‫ﻫﻴﺌﺔ ﺍﻝﺘﻘﻴﻴﺱ ﻝﺩﻭل ﻤﺠﻠﺱ ﺍﻝﺘﻌﺎﻭﻥ ﻝﺩﻭل ﺍﻝﺨﻠﻴﺞ ﺍﻝﻌﺭﺒﻴﺔ‬

STANDARDIZATION ORGANIZATION FOR G.C.C (GSO)

GSO ISO 1067 :1994

ISO 1067:1974

‫ﺘﺤﻠﻴل ﺍﻝﺼﺎﺒﻭﻥ ـ ﺘﻘﺩﻴﺭ ﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻭﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ‬
‫ﻭﺍﻝﻤﻭﺍﺩ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ‬
ANALYSIS OF SOAPS – DETERMINATION OF
UNSAPONIFIABLE, UNSAPONIFIED AND
UNSAPONIFIED SAPONIFLABLE MATTER

ICS: 71.100
‫ﺘﺤﻠﻴل ﺍﻝﺼﺎﺒﻭﻥ ـ ﺘﻘﺩﻴﺭ ﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻭﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ‬
‫ﻭﺍﻝﻤﻭﺍﺩ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ‬

‫‪1415/06/13‬ﻫـ )‪(1994/11/16‬‬ ‫‪:‬‬ ‫ﺘــﺎﺭﻴﺦ ﺍﻻﻋﺘﻤــﺎﺩ ﻤــﻥ ﻤﺠﻠــﺱ ﺍﻹﺩﺍﺭﺓ‬

‫ﻻﺌﺤﺔ ﻓﻨﻴﺔ‬ ‫‪:‬‬ ‫ﺼﻔﺔ ﺍﻻﺼﺩﺍﺭ‬
‫‪GSO ISO 1067 :1994‬‬ ‫ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ‬

‫ﻤﻘﺩﻤﺔ‬

‫ﻗﺎﻤﺕ ﻫﻴﺌﺔ ﺍﻝﺘﻘﻴﻴﺱ ﻝﺩﻭل ﻤﺠﻠﺱ ﺍﻝﺘﻌﺎﻭﻥ ﻝﺩﻭل ﺍﻝﺨﻠﻴﺞ ﺍﻝﻌﺭﺒﻴﺔ ﺒﺘﺒﻨـﻲ ﺍﻝﻤﻭﺍﺼـﻔﺔ ﺍﻝﻘﻴﺎﺴـﻴﺔ ﺍﻝﺩﻭﻝﻴـﺔ‬
‫‪" 1064:1974‬ﺘﺤﻠﻴل ﺍﻝﺼﺎﺒﻭﻥ – ﺘﻘﺩﻴﺭ ﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻭﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ ﻭﺍﻝﻤﻭﺍﺩ ﺍﻝﻘﺎﺒﻠﺔ‬
‫ﻝﻠﺘﺼﺒﻥ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ" ﺍﻝﺘﻲ ﺃﺼﺩﺭﺘﻬﺎ "ﺍﻝﻤﻨﻅﻤﺔ ﺍﻝﺩﻭﻝﻴﺔ ﻝﻠﺘﻘﻴﻴﺱ" ﻭﺘﻤﺕ ﺘﺭﺠﻤﺘﻬﺎ ﺇﻝـﻰ ﺍﻝﻠﻐـﺔ ﺍﻝﻌﺭﺒﻴـﺔ‬
‫ﻭﺍﻋﺘﻤﺩﺕ ﻜﻤﻭﺍﺼﻔﺔ ﻗﻴﺎﺴﻴﺔ ﺨﻠﻴﺠﻴﺔ ﺩﻭﻥ ﺇﺩﺨﺎل ﺃﻴﺔ ﺘﻌﺩﻴﻼﺕ ﻓﻨﻴﺔ ﻋﻠﻴﻬﺎ ‪.‬‬

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‫‪GSO ISO 1067 :1994‬‬ ‫ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ‬

‫ﺘﺤﻠﻴل ﺍﻝﺼﺎﺒﻭﻥ‬
‫ﺘﻘﺩﻴﺭ ﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ‪ ،‬ﻭﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ‬
‫ﻭﺍﻝﻤﻭﺍﺩ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ‬

‫ﺍﻝﻤﺠﺎل‬ ‫‪-1‬‬

‫ﺘﺨﺘﺹ ﻫﺫﻩ ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺒﻁﺭﻴﻘﺔ ﺘﻘﺩﻴﺭ ﻤﺤﺘﻭﻯ ﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ‪ ،‬ﻭﺍﻝﻤﻭﺍﺩ‬
‫ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ ﻭﺍﻝﻤﻭﺍﺩ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ ﻓﻲ ﺍﻝﺼﺎﺒﻭﻥ ﺍﻝﻌﺎﺩﻱ‪ ،‬ﻭﻻ ﺘﺨﺘﺹ‬
‫ﺒﻤﻨﺘﺠﺎﺕ ﺍﻝﺼﺎﺒﻭﻥ ﺍﻝﻤﺭﻜﺒﺔ ‪.‬‬

