENDUM 1: Characteristic Temperature & Electric Resistance of PT100.. 41
ADDENDUM 2: Thermocouple Type K ………………………………………….. 42
ADDENDUM 3: Table for (NTC) Thermistor Probe …….………………………. 43
ADDENDUM 4: Temperature Indicator …………………………………………. 44
ADDENDUM 5: Calibration Certificates …………………………………………. 47
All rights reserved. No part of this publication may be reproduced in any material form (including photocopying or storing in any
medium by electronic means and whether or not transiently or incidentally to some other use of this publication) without the written
permission.
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TD 005 Temperature Measurement Bench
RECEIPT OF GOODS
1. On Receipt of Goods
(a) On receipt of the goods at the customer’s premises, the shipment should be inspected for any damages
or missing items. These items should be checked against the delivery note, packing list or shipping
documents.
(b) If there is any damage to the equipment or a discrepancy in missing items as listed shipping documents,
then the insurance company should be notified within three working days on receipt of the shipment if
the loss or damage was not apparent at the time of taking delivery from the port.
(c) If insurance has been arranged by the buyer then you must notify your insurer in writing of any damage
or loss of parts which was observed regarding this shipment within a specified period of time as stated
in the Terms and Conditions. This should include detailed photographs of the damaged equipment.
(d) If insurance has been arranged by the seller you should notify the insurances representative along with
any correspondence including the insurance certificate supplied by the seller. These should include
detailed photographs for evaluation of damages or replacement parts pertaining to the shipment.
(e) The seller will only replace damaged parts on notification by the insurance company that the claim has
been accepted.
2. Manufacturers Liability
(a) Before proceeding to install, commission or operate the equipment listed in the instruction manual, we
would like to alert the user to the health and safety aspects of people who will work on or operate our
equipment with regard to the liability of the manufacturers or suppliers.
(b) Manufacturers or suppliers are absolved of any responsibilities with regard to misuse of their equipment
causing harm or financial charges being incurred against them from clients or third parties for
consequences of failure or damage of the equipment in any way if the equipment is not installed,
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maintained and operated as outlined in the instruction manual published by the manufacturers or
suppliers.
(c) In order to safeguard the students and operators of the equipment it is vital that all safety aspects as
outlined in the instruction manual are observed.
3. Safety Guidelines
1.3.1 General Safety Concerns
Before proceeding to install, commission, or operate the equipment described in the instruction manual we
would like to alert you to the dangerous potential hazards that would be present if safety practices were not
performed in accordance with the local standards and governing bodies regulations.
-Injury would occur to the operational staff of the equipment through misuse, electric shock, rotating
equipment hazards and lack of cleanliness.
To be able to achieve the aim, of “accidents can be avoided” it must be ensured that the equipment is
installed correctly, regularly maintained and operators of the equipment are made aware of the potential
hazards associated with the particular equipment.
We would like to inform our valuable customers of the safety guide lines when using their equipment.
1.3.2 Awareness of Safety Hazards
(a) Before attempting to work on the equipment the personnel who are going to install, commission, or
operate the equipment must be qualified and fully aware of all the manufacturers and suppliers
recommendations and instructions.
(b) Ensure that the all the recommendations specified in the instruction manuals are maintained as stated in
the contents.
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TD 005 Temperature Measurement Bench
4. Electrical Safety
(a) Ensure that the person who works on the equipment is a qualified electrical engineer/technician who is
competent in the safety aspects and operational mode of the equipment.
(b) If the electrical supply to the equipment is supplied by means of a portable trailing cable, protective
devices such as an Earth Leakage Circuit Breaker (ELCB) must be installed.
This protective device must have a very high sensitivity (20-30mA).This device is also referred to as a
residual current device(R C D) within the electrical supply circuitry for personnel protection.
(c) The supply cable must be sized accordingly for all fault and physical conditions pertaining to its use.
The supply network must also incorporate a protection device that will disconnect and isolate the
supply voltage in the case of an overload in a specified period of time without causing any damage to
the equipment. (An overload relay)
5. Installation
(a) On receipt of the equipment extreme care should be used to avoid damage to the equipment on
handling and unpacking. If slings are used ensure they are held on a rigid part of the equipment, the
structure. In the case of a mechanical lift such as a fork lift ensure the lifting forks are beneath the
structure framework so that no damage will occur during the lifting operation.
(b) In some cases it is imperative that the equipment be installed on a level and solid foundation
5.1 Electrical Supply Cables
(a) The normal color code of the power cables supplied on this equipment is as follows:
- Black----------------------------Line.
-Gray or white. -----------------Neutral.
- Red------------------------------Ground.
(b) The three phase power cable has five wires.
- Red, blue and black. ---------Line.
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TD 005 Temperature Measurement Bench
(c) Safety valves should be calibrated on a regular basis with mandatory service records maintained. This
should also include pressure reducing valves.
(d) Calibration of any instrumentation such as pressure gauges, thermometers and sensors should be
checked regularly.
(e) Visual inspection of the equipment should be regularly observed for leaks of steam etc and any
frameworks or joints should have the hardware checked for tightness.
(f) Always use protective clothes including gloves when carrying out maintenance on the equipment.
5.5 High Temperature Equipment
(a) When using high temperature equipment there are a number of vital precautions which must be
remembered by the operators and maintenance crew and observed when both operating and performing
maintenance schedules. During operation of this equipment the air, gas or water is at a high
temperature and pressure which can have a very damaging and hazardous effect on students if safety
precautions are not observed.
(b) Ensure that critical values of temperature and pressures listed in the instruction manual are maintained
and not exceeded on the equipment.
(c) Calibration of any instrumentation such as, thermometers and sensors must be checked regularly for
safe operation.
