tAPERIMENI NO.

(CS)' rom gdone.

Corical tlauk fund,
Juipod stand', few test tube:
kors and titler papers
beakexs filteu he micture
mnt

Cherteal eauised - -

Sodi'ne (5)
dcetone (6my)
61- Na oH Bolution
) Water (Ho)
Cherical Equaon -
Ce-cry + 3I + HNaoH ’ CHIt Na-d-chtal
(Bodine) (16-)
(gaone)
Siguatone
No. Dated .2..08.1.2022

txPERTMENI No. 1 1

(CHIL) fomAcetane
Raratus Reguired t Conioal (lask Jumel
Tri pod stand.ew test Tubes beokess
and ites þapess o ftor the mixtuR

Chemieal Rtguked :>

Godine (6)
3 61- NooH Soltion

Chemical Eauatian
CH-C-ch+ 3,t HNaDH 3 t Na--cH, +3Na
+ 3H,O

Place 5am o Tocine, in aa flask dissolve itt

in 5ml of octont.
pe No
3 Dated ,032

Result of.bperiment :
Calaur of Jodeforin : ale yelirw
Smell : Ru todine
bxpected yield :
Melin sint .
nep
 Dated..3!.I.98.12023
No.

lnLaith Continunus shaking, 6-l

Add sioode &altion
Sodium
undex tap
theAddition till the BroLon Colouk
3 Continut3
disappeatk
migtie toistand or Somé time
4lloothe.
famed
5) iltexthe pxacthttate and dsy bla the
pldsef iter baper
Kesult i
Pale Yellaua
Coloux oáodofom ike
Snell Sodine

19C
Melting. "boint
 ExPERIMENT Noo:2
glucosazone from ioe
Round. Botlom Beakexs ,
Measuing, Cyindex Hatey Bath ,Test
Lubes
Bte bapebs, Taipod Stard Funnel ete
Chenicols :’ Gluiose, Phenghdzozine 6ml, Gtaial
6ne and Wate

Chemical Eiuatian
CHO
HC=N- NH
CHOH
t 30N-N C=N-NH

(çHo"),
cHoH
+NH +NHgss +2M,0

Signatne
age No
6 Dated )409. L2023

bxpaRMENT No.2

dgpaxatus Round Brtiam losk, Beakeas ,

klatex Bath Tesl Tubes.
Measusing Lylinder
paperTipod. sond, Juneel eto
Chemioals: qlucose Phenylhydnzin
ondata.
bmb

Jheoy ’ Glucsazono
dGrdensain
Concensaton 9eodien of' Glusose Saith henl
hydrazins abich ia Caxsied ou in
medim Jo achieve AA henghnyara~ince is dissoved.

Chemical
HO
Equation i
HC=N- NHo>
CHOH C=N-NHO>
+3-NH-NH

CHOH (CHO),
+ NH t NHGH5 t24,0
-ge No.
Dated .I.01..203

(Water Bath)
)
-ge No.
8 Dated . . e 2 c 2 3

Pocedure o ExpERIMENT
Disaolve3am of glucose in 15 mb of Water
in aa flask

l3) n a test tube diss alve 6ml of qlaal geeto

Aid in 15mb o hlates Add 6 of PhNH-NH,
4dd his Sokution to th6 gluccu Joltion.
3) Aace the Contont in Boiling. klates Bak Ylaa
þxccahitate. oil. 0m n 15mih Goatinue hesing
oT 45 inutes

tham and mote Betc

and Rinse the 4gpasatus Complctely itk

Aatex and Aetore bckose enzming
Bxpesimact
2) We should make a
Cavtfat.
theswiss they con give nj
Chemicas also cdomas Qur
to bur
thea
bod
) We sheudd nt make the lastag of Chomiuols
UsHhcm as
ge No. Dated...e

Colous of Gluosazore Vlovs

Melting porht-250'c
Chem'ca formda : (HC=N-NM-3)
(H=N-N 2
(ÇHO,
CHoH
No.
Dated.I.0.2.12o3.