‫ﻨﻁﺎﻕ ﺍﻝﺘﻁﺒﻴﻕ‬ ‫‪-2‬‬

‫ﺘﺴﺘﺨﺩﻡ ﻫﺫﻩ ﺍﻝﻁﺭﻴﻘﺔ – ﻝﺘﻘﺩﻴﺭ ﻤﺤﺘﻭﻴﺎﺕ ﺍﻝﻤﻨﺘﺠﺎﺕ – ﺒﺨﻼﻑ ﺍﻷﺤﻤﺎﺽ ﺍﻝﺩﻫﻨﻴﺔ ﺍﻝﻁﻠﻴﻘﺔ –‬
‫ﺍﻝﺘﻲ ﺘﺫﻭﺏ ﻓﻲ ﺍﻝﻬﻜﺴﺎﻥ ﺃﻭ ﺍﻝﻤﺴﺘﻘﻁﺭ ﺍﻝﺒﺘﺭﻭﻝﻲ ﺍﻝﺨﻔﻴﻑ )ﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻭﺍﻝﻤﻭﺍﺩ‬
‫ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ( ‪ ،‬ﻭﺘﻠﻙ ﺍﻝﺘﻲ ﻴﻤﻜﻥ ﺘﺼﺒﻨﻬﺎ )ﺍﻝﻤﻭﺍﺩ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ( ‪ .‬ﻭﻻ‬
‫ﺘﺴﺘﺨﺩﻡ ﻓﻲ ﺤﺎﻝﺔ ﺍﻝﺼﺎﺒﻭﻥ ﺍﻝﺫﻱ ﻴﺤﺘﻭﻱ ﻋﻠﻰ ﻨﺴﺒﺔ ﻜﺒﻴﺭﺓ ﻤﻥ ﺍﻻﺴﺘﻴﺭﻭﻻﺕ ﺃﻭ ﺍﻝﻜﺤﻭﻻﺕ ‪،‬‬
‫ﻁﻭﻴﻠﺔ ﺍﻝﺴﻠﺴﻠﺔ ‪ ،‬ﺃﻭ ﺍﻝﺼﺎﺒﻭﻥ ﺍﻝﺫﻱ ﻴﺤﺘﻭﻱ ﻋﻠﻰ ﺭﻭﺍﺌﺢ ﻋﻁﺭﻴﺔ ‪.‬‬

‫ﺃﺴﺎﺱ ﺍﻝﻁﺭﻴﻘﺔ‬ ‫‪-3‬‬

‫ﺘﺴﺘﺨﻠﺹ ﺍﻝﻤﻭﺍﺩ ﺍﻝﺘﻲ ﺘﺫﻭﺏ ﻓﻲ ﺍﻝﻬﻜﺴﺎﻥ ﻭﺘﻌﺎﻴﺭ ﺍﻷﺤﻤﺎﺽ ﺍﻝﺩﻫﻨﻴﺔ ﺍﻝﻁﻠﻴﻘﺔ ﺍﻝﻤﺴﺘﺨﻠﺼﺔ‬
‫ﺒﻤﺤﻠﻭل ﻫﻴﺩﺭﻭﻜﺴﻴﺩ ﺒﻭﺘﺎﺴﻴﻭﻡ ﻝﺘﺘﺼﺒﻥ ﻭﺘﺒﻘﻰ ﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﺫﺍﺌﺒﺔ ﺒﺎﻝﻬﻜﺴﺎﻥ‪.‬‬

‫ﺍﻝﻜﻭﺍﺸﻑ‬ ‫‪-4‬‬

‫ﻴﺠﺏ ﺃﻥ ﻴﻜﻭﻥ ﺍﻝﻤﺎﺀ ﺍﻝﻤﺴﺘﺨﺩﻡ ﻤﻘﻁﺭﹰﺍ ﺃﻭ ﻤﺎﺀ ﻴﻜﺎﻓﺌﻪ ﻓﻲ ﺍﻝﻨﻘﺎﻭﺓ ‪ ،‬ﻭﺃﻥ ﺘﻜﻭﻥ ﺍﻝﻜﻭﺍﺸﻑ‬
‫ﺒﺎﻝﺨﺼﺎﺌﺹ ﺍﻝﺘﺎﻝﻴﺔ ‪:‬‬

‫ﺍﻴﺜﺎﻨﻭل ‪ ،‬ﺨﺎﻝﻲ ﻤﻥ ﺜﺎﻨﻲ ﺃﻜﺴﻴﺩ ﺍﻝﻜﺭﺒﻭﻥ ‪ :‬ﻴﺴﺨﻥ ﻭﻴﻌﺎﺩل ﺍﻻﻴﺜﺎﻨﻭل ﺒﻤﺤﻠﻭل ﻫﻴﺩﺭﻭﻜﺴﻴﺩ‬ ‫‪1/4‬‬
‫ﺍﻝﺒﻭﺘﺎﺴﻴﻭﻡ ﺍﻻﻴﺜﺎﻨﻭﻝﻲ )ﺒﻨﺩ ‪ (4/4‬ﻓﻲ ﻭﺠﻭﺩ ﻤﺤﻠﻭل ﺍﻝﻔﻴﻨﻭﻝﻔﺜﺎﻝﻴﻥ )ﺒﻨﺩ ‪ (6/4‬ﻜﺩﻝﻴل ‪.‬‬

‫ﻤﺤﻠﻭل ﺒﻴﻜﺭﺒﻭﻨﺎﺕ ﺼﻭﺩﻴﻭﻡ ‪ 10 ،‬ﻏﻡ‪/‬ﻝﺘﺭ ‪.‬‬ ‫‪2/4‬‬

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‫‪GSO ISO 1067 :1994‬‬ ‫ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ‬

‫ﻫﻜﺴﺎﻥ ﻋﺎﺩﻱ ﺘﺠﺎﺭﻱ ‪ ،‬ﺃﻭ ﻤﺴﺘﻘﻁﺭ ﺒﺘﺭﻭﻝﻲ ﺨﻔﻴﻑ ﻤﺩﻯ ﺘﻘﻁﻴﺭﻩ ﺒﻴﻥ ْ‪ 40‬ﺱ ‪ 60ْ -‬ﺱ ‪،‬‬ ‫‪3/4‬‬
‫ﻕ‪.‬‬
‫ﻭﺭﻗﻤﻪ ﺍﻝﺒﺭﻭﻤﻲ ﺃﻗل ﻤﻥ ‪ ، 1‬ﻭﻻ ﻴﺘﺨﻠﻑ ﻋﻨﻪ ﻤﺘﺒ ﹰ‬