6. Maintenance Safety Practices
(a) Always isolate the equipment from the electrical supply when carrying out maintenance on the
equipment
(b) Ensure that safety notices are placed on the equipment supply advising personnel that the equipment is
being worked on, inspected and should not be operated.
(c) Check the operation of any protective devices, such as an ELCB so that it operates in accordance with
its specifications thus ensuring the safety of all operational personnel working on the equipment. Any
malfunction of the device must be corrected by a qualified electrician before returning the equipment
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TD 005 Temperature Measurement Bench
1. General Description
The Temperature Measurement Bench is bench-top unit designed to for studying methods of
temperature measurement of several commonly used devices as well as understanding related
principles. The apparatus is equally suitable for student experiments or demonstration.
Heat sources and means of calibration and accuracy comparison of the different devices are
provided.
3 5
2
1
6
7
4
a7
b 1
2
8 1
1
1
3
1
69
1
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41
5 1
0
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TD 005 Temperature Measurement Bench
Heat sources
• Water heater, consisting of hot plate and stainless steel pot.
• Hot air heater with blower and stand.
• Ice pail.
Other instruments
• Digital millivoltmeter
• Digital read-out units; for platinum resistance thermometer, thermistor and thermocouple.
Power supply : 220 V, 1 Ph, 50 Hz, Other voltages are available upon request.
(boiling water).
Hot air blower is used for measurement from room temperature to above 100°C.
Alternatively, flushing oil (for flushing engine) which is available at petrol station can also be used
for measurement from room temperature to above 100°C.
Alternative calibration / measurement
The indicators for platinum resistance, type K thermocouple, and thermistor are pre-circuited and
calibrated to indicate temperature directly. However, precision resistors are provided for
calibration of 0°C and 100°C;
100 for setting 0°C for platinum resistance thermometer PT100.
1 k for setting 100°C for thermistor.
10 k for setting 25°C for thermistor
This is simply done by connecting the resistor to the indicator terminals in place of the sensors.
For type K thermocouple temperature may be alternatively determined by connecting the
thermocouple to the milli-voltmeter the temperature can then be determined from the provided
voltage-temperature table.
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TD 005 Temperature Measurement Bench
2. Theory
2.1 General Principle of Temperature Scale
It is a common experience that bodies feel hot or cold to the sense of touch, depending upon
their temperature. In setting up a scale for the measurement of temperature, it is customary to
use for one reference point the temperature of a mixture of cracked ice and water and for a
second reference point the temperature of boiling water at standard barometric pressure. On the
Fahrenheit (°F) scale the numbers 32 and 212 are assigned to these reference temperatures.
The numbers 0 and 100 are assigned to those temperatures on Celcius (°C) or centigrade
scale. Referring to Fig. 2, 212 °F is equivalent to 100°C, 1°F is equal to 5/9 °C, or
F Fahrenheit scale
R Absolute temperature, degree Rankine
C Centigrade scale
K Absolute temperature, degree Kelvin
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TD 005 Temperature Measurement Bench
The basic for establishing a temperature scale to serve as a primary standard is the fact that at
constant temperature, the pressure-volume product for a pure gas approaches a constant finite
value as the pressure approaches zero. The basic standard fixed points of International Standard
Temperature Scale are as follows:
- temperature of equilibrium between liquid and gaseous oxygen at the pressure of 1
standard atmosphere (oxygen point) = -182.97°C
- between ice and air-saturated water at normal atmospheric pressure (ice point) = 0°C
- between liquid water and its vapour at the pressure of 1 standard atmosphere (steam point) =
100°C
- between liquid sulphur and its at the pressure of 1 standard atmosphere (sulphur point) =
444°C
- between solid silver and liquid silver at normal atmospheric pressure (silver point) = 960.5°C
- between solid gold and liquid gold at normal atmospheric pressure (gold point) = 1063°C
For ordinary use, the mercury thermometer agrees closely with the International Standard Scale,
but above 200°C the divergence between the two scales may be appreciable.
The common mercury thermometer can be used to about 250°C. This limit may be extended to
500°C if the capillary tube above the mercury is filled with nitrogen or carbon dioxide under high
pressure. The lower limit for the mercury thermometer is -39°C. For lower temperatures, alcohol,
pentane, or petroleum ether may be used as thermometric substance. When the stem of a total-
immersion thermometer is only partial immersed, as in a thermometer well, a correction for stem
exposure must be made. Temperatures are also measured by means of bimetallic strip expansion,
electrical resistance, thermocouples and various forms of optical pyrometers.
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TD 005 Temperature Measurement Bench
2.2.1 Liquid-in-glass Thermometers
The liquid-in-glass thermometers are usually filled with mercury and have a vacuum in the
capillary. Since freezing point of mercury is -39°C, alcohol or pentane is used where lower
temperature is encountered. To measure temperatures above 300°C, the mercury is scaled under
pressure with nitrogen or carbon dioxide in the capillary. With special glass, such thermometers
may be usable up to 500°C, although difficulties with bulb and stem distortion may be encountered
above 500°C. The quality of the glass has an important bearing on the accuracy and
permanence of the thermometer.
use.
Bimetallic Thermometer
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TD 005 Temperature Measurement Bench
2.2.4 Thermocouples
Thermocouples are pairs of wires, of dissimilar metals, connected at both ends. When the two
junctions are subjected to different temperatures, an electrical potential is set up between them.
This voltage is almost directly proportional to the temperature difference, and hence a voltage
measuring instrument placed in the circuit will measure temperature. Table 2 gives the e.m.f.
generated at various temperatures with commonly used thermocouples. For use at
temperature below 300°C, copper-constantan (copper 60% with nickel 40%) thermocouples are
best because of their resistance to correction and consequent long life with stable calibration.