Result of Egurnent
Calour of Glucosaxanê. -YelloA
-

Expedee yield 'g

Meltng bofnt50'o ,
Chomilal formule - (HC=N- NH- aHa

oH
age No. Dated.,09

ExPERIMENT No 3 c
Aim : Jo detesmine Calorimetvicaly he inteqva
ieat Saludion the fiven Slid plass ium
Nits at (HNOJ)

Aprovatus ’3 Thesmous lask, Tio Bea kess, Yoh

Thexmoneaea

Chenicals stilled kater , Solid Patassium Nit.

Obsesvation : A) Fox Watex Eguu valent ot Cabosfmetes:

Yolume Cold
Cold Wates Taken (,o) = |00 ml
Tempexatve Cold Wotey = 25c (tc)
Voume hot atex = looml
Tenpexatwae o Rt mater = 52e E)
amperatse fMicture
of 38-c (tic)
 Dated.2!..I09.123
geNo.

CxeERI MENI No. 33

Aimlo datesmine Colerínnatsicalky the.
nteqxal.heat o Solution o the given
Solidl þotossiunm Nits ale(kNÖ,)

Appaxotus 8 Thesmous flask Two Beakess, ioh

TheÑnometes.

Chemicals 8’ Bistilled klater Spld PotassTum

Nitrate
Jheot y 3 The issolutfonot KNDís an
ecosh exmic broCeSs o defexmine the integral
heat ot Solution mole o Solute (KNOshs dissolved
Jn z00 moles o klater
Jox maintainin thi_ ratio 5-6lgm kND, is
di'ssolved in 200ml Wates lhich s Carried out
in a theimousu ask And aise in tenperatue
is noted. Knowing the tatex eq uvalend o Caloi
-mder ond the
ond the chongeîn domperatuae amount o
Beat evolved is. Coloated.

Bioceduze s 4) o detesmine wlates Eauivalert

JaRe loo m at Water in a Beaker and
rode d temperatua c
 Dated
age No.

B)ox heat oSolutten 1

hagt | Mas Solute 7N9g token : 5-61gm
Yolune o later= 200ml
Weight o Wates Jaken = 2004
fnttial tempexatuNe o Hyo= 256
Jin ali
temperatut Salution 24;20

A) fox keight 5quivalent odaosimeter 3

Heat tost by hot Ho = Heatganed by Cl ts

(381- 25)
13-J

13-1
Signatee
 Dated. . 3
PaaeNa

2) Jake L00 m, o Wate in anaihex Beakex.

and heatit ta 15-loc high3 than foom
tempexature
and note
3)Pourt Tnto the themous sk
jts empexauxe
Pourt lbonliot Gold Wates sopidly tohe
thes mous ask And Note he tempetatre
mixtuxe .

8) To deteamine Heat o Solutien :

thesmou
) Take oo ml o - distlled wates in a
jlack and ; note stse tompcsatre by using
degreo iheamametex
2) Jake S-61gm þomdexcd KNO, and
Jsonsfest"into the thesmous lask sir dhe
condent thoroughly or" Complete' dissolutien
Nate the demperatuxe o Solution
Obsesvations:A) for water Eaui valent o
Volume o Cold water dtaken H,o) l0o ml
Tem pexohuye Cotd Mates = t c
Volume othot hotex = |DOml
Tempexotxe o hot otes = e ml tc
TembetatüYe Miytüse
Page No. I5 Dated .....

8) do alculate Reat f Soltion kND, and KNater ?

Heat o Salution
Heat1 absoy bed when
Imole o Solute sHeat Sduation (+20)
= x(taty)x4-184XM

M= 1 0 1 y

)e2be s+ X 08 x 422:584
B5-61
694)16352 = 12461-96 Jnal
As 5-61
a- Heat So luton AHSal = 12 H61 KImol

Signatre
 Dated..21..D3

B) Jox heat ef Solution :

Volsme ot laterr 200n
Weight of Wates taken = 200ga
gnihtal Jempexatute o H,0= te
dtnal Solutíon t,C
Jemgetataxe

Resutis Heat otSolution o kNo, = 42-46| KJ mal-l

Page No Dated 28, 4 202

ExrERIMENT NO. ;4
Aim sto
do detesmine heat f neutraligation otaorimd'
stzong Bau (Na oH)
sically
Appaxatus s ThedmeusLak Jwo Beakess , Meauning
Begee Thednomeder