‫ﻤﺤﻠﻭل ﻗﻴﺎﺴﻲ ﻤﻥ ﻫﻴﺩﺭﻭﻜﺴﻴﺩ ﺒﻭﺘﺎﺴﻴﻭﻡ ﻓﻲ ﺇﻴﺜﺎﻨﻭل ‪ 0.1 ،‬ﻉ ‪.‬‬ ‫‪4/4‬‬

‫ﻤﺤﻠﻭل ﻗﻴﺎﺴﻲ ﻤﻥ ﻫﻴﺩﺭﻭﻜﺴﻴﺩ ﺒﻭﺘﺎﺴﻴﻭﻡ ﻓﻲ ﺇﻴﺜﺎﻨﻭل ‪ 2 ،‬ﻉ ‪.‬‬ ‫‪5/4‬‬

‫ﻤﺤﻠﻭل ﻓﻴﻨﻭﻝﻔﺜﺎﻝﻴﻥ ﻓﻲ ﺇﻴﺜﺎﻨﻭل ‪) %95‬ﺤﺠﻡ ‪ /‬ﺤﺠﻡ( ‪ 10 ،‬ﻏﻡ‪/‬ﻝﺘﺭ ‪.‬‬ ‫‪6/4‬‬

‫ﺍﻷﺠﻬﺯﺓ ﻭﺍﻷﺩﻭﺍﺕ‬ ‫‪-5‬‬

‫ﺃﺠﻬﺯﺓ ﺍﻝﻤﺨﺘﺒﺭ ﺍﻝﻌﺎﺩﻴﺔ ﻭﻋﻠﻰ ﻭﺠﻪ ﺍﻝﺨﺼﻭﺹ ‪:‬‬

‫ﻜﺄﺱ ‪ ،‬ﺴﻌﺔ ‪ 250‬ﻤل ‪.‬‬ ‫‪1/5‬‬

‫ﺃﻗﻤﺎﻉ ﻓﺼل ‪ ،‬ﺴﻌﺔ ‪ 50‬ﻤل ﻭ ‪ 250‬ﻤل ‪ ،‬ﻤﻁﺎﺒﻘﺔ ﻝﻠﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ ﺍﻝﺘﻲ‬ ‫‪2/5‬‬
‫ﺘﺼﺩﺭﻫﺎ ﺍﻝﻬﻴﺌﺔ ‪.‬‬

‫ﺩﻭﺍﺭﻕ ﻤﺴﺘﺩﻴﺭﺓ ﺍﻝﻘﺎﻉ ‪ ،‬ﺴﻌﺔ ‪ 100‬ﻭ ‪ 250‬ﻤل ‪.‬‬ ‫‪3/5‬‬

‫ﺴﺤﺎﺤﺔ ﺩﻗﻴﻘﺔ ‪ ،‬ﺴﻌﺔ ‪ 2‬ﻤل ‪.‬‬ ‫‪4/5‬‬

‫ﻤﺎﺼﺔ ‪ ،‬ﺴﻌﺔ ‪ 10‬ﻤل ‪ ،‬ﻤﻁﺎﺒﻘﺔ ﻝﻠﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ ﺍﻝﺘﻲ ﺘﺼﺩﺭﻫﺎ ﺍﻝﻬﻴﺌﺔ ‪.‬‬ ‫‪5/5‬‬

‫ﻓﺭﻥ ‪ ،‬ﻴﻤﻜﻥ ﻀﺒﻁ ﺩﺭﺠﺔ ﺤﺭﺍﺭﺘﻪ ﻋﻨﺩ )‪ ْ (2 ± 103‬ﺱ ‪.‬‬ ‫‪6/5‬‬

‫ﺃﺨﺫ ﺍﻝﻌﻴﻨﺎﺕ‬ ‫‪-6‬‬

‫ﻴﺠﺏ ﺃﻥ ﺘﺠﻬﺯ ﻭﺘﺤﻔﻅ ﻋﻴﻨﺎﺕ ﺍﻝﺼﺎﺒﻭﻥ ﺍﻝﻤﺨﺼﺼﺔ ﻝﻠﻤﺨﺘﺒﺭ ﻁﺒﻘﹰﺎ ﻝﻠﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ‬
‫ﺍﻝﺨﻠﻴﺠﻴﺔ ﺍﻝﺘﻲ ﺘﺼﺩﺭﻫﺎ ﺍﻝﻬﻴﺌﺔ ﻭﺍﻝﺨﺎﺼﺔ ﺒـ "ﺍﻝﺼﺎﺒﻭﻥ – ﺃﺨﺫ ﺍﻝﻌﻴﻨﺎﺕ" ‪.‬‬

‫ﺍﻝﻁﺭﻴﻘﺔ‬ ‫‪-7‬‬

‫ﻋﻴﻨﺔ ﺍﻻﺨﺘﺒﺎﺭ‬ ‫‪1/7‬‬

‫ﻴﻭﺯﻥ ﻷﻗﺭﺏ ‪ 0.001‬ﻏﻡ ﺤﻭﺍﻝﻲ ‪ 5‬ﻏﻡ ﻤﻥ ﻋﻴﻨﺔ ﺍﻝﻤﺨﺘﺒﺭ ‪ ،‬ﺍﻝﻤﺒﺸﻭﺭﺓ ﻋﻠﻰ ﻨﺤﻭ ﺩﻗﻴﻕ ‪،‬‬
‫ﻭﺘﻭﻀﻊ ﻓﻲ ﺍﻝﻜﺄﺱ ﺴﻌﺔ ‪ 250‬ﻤل )ﺒﻨﺩ ‪. (1/5‬‬

