MS DETECTOR LINEARITY

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_TQD Acquired By: sqte
Project Name: SQT_E_BSM_SM_TQD_data Column serial Number:
Sample Set Method: 04b MS Detector Lin Sens SSM Sample Kit 1 Expiration Date:
Processing Method MS Detector Area PM, MS Detector Sample Kit 1 Lot Number:
Report Method Name: MS Detector Lin Sens RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 2512 Result Set Id 3099
Sample Set Name: MS Detector Lin Sens SSM Sample Set Start Date: 1/4/2011 10:06:59 PM EST

T he MS Detector Linearity qualification injects several amounts of Sulfadimethoxine and plots the
Response vs. Sulfadimethoxine Amount.

T he qualification passes if the Linearity R^2 value for Area is > or = 0.990 and the R^2 value for Height
is > or = 0.990.

MS Detector Area Linearity

Area Linearity Area Linearity MS Detector Height Linearity

Area Linearity
Curve R^2 Curve R^2
Curve R^2
Specification Pass Fail Height Linearity Height Linearity
Height Linearity
1 R^2 > or = 0.990 0.9996 PASS Curve R^2 Curve R^2
Curve R^2
Specification Pass Fail
1 R^2 > or = 0.990 0.999 PASS

Printed 8:13:36 PM US/Eastern 4/26/2011 Page: 1 of 4

 MS DETECTOR LINEARITY

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_TQD Acquired By: sqte
Project Name: SQT_E_BSM_SM_TQD_data Column serial Number:
Sample Set Method: 04b MS Detector Lin Sens SSM Sample Kit 1 Expiration Date:
Processing Method MS Detector Area PM, MS Detector Sample Kit 1 Lot Number:
Report Method Name: MS Detector Lin Sens RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 2512 Result Set Id 3099
Sample Set Name: MS Detector Lin Sens SSM Sample Set Start Date: 1/4/2011 10:06:59 PM EST

MS Detector Area Linearity Results

Calibration Id 3100 Y Intercept 92844.7

Date Calibrated 4/26/2011 8:13:30 PM EDT Slope 17671.6

Fit Type Linear (1st Order) R^2 0.99963

Calibration Plot
Area v s. Amount

1.0x107

8.0x106

6.0x106
Area

4.0x106

2.0x106

0.0
0.00 50.00 100.00 150.00 200.00 250.00 300.00 350.00 400.00 450.00 500.00
Amount
Area R^2: 0.99963

Printed 8:13:36 PM US/Eastern 4/26/2011 Page: 2 of 4

 MS DETECTOR LINEARITY

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_TQD Acquired By: sqte
Project Name: SQT_E_BSM_SM_TQD_data Column serial Number:
Sample Set Method: 04b MS Detector Lin Sens SSM Sample Kit 1 Expiration Date:
Processing Method MS Detector Area PM, MS Detector Sample Kit 1 Lot Number:
Report Method Name: MS Detector Lin Sens RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 2512 Result Set Id 3099
Sample Set Name: MS Detector Lin Sens SSM Sample Set Start Date: 1/4/2011 10:06:59 PM EST

MS Detector Height Linearity Results

Calibration Id 3108 Y Intercept 53948.8

Date Calibrated 4/26/2011 8:13:33 PM EDT Slope 6957.0

Fit Type Linear (1st Order) R^2 0.9992

Calibration Plot
Height v s. Amount

4x106

3x106
Height

2x106

1x106

0
0.00 50.00 100.00 150.00 200.00 250.00 300.00 350.00 400.00 450.00 500.00
Amount
Height R^2: 0.9992

Printed 8:13:36 PM US/Eastern 4/26/2011 Page: 3 of 4

 MS DETECTOR LINEARITY

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_TQD Acquired By: sqte
Project Name: SQT_E_BSM_SM_TQD_data Column serial Number:
Sample Set Method: 04b MS Detector Lin Sens SSM Sample Kit 1 Expiration Date:
Processing Method MS Detector Area PM, MS Detector Sample Kit 1 Lot Number:
Report Method Name: MS Detector Lin Sens RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 2512 Result Set Id 3099
Sample Set Name: MS Detector Lin Sens SSM Sample Set Start Date: 1/4/2011 10:06:59 PM EST

Sulfadimethoxine Detector Linearity Ov erlaid Chromatogram

3.5x106

3.0x106

2.5x106

2.0x106
Intensity

1.5x106

1.0x106

5.0x105

0.0

0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00
Minutes

Printed 8:13:36 PM US/Eastern 4/26/2011 Page: 4 of 4