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Between 400°C and 760°C iron-constantan thermocouples are best and are and can be used
either an oxidizing or reducing atmosphere. The rusting of the iron at low temperature in the
present of moisture make iron-constantan less desirable than copper-constantan for temperature
range in which the latter can be used. For high temperature work platinum-platinum 10 percent
rhodium thermocouples should be used. In reducing atmosphere the couple must be thoroughly
protected. A slightly more sensitive high-temperature thermocouple consists of platinum-platinum
13 percent rhodium. Chromel (chromium 90% with nickel 10%) -alumel (nickel 95% with 5% of
aluminium, manganese and silicon) thermocouples are more stable than iron-constantan but less
stable than platinum-platinum rhodium thermocouples for higher-temperature work of up to 1260
°C as well as for low-temperature work of as low as -250 °C.
Any convenient size of wire may be used, but a good electrical contact at the junctions and the
insulation of the rest of the wire are important. Junctions may be twisted together, but for
mechanical strength and to ensure good electrical contact in spite of oxidation, welded or soldered
junctions are preferable. Insulation may be enamel, silk, cotton, or other fibres for low
temperatures, and asbestos, glass fibre, porcelain or other refractory for high temperatures.
Selected metals should be used for Fig. 6, and each batch of wire should be calibrated.
Figure 6: Thermocouple
Thermocouples may be either of the millivoltmeter type or of the potentiometer type. Millivoltmeter
instruments have the advantage of direct reading. The accuracy of a high grade millivoltmeter
pyrometer with 15 cm scale and with calibrated couple and leads is usually within 1 or 2 percent of
scale range. The potentiometer instruments measure the thermocouple voltage as shown in Fig. 7
by balancing a known battery voltage against it. Potentiometer-type industrial recorders and
controllers using thermocouples are commonly used in industry because of their advantage of
high accuracy. The usual guarantee on such instruments is normally less than 1 percent of scale
range. Potentiometer-type industrial temperature recorders and controllers using thermocouples
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TD 005 Temperature Measurement Bench
are widely used because of their advantage of high accuracy. The usual guarantee on such
instruments by the manufacturers is less than 1 percent of scale range.
Copper
A A Copper wire
wire
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Figure 8.1: Keep reference junction with ice Figure 8.2: Keep reference junction with bridge circuit
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TD 005 Temperature Measurement Bench
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TD 005 Temperature Measurement Bench
electric lamp. In this later type, if the lamp filament and the object are both in focus in the same
field, the filament will disappear when the current has been adjusted to give the filament the same
brightness as the object. This type of instruments was used to determine the international
temperature scale above the gold point.
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TD 005 Temperature Measurement Bench
2.2.9 Psychrometer (wet and dry bulb thermometers)
The combined wet- and dry-bulb dual ordinary mercury thermometer called "psychometer" is most
widely used for air humidity measurement. The dry-bulb thermometer gives a room or atmospheric
air temperature where as the wet-bulb gives a saturation temperature of water which is
corresponded to the dew point. The radiation from surrounding warmer surfaces tends to make the
wet-bulb thermometer read higher than actual saturation temperature; therefore this is offset by the
velocity of air flow over the wet-bulb. This velocity for correction can be offset by velocity of air flow
over the wet-bulb. At 270-300 m/min the effect balances.
This velocity is set up by a fan blowing over the wet-bulb in the case of a stationary type
psychometer or by swinging the wet-bulb vigorously in the case of sling type psychometer.
The humidity measurement is then determined from the humidity chart as shown in Fig. 13.
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TD 005 Temperature Measurement Bench
2.4 Errors Associated with Incorrect Application
2.4.1 Accuracy of Temperature Instruments
The accuracy of temperature measurement depends on instrument and on method of application.
Almost any required degree of accuracy in scale and calibration may be obtained with glass -
stem thermometers, electrical-resistance thermometers, or thermocouples, but large errors may be
introduced by improper application. Most of these errors are due to
• Stratification or poor mixing of the fluid,
• Radiation, and
• Incomplete immersion or conduction.
As the ambient temperature increases, these errors become greater.
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TD 005 Temperature Measurement Bench
where FG is a geometric factor and F€ is a radiation factor.
As illustrated in Fig. 14, a thermocouple junction is installed in the flat plate whose temperature is to
be measured. The plate is exposed to a convection environment on both sides and the
thermocouple wires are also exposed to the same environment.
0.8
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0.6
Tf-Tp
Ti-Tp
0.4
0.2
0
0.01 0.1 1 10
k
K
Figure 15: Temperature-compensation curves for installation as per Fig. 14.
The thermocouple wires are covered with insulating materials as shown. If the plate temperature is
higher than the convection environment, heat will be conducted along the thermocouple wire and
the temperature of the junction will be lower than the true plate temperature. An analytical solution
to this problem is given in Fig. 15. This solution neglects radiation heat-transfer effects. The
nomenclature for the parameters in Fig. 15 is as follows:
h1, h2 = convection heat-transfer coefficients on the sides of the plate as indicated, W/m²K
ht = convection heat-transfer coefficient from each of the thermocouple wires, W/m²K
k = thermal conductivity of the plate material, W/mK
= plate thickness, m
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TD 005 Temperature Measurement Bench
Tf = fluid temperature surrounding the thermocouple wire, K
Ti = temperature indicated by the thermocouple, K
Tp = true plate temperature (at a large distance away from the thermocouple junction), K
1
h h2 2
m 1 m-1 (7)
k
3 1
K 2 k A 2 k B 2 rt 2 i W/K
1 3
(8)
ht k i
where, kA and kB are the thermal conductivities of the two thermocouple materials, i is the thickness
of the thermocouple insulation, and ki is the thermal conductivity of the insulation.