‫ﺇﺠﺭﺍﺀ ﺍﻻﺨﺘﺒﺎﺭ‬ ‫‪2/7‬‬

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‫‪GSO ISO 1067 :1994‬‬ ‫ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ‬

‫ﻴﻀﺎﻑ ‪ 50‬ﻤل ﻤﻥ ﺍﻹﻴﺜﺎﻨﻭل ﺍﻝﻤﺘﻌﺎﺩل )ﺒﻨﺩ ‪ ، (1/4‬ﻭ ‪ 50‬ﻤل ﻤﻥ ﺒﻴﻜﺭﺒﻭﻨﺎﺕ ﺍﻝﺼﻭﺩﻴﻭﻡ‬

‫)ﺒﻨﺩ ‪ (2/4‬ﺇﻝﻰ ﻋﻴﻨﺔ ﺍﻻﺨﺘﺒﺎﺭ ﻭﻴﺫﺍﺏ ﺍﻝﺼﺎﺒﻭﻥ ﺘﻤﺎﻤﹰﺎ ﺒﺎﻝﺘﺴﺨﻴﻥ ﻋﻨﺩ ﺩﺭﺠﺔ ﺤﺭﺍﺭﺓ ﻻ ﺘﺯﻴﺩ‬
‫ﻋﻠﻰ ْ‪ 70‬ﺱ ﻴﺘﺭﻙ ﺍﻝﻤﺤﻠﻭل ﻝﻴﺒﺭﺩ ﻭﻴﻨﻘل ﻜﻤﻴﹰﺎ ﺇﻝﻰ ﻗﻤﻊ ﺍﻝﻔﺼل ﺴﻌﺔ ‪ 250‬ﻤل )ﺒﻨﺩ ‪، (2/5‬‬
‫ﻤﻊ ﺸﻁﻑ ﺍﻝﻜﺄﺱ ﻋﺩﺓ ﻤﺭﺍﺕ ﺒﺨﻠﻴﻁ ﻤﻥ ﺤﺠﻤﻴﻥ ﻤﺘﺴﺎﻭﻴﻴﻥ ﻤﻥ ﺍﻹﻴﺜﺎﻨﻭل ﺍﻝﻤﺘﻌﺎﺩل )ﺒﻨﺩ‬
‫‪ (1/4‬ﻭﻤﺤﻠﻭل ﺒﻴﻜﺭﺒﻭﻨﺎﺕ ﺍﻝﺼﻭﺩﻴﻭﻡ )ﺒﻨﺩ ‪ . (2/4‬ﻴﺘﻡ ﺍﺴﺘﺨﻼﺹ ﻤﺤﻠﻭل ﺍﻝﺼﺎﺒﻭﻥ ﺜﻼﺙ‬
‫ﻤﺭﺍﺕ ﺒﺎﺴﺘﺨﺩﺍﻡ ‪ 50‬ﻤل ﻤﻥ ﺍﻝﻬﻜﺴﺎﻥ ﺃﻭ ﺍﻝﻤﺴﺘﻘﻁﺭ ﺍﻝﺒﺘﺭﻭﻝﻲ ﺍﻝﺨﻔﻴﻑ )ﺒﻨﺩ ‪ (3/4‬ﻓﻲ ﻜل ﻤﺭﺓ‬
‫‪ ،‬ﻤﻊ ﺍﻝﺘﺤﺭﻴﻙ ﺒﺎﺤﺘﺭﺍﺱ ‪ .‬ﺘﺠﻤﻊ ﺍﻝﻤﺴﺘﺨﻠﺼﺎﺕ ‪ ،‬ﻭﺘﺭﺸﺢ ﺇﺫﺍ ﻝﺯﻡ ﺍﻷﻤﺭ ‪ ،‬ﻭﺘﻐﺴل ﻋﺩﺓ‬
‫ﻤﺭﺍﺕ ﺇﻝﻰ ﺃﻥ ﺘﺼﺒﺢ ﻤﺘﻌﺎﺩﻝﺔ ﻤﻊ ﺍﻝﻔﻴﻨﻭﻝﻔﺜﺎﻝﻴﻥ ‪ ،‬ﺒﺎﺴﺘﺨﺩﺍﻡ ‪ 50‬ﻤل ﻤﻥ ﺨﻠﻴﻁ ﻤﻥ ﺤﺠﻤﻴﻥ‬
‫ﻤﺘﺴﺎﻭﻴﻴﻥ ﻤﻥ ﺍﻹﻴﺜﺎﻨﻭل ﺍﻝﻤﺘﻌﺎﺩل )ﺒﻨﺩ ‪ (1/4‬ﻭﺍﻝﻤﺎﺀ ﻓﻲ ﻜل ﻏﺴﻠﺔ ‪ ،‬ﻭﺘﻜﻔﻲ ﻋﺎﺩﺓ ﺜﻼﺙ‬
‫ﻏﺴﻼﺕ ‪ .‬ﻴﻨﻘل ﺍﻝﻤﺤﻠﻭل ﻜﻤﻴﹰﺎ ﺇﻝﻰ ﺍﻝﺩﻭﺭﻕ ﺴﻌﺔ ‪ 250‬ﻤل )ﺒﻨﺩ ‪ (3/5‬ﺴﺒﻕ ﺘﺠﻔﻴﻔﻪ ﻓﻲ ﺍﻝﻔﺭﻥ‬
‫)ﺒﻨﺩ ‪ (6/5‬ﻋﻨﺩ ﺩﺭﺠﺔ ﺤﺭﺍﺭﺓ )‪ ْ (2 + 103‬ﺱ ﻭﻴﺘﺭﻙ ﻝﻴﺒﺭﺩ ﻓﻲ ﻤﺠﻔﻑ ﻭﻴﻭﺯﻥ ﻷﻗﺭﺏ‬
‫‪ 0.2‬ﻤﻐﻡ ‪.‬‬