Chemicalo 3 0-2 molas HCe, 0-2 MNaoH, distlled

Nateu

Obses vatons i+
A) 2o detet mineWates Egui valent o Caloimetey (a
CoLd Satex Jaken = l00 mL
Tempevat we of Cold
Cd water =24ec)
Volume oj Bot Weadex = loomL
Temperatre ot hot water =sa;e)
Tempey atuwe o Mictuye=ic)
=
9 o detesmine heat. Neutralizalion
Volume o HCL Joken Yolume o< Na oH Sel" ta kon= lo
Signatne
 Dated20.2023

EXPERIMENI NO:4
Aim: o detesmine heat ofi neutralisaton of sron
stvongiBaL (NaOH) Cabrimetes
-Coly
ppaxatusH JhedmoLs Hlask ao beakers, Measusivg
lask, o Beree hesmometos.
Chemicals : 0-2 mola Hcl, 0-2 MNa 0H, dishled
kater.

: Heat o Neutyalization may be deined

he om ount o hegt evolved - bhen lgm
-valent t an aad. is Gmpletely neutrated sish
equcvalent f Bae o Vteess a. in dilte
soltion
Auarding ta rehenius Theoty stinq
Ond baNes ase [ostised. in aquesw
Solubion.
HCL 4) + NaoH (a9,)’Nacl a) + H,0
As a. gasult o meutvalisotion the tenpetatr
Aises which is noted with help of Vo
thesmometex - tom th+s heot o meutvalisatron
Con be Caloulated..
ge No. Dated..o?,203

Jempeuatune ter, ngtralton zsst(c9

Ealaulations : 4) do deleanine the Nate SAuialent
Calosimetex :

o Heat tost by hot Ho Heat gained b Çold Hao +

Caloximeto

t-t)
l00C45-2,- 33-8)-10D
l33,8-24)J

25-279
W 25-2% |
20 Dated 0.a023

Ctoce davue 16 deteamiát dlates Ggitvalani

o Caleximetex lw)
1b0 l ot. Watex în a Beakez and nate
ts Jem pez atue

2) dake l00ml a! Water fn anothex Beakex ond

-heat ti to 16 2o° higher than soos denpesdta
and-note
3) Pous it indo the theSmous
ts Jem peratue.

Pouxe looml o t cold nater. Rapidly to

Jhe thexmous laskAnd. nate the temhexatre

B) do detexmine heat ot Neutralisaton of HCL

nith NaoH
00ml o HC
0:2MMHC
0-2- in Thesmous
I) Jake
ond nate is tempesatuse
Jake l00 ml ot în a Beakex
-2 M NabH in and
mde its Jempe atxegt is impoxt ant hat
Jhe tempexa ue o NaoH must be to

thot ot Hd.
Pour loo mL ot 0-2 M Na0H Sol Qutckly indo
the in Thetmous glask sing (axe
 .MeAJ24-21ku at(aos).
auid strong- meutli_of ian Basu. siong
Heat ith Gesulti
i n it
R9:24.kT Nitralisation
= Heat
lki KJ
24-21
x2:9;D)
kJ 2262)l00
Ibo
3-x4-184 (RR5-23)
x =
.
28:5+25-4)
1y24 x4 2523)
)x; (206+ = hon
34
k3 NeutYalisation=
(2oog Heat
of
eutralisation
Hct detesmineRat oHNa
koidh Jo B)
No....
Dated
No.
Dated
2309.223

hgheat dempesatuve attained.

"Obscs vationg: 4) o datoktniné alater Eqjvalent
Colotnedex Tu) -
"Volume ot Caid-late taken = lo0 mL
lemp Cold Watex = tc
Volume ot hot- Watex = loD ml
Jempesot unye of hot ulatey.=, t'

B Jo deteamine hcat o Neutraksation Hcl N NaoH):

Volume HCæ tokn = Volume ot NaoH doken

Tempetatsern ateoi meutsaliatenz

ResutaJhe aheot ofa Neutsali'sat'on oshong

and wihStsong Base (Na oH
29- 21 kJ