If the solid is a relatively massive one, the temperature correction can be made in accordance with
calculations is presented in graphical form in Fig. 16. In this figure k is the thermal conductivity of
the solid, r is the radius of the wire or 2 times the radius for two wires, L is the length of the
thermocouple leads, hs is the convection heat-transfer coefficient between the solid and the fluid, kA
is the equivalent conductivity area product for axial conduction in the wire, and R is the radial
thermal resistance of the wire, insulation, and convection to the fluid. For a wire of radius rw,
covered by a layer of insulation having an outside radius rt and thermal conductivity ki the value of R
is calculated from
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r
ln i
1
w
r
R (9)
h2ri 2k i
where, h is the convection heat-transfer coefficient from the outside of the insulation to the fluid. We
should note that the length L is sufficiently long in many applications to make the hyperbolic tangent
term unity in the equation for X in Fig. 16.
The term Bi=hsr/k is called the Biot number of Biot modulus and is important in heat transfer
applications which involve combined conduction-convection systems like the thermocouple
installations illustrated here. This parameter indicates the relative magnitude of the resistance to
heat transfer resulting from convection to the resistance to heat transfer from conduction. Large
values of Bi indicate just the opposite. The function F (Bi) in Fig. 16 is an approximation and can be
extended somewhat beyond the range of Bi < 1.0; however, larger values of Bi would indicate a
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TD 005 Temperature Measurement Bench
large effect of convection and thus a larger temperature error. In these cases, the installation should
be modified.
The conduction lead error may be reduced by laying the wire along the solid to reduce the
temperature gradient. Obviously, the wire must be electrically insulated from the solid if the solid is
a metal.
Example 1: Conduction error for thermocouple.
A copper-constantan thermocouple is attached to a 1/16” thick stainless-steel plate [k=35Btu/h.ft] as
shown in Fig. 14. The diameter of the wires is 0.04”, and the following estimates are made of the
significant heat-transfer parameters:
h1 = 4.0 Btu/h.ft².°F
h2 = 2.5 Btu/h.ft².°F
ht = 20 Btu/h.ft².°F
hA = 14 Btu/h.ft².°F
hB = 220 Btu/h.ft².°F
Tf = 500 Btu/h.ft².°F
The thermocouple wires are coated with an electrically insulating lacquer which may be considered
negligibly thin insofar as heat transfer is concerned. The plate is cooled on the side opposite the
thermocouple installation, and the thermocouple indicates a temperature of 300°F. Calculate the
true plate temperature.
Solution: we observe that
1
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in 0.0071 ft
16
rt = 0.02 in = 0.00167 ft
i ≈ 0
Ti = 300°F
From Eqn. (7):
4.0 2.5 1 2
m 3.62
350.0142
From Eqn. (8):
0.00167
1 2
12 12 32 1
K 2 14 220 0 0.0251
20
The parameters for use with Fig. 15 are thus
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TD 005 Temperature Measurement Bench
300 – Tp = (0.08)(500 – Tp), and Tp = 282.6 °F
The thermocouple conduction error is Ti-Tp = 17.4°F. This error could be reduced by either using
smaller thermocouple wires or insulating the wires.
Example 2: Error in low-conductivity solid.
A thermocouple wire having an effective diameter of 1.5mm is attached to a ceramic solid having
the properties of: =2500kg/m³, c=0.7kJ/kg.K, and k=0.9W/m.K. The thermocouple has an effective
conductivity of 80W/m.K. The wire is very long and essentially bare, with a convection coefficient of
250W/m².K. The convection coefficient hs is 20W/m².K. Calculate the true plate temperature when
the thermocouple indicates 200°C and the fluid temperature is 90°C.
Solution: we make use of Fig. 16 and Eqn. (9) and calculate the quantities
1 1
R 0.849
h2ri 2502 0.75 10 3
k A 80 0.75 10 3
2
1.414 10 4
Because L ∞ 1.0, and
X
kA / R
1.414 10 4 0.208
12
X
kA / R
1.414 10 4 0.849
12
0.0274
rk
0.75 10 3 200
Bi
hs r 250 0.75 10 3
9.36 10 4 ; F Bi 1.271
k 200
Then,
T p Ti 0.0274 9.36 10 4
0.0204
Tp T f 0.0274 1.271
And Tp = 202.3°C
Of course, this indicates the extreme importance of the conductivity of the solid to the measurement
error.
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TD 005 Temperature Measurement Bench
2.6 Transient Response of Thermal Systems
When a temperature measurement is to be made under non-steady-state conditions, it is important
that the transient response characteristics of the thermal system be taken into account. Consider
the simple system shown in Fig. 17. The thermometer is represented by the mass m and specific
heat c and is suddenly exposed to a convection environment of temperature T∞. The convection
heat-transfer coefficient between the thermometer and fluid is h, and radiation heat transfer is
assumed to be negligible. It is also assumed that the thermometers substantially uniform in
temperature at any instant of time; i.e., the thermal conductivity of the thermometer material is
sufficiently large in comparison with the surface conductance because of the convection heat-
transfer coefficient. The energy balance for the transient process may be written as
hAT T mc
dT
(10)
d
For this equation appropriate units are:
h in W/m².K
A in m²
T in K
m in kg
c in J/kg.K
in s or h
The temperature of the thermometer as a function of time can be expressed as:
T T
e hA mc (11)
T0 T
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where, T0 is the thermometer temperature at time zero. The time constant for the system in Fig. 17
is:
mc
(12)
hA
dT
q hA(T T) mc
dτ
T, m, c
Surface area,A
Figure 17: Simple thermal system exposed to a sudden change in ambient temperature
When the heat-transfer coefficient is sufficiently large, there may be substantial temperature
gradients within the thermometer itself and a different time.