‫ﻴﺒﺨﺭ ﻤﻌﻅﻡ ﺍﻝﻤﺫﻴﺏ ﻋﻠﻰ ﺤﻤﺎﻡ ﻤﺎﺀ ﻴﻐﻠﻲ ﻭﻴﺘﻡ ﺍﻝﺘﺨﻠﺹ ﻤﻥ ﺍﻵﺜﺎﺭ ﺍﻷﺨﻴﺭﺓ ﺒﺘﻭﺠﻴﻪ ﺘﻴﺎﺭ‬
‫ﺨﻔﻴﻑ ﻤﻥ ﺍﻝﻬﻭﺍﺀ ﺍﻝﺠﺎﻑ ﺩﺍﺨل ﺍﻝﺩﻭﺭﻕ ﺍﻝﻤﻐﻤﻭﺭ ﻝﻘﺭﺏ ﻨﻬﺎﻴﺘﻪ ﻓﻲ ﺍﻝﺤﻤﺎﻡ ﺃﺜﻨﺎﺀ ﺍﻤﺴﺎﻜﻪ‬
‫ﻭﺇﺩﺍﺭﺘﻪ ﻓﻲ ﻭﻀﻊ ﻤﺎﺌل ‪.‬‬

‫ﻴﺠﻔﻑ ﺍﻝﺩﻭﺭﻕ ﻭﺍﻝﻤﺘﺒﻘﻲ ﻝﻤﺩﺓ ‪ 5‬ﺩﻗﺎﺌﻕ ﻓﻲ ﺍﻝﻔﺭﻥ )ﺒﻨﺩ ‪ (6/5‬ﻋﻨﺩ ﺩﺭﺠﺔ ﺤﺭﺍﺭﺓ‬
‫)‪ ْ (2 ± 103‬ﺱ ﻭﻴﺘﺭﻙ ﻝﻴﺒﺭﺩ ﻓﻲ ﻤﺠﻔﻑ ﻭﻴﻭﺯﻥ ﻷﻗﺭﺏ ‪ 0.2‬ﻤﻐﻡ ‪ .‬ﺘﻜﺭﺭ ﻋﻤﻠﻴﺎﺕ‬
‫ﺍﻝﺘﺠﻔﻴﻑ ﻭﺍﻝﺘﺒﺭﻴﺩ ﻭﺍﻝﻭﺯﻥ ﺤﺘﻰ ﻴﺘﻡ ﺍﻝﺤﺼﻭل ﻋﻠﻰ ﻭﺯﻨﺘﻴﻥ ﻤﺘﺘﺎﻝﻴﺘﻴﻥ ﻻ ﻴﺯﻴﺩ ﺍﻝﻔﺭﻕ ﺒﻴﻨﻬﻤﺎ‬
‫ﻋﻠﻰ ‪ 2‬ﻤﻐﻡ ‪ ،‬ﻭﻝﺘﻜﻥ ﻫﺫﻩ ﺍﻝﻜﺘﻠﺔ ﻙ‪. 1‬‬

‫ﻴﺫﺍﺏ ﺍﻝﻤﺘﺒﻘﻲ ﻓﻲ ﻜﻤﻴﺔ ﻗﻠﻴﻠﺔ ﻤﻥ ﺍﻹﻴﺜﺎﻨﻭل ﺍﻝﻤﺘﻌﺎﺩل )ﺒﻨﺩ ‪ ، (1/4‬ﻭﻴﻌﺎﻴﺭ ﺒﻤﺤﻠﻭل‬

‫ﻫﻴﺩﺭﻭﻜﺴﻴﺩ ﺍﻝﺒﻭﺘﺎﺴﻴﻭﻡ )ﺒﻨﺩ ‪ (4/4‬ﺒﺎﺴﺘﺨﺩﺍﻡ ﺴﺤﺎﺤﺔ ﺩﻗﻴﻘﺔ ﻝﻤﻌﺎﺩﻝﺔ ﺍﻷﺤﻤﺎﺽ ﺍﻝﻁﻠﻴﻘﺔ ﻓﻲ‬
‫ﻭﺠﻭﺩ ﻤﺤﻠﻭل ﺍﻝﻔﻴﻨﻭﻝﻔﺜﺎﻝﻴﻥ )ﺒﻨﺩ ‪ (6/4‬ﻜﺩﻝﻴل ﺇﻝﻰ ﺃﻥ ﻴﺼﻴﺭ ﻝﻭﻥ ﺍﻝﻤﺤﻠﻭل ﺃﺤﻤﺭ ﻭﺭﺩﻴﹰﺎ ‪.‬‬
‫)ﺒﻨﺩ‬ ‫ﻴﺴﺠل ﺤﺠﻡ ﺍﻝﻤﺤﻠﻭل ﺍﻝﻤﺴﺘﺨﺩﻡ ﻓﻲ ﺍﻝﻤﻌﺎﻴﺭﺓ ‪ ،‬ﻭﻝﻴﻜﻥ ﺡ ‪ .‬ﻴﻀﺎﻑ ﺒﻭﺍﺴﻁﺔ ﺍﻝﻤﺎﺼﺔ‬
‫‪ 10 (5/5‬ﻤل ﻤﻥ ﻤﺤﻠﻭل ﻫﻴﺩﺭﻭﻜﺴﻴﺩ ﺍﻝﺒﻭﺘﺎﺴﻴﻭﻡ )ﺒﻨﺩ ‪ ، (5/4‬ﻭﻴﺴﺨﻥ ﺤﺘﻰ ﺍﻝﻐﻠﻴﺎﻥ ﻭﻴﺘﺭﻙ‬
‫ﻝﻴﻐﻠﻲ ﺘﺤﺕ ﻤﻜﺜﻑ ﺇﺭﺠﺎﻉ ﻝﻤﺩﺓ ‪ 30‬ﺩﻗﻴﻘﺔ ‪ ،‬ﺜﻡ ﻴﻀﺎﻑ ﺇﻝﻴﻪ ﺤﺠﻡ ﻤﺴﺎﻭ ﻤﻥ ﺍﻝﻤﺎﺀ ‪ .‬ﻴﻨﻘل‬
‫)ﺒﻨﺩ ‪ (2/5‬ﻭﻴﺸﻁﻑ ﺍﻝﺩﻭﺭﻕ ﺒﻜﻤﻴﺔ ﻗﻠﻴﻠﺔ ﻤﻥ‬ ‫ﺍﻝﻤﺤﻠﻭل ﻜﻤﻴﹰﺎ ﺇﻝﻰ ﻗﻤﻊ ﺍﻝﻔﺼل ﺴﻌﺔ ‪ 50‬ﻤل‬
‫ﺨﻠﻴﻁ ﻤﻜﻭﻥ ﻤﻥ ﺤﺠﻤﻴﻥ ﻤﺘﺴﺎﻭﻴﻴﻥ ﻤﻥ ﺍﻹﻴﺜﺎﻨﻭل ﺍﻝﻤﺘﻌﺎﺩل )ﺒﻨﺩ ‪ (1/4‬ﻭﺍﻝﻤﺎﺀ ‪ .‬ﻴﺴﺘﺨﻠﺹ‬
‫ﺍﻝﻤﺤﻠﻭل ﺜﻼﺙ ﻤﺭﺍﺕ ﺒﺎﺴﺘﺨﺩﺍﻡ ‪ 10‬ﻤل ﻤﻥ ﺍﻝﻬﻜﺴﺎﻥ ﺃﻭ ﺍﻝﻤﺴﺘﻘﻁﺭ ﺍﻝﺒﺘﺭﻭﻝﻲ ﺍﻝﺨﻔﻴﻑ )ﺒﻨﺩ‬

‫‪4‬‬
‫‪GSO ISO 1067 :1994‬‬ ‫ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ‬

‫‪ (3/4‬ﻓﻲ ﻜل ﻤﺭﺓ ﻭﺘﺠﻤﻊ ﺍﻝﻤﺴﺘﺨﻠﺼﺎﺕ ﻭﺘﻐﺴل ﻋﺩﺓ ﻤﺭﺍﺕ ﺇﻝﻰ ﺃﻥ ﺘﺼﺒﺢ ﻤﺘﻌﺎﺩﻝﺔ ﻤﻊ‬
‫ﺍﻝﻔﻴﻨﻭﻝﻔﺜﺎﻝﻴﻥ ‪ ،‬ﺒﺎﺴﺘﺨﺩﺍﻡ ‪ 10‬ﻤل ﻤﻥ ﺨﻠﻴﻁ ﻤﻜﻭﻥ ﻤﻥ ﺤﺠﻤﻴﻥ ﻤﺘﺴﺎﻭﻴﻴﻥ ﻤﻥ ﺍﻹﻴﺜﺎﻨﻭل‬
‫ﺍﻝﻤﺘﻌﺎﺩل )ﺒﻨﺩ ‪ (1/4‬ﻭﺍﻝﻤﺎﺀ ﻓﻲ ﻜل ﻏﺴﻠﺔ ﻭﺘﻜﻔﻲ ﻋﺎﺩﺓ ﺜﻼﺙ ﻏﺴﻼﺕ ‪ .‬ﻴﻨﻘل ﺍﻝﻤﺤﻠﻭل ﻜﻤﻴﹰﺎ‬
‫ﺇﻝﻰ ﺍﻝﺩﻭﺭﻕ ﺴﻌﺔ ‪ 100‬ﻤل )ﺒﻨﺩ ‪ (3/5‬ﺴﺒﻕ ﺘﺠﻔﻴﻔﻪ ﻓﻲ ﺍﻝﻔﺭﻥ )ﺒﻨﺩ ‪ (6/5‬ﻋﻨﺩ ﺩﺭﺠﺔ ﺤﺭﺍﺭﺓ‬
‫)‪ ْ (2 ± 103‬ﺱ ﻭﻴﺘﺭﻙ ﻝﻴﺒﺭﺩ ﻓﻲ ﻤﺠﻔﻑ ﻭﻴﻭﺯﻥ ﺇﻝﻰ ﺃﻗﺭﺏ ‪ 0.2‬ﻤﻐﻡ ‪.‬‬

‫ﻴﺒﺨﺭ ﻤﻌﻅﻡ ﺍﻝﻤﺫﻴﺏ ﻋﻠﻰ ﺤﻤﺎﻡ ﻤﺎﺀ ﻴﻐﻠﻲ ﻭﻴﺘﻡ ﺍﻝﺘﺨﻠﺹ ﻤﻥ ﺍﻵﺜﺎﺭ ﺍﻷﺨﻴﺭﺓ ﺒﺘﻭﺠﻴﻪ ﺘﻴﺎﺭ‬
‫ﺨﻔﻴﻑ ﻤﻥ ﺍﻝﻬﻭﺍﺀ ﺍﻝﺠﺎﻑ ﺩﺍﺨل ﺍﻝﺩﻭﺭﻕ ﺍﻝﻤﻐﻤﻭﺭ ﻝﻘﺭﺏ ﻨﻬﺎﻴﺘﻪ ﻓﻲ ﺍﻝﺤﻤﺎﻡ ﺃﺜﻨﺎﺀ ﺍﻤﺴﺎﻜﻪ‬
‫ﻭﺇﺩﺍﺭﺘﻪ ﻓﻲ ﻭﻀﻊ ﻤﺎﺌل ‪.‬‬