To indicate the approximate response times for semi-infinite solids, Fig. 18 and Fig. 19 show the
surface temperature rises to be expected from different heat-flux inputs. The approximate signal
outputs from resistance thermometers and different thermocouple materials are also indicated.
These figures may be used to estimate when transient effects become important.
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TD 005 Temperature Measurement Bench
Figure 18: Surface temperature rise for semi-infinite insulating solids subjected to constant surface heat fluxes between 1
W/m² and 10 kW/m². Signal levels to be expected from platinum and gold resistance thermometers and chromel-alumel
thermocouples are also indicated.
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Figure 19: Surface temperature rise for semi-infinite metallic solids subjected to constant heat fluxes between 1 W/m² and
10 kW/m². Signal levels to be expected from chromel-alumel-constantan and copper-constantan thermocouples are also
indicated.
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TD 005 Temperature Measurement Bench
2.7 Thermocouple Compensation
Suppose a thermocouple is used to measure a transient temperature variation. The response of the
thermocouple will be dependent on several factors, as outlined above, and will follow a variation like
that of Eqn. (11) when subjected to a step change in environment temperature. If a compensating
electric network is applied to the system, it is possible to increase the frequency response of the
thermocouple. The disadvantage of the compensating network is that it reduces the thermocouple
output; however, if the measuring instrument is sufficiently sensitive, this problem is not too critical.
Rc
Thermocouple Ei C R Output
input
A typical thermocouple-compensation network is shown in Fig. 20. The thermocouple input voltage
is represented by Ei, the output voltage is represented by Eo. This particular network will attenuate
low frequencies more than high frequencies and has a frequency response to a step input that is
approximately opposite to that of a thermocouple. The network and thermocouple may thus be used
in combination to produce a more nearly flat response over a wide frequency range. The output of
the network is given by:
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Eo 1 j c
(13)
Ei 1 j c
R
where,
R Rc
c Rc C
frequency of the input signal
j 1
The amplitude response is given by the absolute value of the function in Eqn. (13). Thus
Eo 1 2 c2
(14)
Ei amplitude 1 2 2 c2
The high-frequency compensation of the network is improved as the value of is decreased, but
this brings about a decreased output since the steady-state output is:
Eo R
(15)
Ei steady state R Rc
In practice, the compensating circuit is usually designed so that c is equal to the time constant for
the thermocouple. Variable resistors may be used to change the compensation with a change in
thermal environment condition.
The overall problem we have described above is one of compensating a thermocouple output so
that higher-frequency response may be obtained.
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TD 005 Temperature Measurement Bench
1.0
0.8
-45o slope
0.6
0.4
0.2
T-T 0.1
To-T 0.08
0.06
0.04
0.02
0.01
0.01 0.02 0.06 0.1 0.2 0.4 0.6 1.0 10
T
2
Figure 21: Thermocouple response to step change in environmental temperature
The step response of the thermocouple given by Eqn. (11) will hold, of course, only for the
conditions described. Therefore, the compensating network of Fig. 20 will achieve the desired
objectives in varying degrees, depending on the exact thermal environment to which the
thermocouple is exposed. Let us examine the thermocouple and compensating-network response
in more detail. Fig. 21 shows the thermocouple response to a step change in temperature of the
environment T∞. We assume that the voltage output of the thermocouple is directly proportional to
temperature over this range so that the voltage output would also follow a similar curve.
Eo
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Ei ( 0.1)
Eo 0.1
Ei
0.01
0.1 1.0 10 100
Tc
Figure 22: response of the network in Fig. 20 for a step voltage input with =0.1
In Fig. 22 we have plotted the output voltage of the compensating network for a step-voltage input
and for =0.1. The thermocouple response is obtained by solving the electric-network equivalent of
the thermocouple. In that network the thermal capacitance is analogous to electric capacitance, and
the convection heat-transfer coefficient is analogous to thermal or electric resistance. If Fig. 21 and
Fig. 22 are added together, we obtain the plot shown in Fig. 23, where the response is shown for
different values of the ratio c/ for c/>1, the response curve “overshoots” the steady-state voltage
ratio of 0.1. It is clear that the curve =c offers a broader frequency response than the
uncompensated curve. Careful inspection will also show that some overshoot can be desirable. The
curve for c/=1.1 indicates a substantial extension of the frequency response within a plus or minus
range of about 5%. Excessive overshoot, of course, gives a decided nonlinear response. Optimal
dynamic response of the network will be obtained when c/≈1.1, provided the thermocouple input
behaves nicely. In practice, variable resistors will be provided in the circuit to adjust the
compensation in accordance with the actual variation in the thermal environment.
We note again that the foregoing discussion pertains a step-function input, and the actual input may
be markedly different. In practice, one should make the thermocouple as small as possible and
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TD 005 Temperature Measurement Bench
calibrate against some known transient temperature. Adjustments to the network can be made to
obtain the best calibration.
No compensation
1.5
Tc / T = 2
1.1
Eo
0.1
Ei
T= Tc
0.01
0.1 1.0 10 100
T
Figure 23: Combined response of thermocouple and compensating network to step change in environment temperature
be taken as those of iron (=7900 kg/m³, c=450 J/kg.K). Estimate the time constant for the
thermocouple.
Solution:
We use Eqn. (12) to calculate the time constant with,
4
m V r 3
3
2
A 4r
So,
43 r 3c
79004500.75 10 3 11.85 s
h4r 2 375
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TD 005 Temperature Measurement Bench
Then, C = 11.85/106 = 1.185 x 10-5 = 11.85 µF. Using the above value of Rc we obtain
R = 0.111 M.