‫ﻴﺠﻔﻑ ﺍﻝﺩﻭﺭﻕ ﻭﺍﻝﻤﺘﺒﻘﻲ ﻝﻤﺩﺓ ‪ 5‬ﺩﻗﺎﺌﻕ ﻓﻲ ﺍﻝﻔﺭﻥ )ﺒﻨﺩ ‪ (6/5‬ﻋﻨﺩ ﺩﺭﺠﺔ ﺤﺭﺍﺭﺓ‬
‫)‪ ْ (2 ± 103‬ﺱ ﻭﻴﺘﺭﻙ ﻝﻴﺒﺭﺩ ﻓﻲ ﻤﺠﻔﻑ ﻭﻴﻭﺯﻥ ﻷﻗﺭﺏ ‪ 0.2‬ﻤﻐﻡ ‪ .‬ﺘﻜﺭﺭ ﻋﻤﻠﻴﺎﺕ‬
‫ﺍﻝﺘﺠﻔﻴﻑ ﻭﺍﻝﺘﺒﺭﻴﺩ ﻭﺍﻝﻭﺯﻥ ﺤﺘﻰ ﻴﺘﻡ ﺍﻝﺤﺼﻭل ﻋﻠﻰ ﻭﺯﻨﺘﻴﻥ ﻤﺘﺘﺎﻝﻴﺘﻴﻥ ﻻ ﻴﺯﻴﺩ ﺍﻝﻔﺭﻕ ﺒﻴﻨﻬﻤﺎ‬
‫ﻋﻠﻰ ‪ 2‬ﻤﻐﻡ ‪ ،‬ﻭﻝﺘﻜﻥ ﻫﺫﻩ ﺍﻝﻜﺘﻠﺔ ﻙ‪. 2‬‬

‫ﺍﻝﺘﻌﺒﻴﺭ ﻋﻥ ﺍﻝﻨﺘﺎﺌﺞ‬ ‫‪-8‬‬

‫ﺍﻝﻨﺴﺒﺔ ﺍﻝﻤﺌﻭﻴﺔ ‪ ،‬ﺒﺎﻝﻜﺘﻠﺔ ‪ ،‬ﻝﻠﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ ﻭﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻓﻲ ﺍﻝﺼﺎﺒﻭﻥ‬

‫ﺡ × ﻭ ( × ‪100‬‬ ‫= )ﻙ‪-1‬‬
‫ﻙ‬ ‫‪1000‬‬

‫ﺍﻝﻨﺴﺒﺔ ﺍﻝﻤﺌﻭﻴﺔ ‪ ،‬ﺒﺎﻝﻜﺘﻠﺔ ‪ ،‬ﻝﻠﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻓﻲ ﺍﻝﺼﺎﺒﻭﻥ‬

‫‪100‬‬ ‫= ﻙ‪× 2‬‬

‫ﻙ‬
‫ﺍﻝﻨﺴﺒﺔ ﺍﻝﻤﺌﻭﻴﺔ ‪ ،‬ﺒﺎﻝﻜﺘﻠﺔ ‪ ،‬ﻝﻠﻤﻭﺍﺩ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻏﻴﺭ ﺍﻝﻤﺘﺼﺒﻨﺔ ﻓﻲ ﺍﻝﺼﺎﺒﻭﻥ‬

‫‪100‬‬ ‫ﺡ × ﻭ ‪ -‬ﻙ ‪× (2‬‬ ‫= )ﻙ‪-1‬‬

‫ﻙ‬ ‫‪10000‬‬
‫ﺤﻴﺙ ﺇﻥ ‪:‬‬

‫ﻜﺘﻠﺔ ﻋﻴﻨﺔ ﺍﻻﺨﺘﺒﺎﺭ ‪ ،‬ﺒﺎﻝﻐﺭﺍﻡ ‪.‬‬ ‫ﻙ=‬

‫ﻜﺘﻠﺔ ﺍﻝﻤﺴﺘﺨﻠﺹ ﺍﻷﻭل ‪ ،‬ﺒﺎﻝﻐﺭﺍﻡ ‪.‬‬ ‫ﻙ‪=1‬‬

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‫‪GSO ISO 1067 :1994‬‬ ‫ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ‬