A more practical set of values would be,
C = 10 µF
Rc = 1.185 M
R = 0.132 M
Reference:
Holman JP, Experimental Methods of Engineers, 6th ed., New York: McGraw-Hill, 1994.
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3. Experimental Procedures
3.1 0°C Test
3.1.5 Connect the sensor cable for PT100, type-K thermometer and thermistor to their respective
indicators according to the colours of the terminals.
3.1.6 Wait until the readings are stable, e.g., 2 minutes. Check that the thermometer indicator
reads 0°C. If not, adjust zero on the temperature indicators. (no adjustment for
millivoltmeter).
3.1.7 Record all thermometer readings.
3.1.8 Remove type-K thermocouple sensor from its indicator and connect it to the millivoltmeter
and record the milli-volt reading.
3.1.9 Fill the wet bulk temperature pot, wait until the temperature readings are stable, and record
the wet and dry bulb temperatures.
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3.3 Water Temperature (0-100°C)
3.3.1 Pour the ice water into the stainless-steel pot to near full and place the pot on the hot
plate.
3.3.2 Place the thermometer plate across the top of the pot.
3.3.3 Stir the pot well. If temperature is well below 10°C by mercury in glass reading, turn on the
hot-plate until the temperature reaches 10°C.
3.3.4 Remove the pot from the hot plate and keep stirring, then record all thermometers
readings after the readings are stable or after 2 minutes.
3.3.5 Switch the Type-K thermocouple sensor to millivoltmeter and record the reading.
Note: Convert the Type-K thermocouple sensor to millivoltmeter and record the reading.
3.3.6 Put the pot back onto the hot plate and heat it to about 20°C and repeat steps 3.3.4 and 3.3.5
3.3.7 Repeat step 3.3.6 every 10°C interval until the temperature reaches boiling point (100 °C).
Switch off the hot plate after all readings have been taken.
3.4.1 Remove the thermometer plate from the water pot and place in on a provided stainless-
steel temperature plate stand.
3.4.2 Put the hot air blower on a stand and tighten it with a wing bolt.
3.4.3 Place a liquid-in-glass thermometer on the thermometer plate by hand and adjust the stand
such that the thermometer is at the centre of the air stream.
3.4.4 Turn on the blower and adjust the distance between the blower and the thermometer such
that the thermometer reads a required temperature, e.g. 110°C, after about 2 minutes.
Record the thermometer reading.
3.4.5 Replace the liquid-in-glass thermometer with another type and record the reading after 2
minutes.
3.4.6 Repeat step 3.4.5 for all thermometers.
3.4.7 Put the liquid-in-glass thermometer back on the thermometer plate. Move the stand closer
to the blower such that the temperature reading is 120°C and record the reading.
3.4.8 Repeat steps 3.4.5 and 3.4.6
3.4.9 Repeat steps 3.4.7 and 3.4.8 at higher temperatures.
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3.5 Alternative Test for Room Temperature to Above 10°C
Flushing oil, which is available at petrol stations, is used in the provided oil pot. The flushing oil
has a flash point well above 200°C. It is recommended that the test can be carried out up to 200°C
using this oil. Procedure is the same as in section 3.3.
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Remarks
1. Temperature reading of PT100 and thermistor can be taken by millivoltmeter in the same
way as in the case of type-K thermocouple by using different charts (Addendum 1 and 3).
2. Note that the temperature reading should be 0°C on ice water and should be 100°C on
boiling water.
If the reading is not 0°C or 100°C, reading error should be considered as deviation which
should be adjusted for other temperature readings on the same thermometer.
3. The thermometers supplied under this experiment has not have not been calibrated and
certified by a recognised authority. Therefore, if two thermometer readings do not agree,
we can not say which one is correct unless they are compared to a calibrated thermometer.
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4. RESULTS
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DATA SHEET
TD 005 TEMPERATURE MEASURING BENCH
Experiment: Comparison of thermometer readings
Tested by: ……………………………… Date: ………………..
° ° ° °
Sling psychrometer readings: Beginning of demonstration: Wet-bulb …… C; Dry-bulb …… C End of demonstration: Wet-bulb …… C; Dry-bulb …… C
Ice water Warm water Hot oil
° ° °
Precision resister: 100 reading = ……. C, 10 k reading = …… C, 1 k reading = …… C
°
K- type thermocouple Temperature readings, C
(1) (2) (3) (4) (5)
Glass thermometer
° Potential ° Platinum Vapour Strip Remarks
C Temp. C Bimetallic
voltage, mV resistance Thermistor pressure Temp.
Temp.
Temp. Temp. indicator
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TD 005 Temperature Measurement Bench
DATA SHEET
TD 005 TEMPERATURE MEASURING BENCH
Tested by: ……………………………… Date: ………………..
Experiments
°
A. Dynamic response (temperature drop from room temperature to 0 C).
B. Incorrect application (degree of immersion). Low and High
Temperature (°C)
Temperature
and time
Remark
0s 10 s 20 s 30 s 40 s 50 s 60 s 70 s 80 s 90 s 100 s 110 s 120 s
Thermometer
and immersion
Liquid in glass
Low
High
Bimetallic
Low
High
Vapour pressure
Low
High
PT 100
Low
High
Type K
Low
High
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Thermistor
Low
High
Type K with
Millivoltmeter
Low
High
Note
Immersion High = ………….mm, Low = ………….mm
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TD 005 Temperature Measurement Bench
DATA SHEET
TD 005 TEMPERATURE MEASURING BENCH
Experiment: Comparison of thermometer readings
Tested by: ……………………………… Date: ……01.06.2006
° ° ° °
Sling psychrometer readings: Beginning of demonstration: Wet-bulb 29 C; Dry-bulb 30 C End of demonstration: Wet-bulb 29 C; Dry-bulb 30.5 C
Ice water Warm water Hot oil
° ° °
Precision resister: 100 reading = …1. C, 10 k reading = 24.3 C, 1 k reading = 97.3 C (Thermistor)
°
K- type thermocouple Temperature readings, C
(1) (2) (3) (4) (5)
Glass thermometer
° Potential ° Platinum Vapour Strip Remarks
C Temp. C Bimetallic
voltage, mV resistance Thermistor pressure Temp.
Temp.
Temp. Temp. indicator
0.0 -1.18 0 -0.03 -0.6 0.0 2.0 - After 5 minutes (in ice box)
10.0 -0.81 9.7 8.9 9.1 10.0 11.0 - After 2 minutes
20.5 -0.41 19.6 19.5 19.4 20.0 20.0 - After 2 minutes
31.5 0.00 30.0 29.2 30.0 31.0 30.8 - After 2 minutes
41.0 0.35 39.4 38.5 38.6 41.0 40.0 - After 2 minutes
50.5 0.74 47.9 47.5 48.2 50.0 49.0 - After 2 minutes
60.5 1.17 57.8 56.1 57.6 60.0 58.0 - After 2 minutes
70.5 1.57 69.3 67.0 66.9 70.0 66.0 - After 2 minutes
80.0 1.97 76.4 75.5 76.2 80.0 75.0 - After 2 minutes
89.8 2.26 85.4 86.7 84.4 88.0 84.0 - After 2 minutes
99.4 2.76 97.0 95.2 94.6 99.0 93.0 - After 2 minutes
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TD 005 Temperature Measurement Bench
DATA SHEET
TD 005 TEMPERATURE MEASURING BENCH
Experiment: Comparison of thermometer readings
Tested by: ……………………………… Date: 01.06.2006
° ° ° °
Sling psychrometer readings: Beginning of demonstration: Wet-bulb …… C; Dry-bulb …… C End of demonstration: Wet-bulb …… C; Dry-bulb …… C
Ice water Warm water Hot oil
° ° °
Precision resister: 100 reading = …1 C (PT100), 10 k reading = 24.3 C (Thermistor), 1 k reading = 97.3 C (Thermistor)
°
K- type thermocouple Temperature readings, C
(1) (2) (3) (4) (5)
Glass thermometer
° Potential ° Platinum Vapour Strip Remarks
C Temp. C Bimetallic
voltage, mV resistance Thermistor pressure Temp.
Temp.
Temp. Temp. indicator
100.5 2.89 97.3 100.1 - 100.0 91 - After 2 minutes
111.0 3.00 104.4 106.2 - 111.0 97 - After 2 minutes
120.5 3.35 114.2 117.2 - 120.0 105 - After 2 minutes
130.0 3.92 124.2 128.0 - 130.0 112 - After 2 minutes
140.0 4.27 133.8 135.1 - 139.8 122 - After 2 minutes
150.0 4.64 144.1 145.5 - 149.6 131 - After 2 minutes
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TD 005 Temperature Measurement Bench
DATA SHEET
TD 005 TEMPERATURE MEASURING BENCH
Tested by: ……………………………… Date: 01.06.2006
Experiments
°
A. Dynamic response (temperature drop from room temperature to 0 C).
B. Incorrect application (degree of immersion). Low and High
Temperature (°C)
Temperature
and time
Remark
0s 10 s 20 s 30 s 40 s 50 s 60 s 70 s 80 s 90 s 100 s 110 s 120 s
Thermometer
and immersion
Liquid in glass
Low 27 4 2 1 1 0.5 0.5 0 0 0 0 0 0
High 27 4 3 2.5 1 0.5 0.5 0 0 0 0 0 0
Bimetallic
Low 29 20 4 3.5 2.5 2.0 1.5 1.5 1.0 1.0 1.0 1.0 1.0
High 29 6 4 2.5 2 1.5 1.5 1.0 1.0 1.0 1.0 0.5 0.5
Vapour pressure
Low 27 30 19 18 18 16 16 16 16 16 15 15 15
High 21 13 11 11 10 10 10 10 10 10 9 9 9
PT 100
Low 27.4 7.6 3.8 2.4 2.0 1.9 1.7 1.5 1.4 1.5 1.5 1.4 1.4
High 27.3 7.2 3.8 2.5 2.0 1.6 1.5 1.4 1.3 1.2 1.1 1.2 1.1
Type K
Low 27.4 7.6 3.8 2.4 2.0 1.9 1.7 1.5 1.4 1.5 1.5 1.4 1.4
High 27.3 7.2 3.8 2.5 2.0 1.6 1.5 1.4 1.3 1.2 1.1 1.1 1.1
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Thermistor
Low 25.1 9.0 5.3 3.5 3.2 3.0 2.9 2.8 2.7 1.6 1.6 1.6 1.6
High 23.8 7.8 3.5 3.5 2.7 2.2 2.0 1.7 1.6 1.0 0.9 0.8 0.8
Type K Milli-
voltmeter (mV)
Low -0.041 -0.659 -0.939 -1.060 -1.100 -1.116 -1.118 -1.123 -1.139 -1.153 -1.165 -1.177 -1.185
High -0.044 -0.754 -0.963 -1.058 -1.099 -1.129 -1.144 -1.155 -1.164 -1.170 -1.175 -1.178 -1.181
Type K
converted to °C
Low 28.98 13.68 6.67 3.62 2.60 2.20 2.15 2.03 1.63 1.28 0.97 0.67 0.46
High 28.98 11.30 6.05 3.67 2.63 1.88 1.50 1.23 1.00 0.85 0.72 0.64 0.56
Note: Immersion High = about 7 mm, Low = about 2 mm
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TD 005 Temperature Measurement Bench
Observations
1. From the test data for section 3.5, it is noted that different devices reach their final
temperature at different times. In a normal reading where temperatures change, 1-2 minutes
should be allowed before the temperatures are recorded. Dynamic response is different for
different thermometers.