‫ﻜﺘﻠﺔ ﺍﻝﻤﺴﺘﺨﻠﺹ ﺍﻝﺜﺎﻨﻲ ‪ ،‬ﺒﺎﻝﻐﺭﺍﻡ ‪.‬‬ ‫ﻙ‪=2‬‬

‫ﻤﺘﻭﺴﻁ ﻜﺘﻠﺔ ﺍﻝﺠﺯﻱﺀ ﺍﻝﻐﺭﺍﻤﻲ ﺍﻝﻨﺴﺒﻲ ﻝﻸﺤﻤﺎﺽ ﺍﻝﺩﻫﻨﻴﺔ ﻓﻲ ﺍﻝﺼﺎﺒﻭﻥ‬ ‫ﻭ =‬

‫)ﺍﻨﻅﺭ ﺍﻝﻤﻠﺤﻭﻅﺔ( ‪.‬‬

‫ﺤﺠﻡ ﻤﺤﻠﻭل ﻫﻴﺩﺭﻭﻜﺴﻴﺩ ﺍﻝﺒﻭﺘﺎﺴﻴﻭﻡ ﺍﻻﻴﺜﺎﻨﻭﻝﻲ ﺍﻝﻘﻴﺎﺴﻲ ‪0.1‬ﻉ )ﺒﻨﺩ ‪(4/4‬‬ ‫ﺡ =‬

‫ﺒﺎﻝﻤﻠﻠﻴﻠﺘﺭ ﺍﻝﻤﺴﺘﺨﺩﻡ ﻓﻲ ﺘﻘﺩﻴﺭ ﺤﻤﻀﻴﺔ ﺍﻝﻤﺴﺘﺨﻠﺹ ﺍﻷﻭل ‪.‬‬

‫ﻤﻠﺤﻭﻅﺔ ‪ :‬ﻴﻤﻜﻥ ﺘﻘﺩﻴﺭ ﻤﺘﻭﺴﻁ ﻜﺘﻠﺔ ﺍﻝﺠﺯﻱﺀ ﺍﻝﻐﺭﺍﻤﻲ ﺍﻝﻨﺴﺒﻲ )ﻭ( ﻝﻸﺤﻤﺎﺽ ﺍﻝﺩﻫﻨﻴﺔ ﻓﻲ ﺍﻝﺼﺎﺒﻭﻥ ﺒﻤﻌﺎﻴﺭﺓ‬
‫ﺍﻷﺤﻤﺎﺽ ﺍﻝﺩﻫﻨﻴﺔ ﺍﻝﻤﺴﺘﺨﻠﺼﺔ ﻤﻥ ﻋﻴﻨﺔ ﺍﻝﺼﺎﺒﻭﻥ ﺍﻷﺼﻠﻴﺔ ‪ ،‬ﻭﺍﺴﺘﺒﻌﺎﺩ ﺍﻝﻤﻭﺍﺩ ﻏﻴﺭ ﺍﻝﻘﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ‪،‬‬
‫ﻭﺘﺤﻤﻴﺽ ﻤﺤﻠﻭل ﺍﻝﺼﺎﺒﻭﻥ‪.‬‬

‫ﺘﻘﺭﻴﺭ ﺍﻻﺨﺘﺒﺎﺭ‬ ‫‪-9‬‬

‫ﻴﺠﺏ ﺃﻥ ﻴﺘﻀﻤﻥ ﺘﻘﺭﻴﺭ ﺍﻻﺨﺘﺒﺎﺭ ﺍﻝﻁﺭﻴﻘﺔ ﺍﻝﻤﺴﺘﺨﺩﻤﺔ ﻭﺍﻝﻨﺘﺎﺌﺞ ﺍﻝﺘﻲ ﻴﺘﻡ ﺍﻝﺤﺼﻭل ﻋﻠﻴﻬﺎ ‪،‬‬
‫ﻭﻅﺭﻭﻑ ﺍﻻﺨﺘﺒﺎﺭ ﻭﺃﻱ ﺒﻴﺎﻨﺎﺕ ﺃﺨﺭﻯ ﻝﻡ ﺘﺘﻀﻤﻨﻬﺎ ﻫﺫﻩ ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺃﻭ ﺘﻌﺘﺒﺭ‬
‫ﺍﺨﺘﻴﺎﺭﻴﺔ ‪ ،‬ﻭﺃﻱ ﻋﻭﺍﻤل ﺃﺨﺭﻯ ﻴﻤﻜﻥ ﺃﻥ ﺘﺅﺜﺭ ﻋﻠﻰ ﺍﻝﻨﺘﺎﺌﺞ ‪.‬‬

‫ﻜﻤﺎ ﻴﺠﺏ ﺃﻥ ﻴﺘﻀﻤﻥ ﺘﻘﺭﻴﺭ ﺍﻻﺨﺘﺒﺎﺭ ﺍﻝﺒﻴﺎﻨﺎﺕ ﺍﻝﻀﺭﻭﺭﻴﺔ ﻝﻠﺘﻤﻴﺯ ﺍﻝﻜﺎﻤل ﻝﻠﻌﻴﻨﺔ ‪.‬‬

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‫‪GSO ISO 1067 :1994‬‬ ‫ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ‬

‫ﺍﻝﻤﺼﻁﻠﺤﺎﺕ ﺍﻝﻔﻨﻴﺔ‬

‫‪Free Fatty acids‬‬ ‫‪...........................................................................‬‬ ‫ﺃﺤﻤﺎﺽ ﺩﻫﻨﻴﺔ ﻁﻠﻴﻘﺔ‬

‫ﻜﺤﻭﻻﺕ ﻁﻭﻴﻠﺔ ﺍﻝﺴﻠﺴﻠﺔ ‪Long chain alcohols .................................................................‬‬

‫‪Sterols‬‬ ‫‪.......................................................................................................‬‬ ‫ﺴﺘﻴﺭﻭﻻﺕ‬

‫ﻤﻭﺍﺩ ﻏﻴﺭ ﻗﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ‪Unsaponifiable matter ...............................................................‬‬

‫‪Unsaponified matter‬‬ ‫‪.......................................................................‬‬ ‫ﻤﻭﺍﺩ ﻏﻴﺭ ﻤﺘﺼﺒﻨﺔ‬

‫ﻤﻭﺍﺩ ﻗﺎﺒﻠﺔ ﻝﻠﺘﺼﺒﻥ ﻏﻴﺭ ﻤﺘﺼﺒﻨﺔ ‪Unsaponified saponifiable matter ..................................‬‬

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