2. Less immersion no only results in slow arrival at final temperature but also incorrect final
temperature reading. Different types of thermometers show different degrees of error.
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TD 005 Temperature Measurement Bench
5. SAMPLE GRAPHS
Dynamic Response
Vapour Pressure Thermometer
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Dynamic Response
(Bimetallic Thermometer)
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Dynamic Response
(Thermocouple Type K)
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Dynamic Response
(Thermistor)
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Dynamic Response
(Thermocouple Type K)
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Dynamic Response
(Mercury-in-glass Thermometer)
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Dynamic Response
(Platinum resistant Thermometer, PT100)
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110 142.29 142.66 143.04 143.42 143.80 144.17 144.55 144.93 145.31 145.68 146.06
120 146.06 146.44 146.81 147.19 147.57 147.94 148.32 148.70 149.07 149.45 149.82
130 149.82 150.20 150.57 150.95 151.33 151.70 152.08 152.45 152.83 153.20 153.58
140 153.58 153.95 154.32 154.70 155.07 155.45 155.82 156.19 156.57 156.94 157.31
150 157.31 157.69 158.06 158.43 158.81 159.18 159.55 159.93 160.30 160.67 161.04
160 161.04 161.42 161.79 162.16 162.53 162.90 163.27 163.65 164.02 164.39 164.76
170 164.76 165.13 165.50 165.87 166.24 166.61 166.98 167.35 167.72 168.09 168.46
180 168.46 168.83 169.20 169.57 169.94 170.31 170.68 171.05 141.42 171.79 172.16
190 172.16 172.53 172.90 173.26 173.63 174.00 174.37 174.74 175.10 175.47 175.84
200 175.84 176.21 176.57 176.94 177.31 177.68 178.04 178.41 178.78 179.14 179.51
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TD 005 Temperature Measurement Bench
Sample Calculations
Thermocouple Type K
At 10 s display:
Low = -0.659
High = -0.754
Tare is a the reading at room temperature.
Room temperature = 30°C, Thermoelectric voltage in millivolt from the table (Addendum 2) is
1.203mV.
Thus the corrected voltage is:
Low = 1.203 – 0.659 = 0.544
High = 1.203 – 0.754 = 0.499
From thermoelectric voltage in Millivolt table at:
Low = 13.68°C
High = 11.30°C
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TD 005 Temperature Measurement Bench
-24 84.85 82.26 79.74 31 8.112 8.014 7.817 86 1.433 1.411 1.370
-23 80.76 78.33 75.96 32 7.826 7.728 7.631 87 1.415 1.373 1.333
-22 76.89 74.61 72.39 33 7.551 7.454 7.358 88 1.377 1.336 1.296
-21 73.23 71.10 68.02 34 7.288 7.192 7.096 89 1.341 1.300 1.261
-20 69.77 67.77 65.82 35 7.035 6.940 6.845 90 1.305 1.266 1.228
-19 66.44 64.57 62.74 36 6.793 6.699 6.605 91 1.271 1.232 1.195
-18 63.30 61.54 59.83 37 6.360 6.497 6.375 92 1.238 1.200 1.163
-17 60.33 58.68 57.07 38 6.337 6.245 6.154 93 1.205 1.168 1.132
-16 57.51 55.97 54.47 39 6.123 6.032 5.942 94 1.174 1.137 1.102
-15 54.85 53.41 51.99 40 5.918 5.827 5.738 95 1.144 1.108 1.073
-14 52.33 50.98 49.65 61 5.718 5.629 5.541 96 1.115 1.079 1.045
-13 49.95 48.68 47.43 42 5.526 5.438 5.351 97 1.086 1.051 1.018
-12 47.69 46.50 45.33 43 5.342 5.255 5.169 98 1.059 1.024 0.9914
-11 45.55 44.43 43.33 44 5.165 5.080 4.993 99 1.032 0.9984 0.9659
-10 43.52 42.47 41.44 45 4.995 4.911 4.827 100 1.006 0.9731 0.9412
-9 41.55 40.57 39.60 46 4.832 0.749 4.666 101 0.9808 0.9489 0.9171
-8 39.69 38.77 37.86 47 4.675 4.593 4.512 102 0.9563 0.9246 0.8938
-7 37.82 37.06 36.21 48 4.524 4.443 4.363 103 0.9326 0.9014 0.8712
-6 36.25 35.44 34.64 29 4.379 4.299 4.22 104 0.9096 0.8789 0.8402
-5 34.66 33.90 33.15 50 4.239 4.160 4.083 105 0.8873 0.8572 0.8280
-4 33.15 32.44 31.74 51 4.103 4.026 3.949 106 0.8656 0.836 0.8074
-3 31.72 31.05 30.39 52 3.972 3.896 3.821 107 0.8446 0.8155
-2 30.36 29.73 29.11 53 3.846 3.771 3.697 108 0.8242 0.7956
-1 29.06 28.40 27.90 54 3.725 3.651 3.579 109 0.8044 0.7763
0 27.83 27.28 26.74 55 3.609 3.536 3.464 110 0.7851 0.7576
1 26.65 26.13 25.62 56 3.496 3.425 3.354
2 25.52 25.03 24.56 57 3.388 3.318 3.249
3 24.44 23.99 23.54 58 3.284 3.215 3.147
4 23.42 23.00 22.58 59 3.184 3.116 3.049
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