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Documents - Tips - Phuong Phap Phan Tich Cod Trong Nuoc
Documents - Tips - Phuong Phap Phan Tich Cod Trong Nuoc
Ha cht:
Dung dch chun K2Cr2O7 0,0167M: Ha tan 4,913 g K2Cr2O7 ( sy 1050C trong 2
gi) trong 500 ml nc ct, thm vo 167 ml H2SO4 m c v 33,3 g HgSO4 khuy tan,
ngui n nhit phng, nh mc thnh 1000 ml.
Dung dch chun K2Cr2O7 0,0417M: Ha tan 12,259 g K2Cr2O7 ( sy kh 1050C
trong 2 gi) trong nc ct v nh mc thnh 1000 ml.
Acid sunfuric reagent: Cn 5,5 g Ag2SO4 trong 1 kg H2SO4 m c (d = 1,84), 1
2 ngy ha tan hon ton.
Ch th mu Ferroin: Ha tan 1,485 g 1,10 phenanthroline monohydrate v 0,695 g
FeSO4.7H2O trong nc ct nh mc thnh 100 ml (khi hai cht ny trn ln vi nhau th
dung dch ch th s tan hon ton v c mu ).
Dung dch FAS (Fe[SO4].[NH4]2[SO4].6H2O) 0,1M: Ha tan 39,2 g Fe(NH4)2(SO4)2.
6H2O trong 500 ml nc ct, cn thn cho thm 20 ml H2SO4 m c, ngui, nh
mc thnh 1.000 ml.
Chun li nng FAS mi ngy vi K2Cr2O7 0,0167M nh sau: Chn th tch
mu (dng nc ct thay cho mu) v ha cht s dng theo bng sau:
Bng 2.3: T l chn th tch mu v ha cht
C ng
DD K2Cr2O7
H2SO4 reagent
Tng V
2,5
5,0
10,0
0,0167M (ml)
1,5
3,0
6,0
(ml)
3,5
7,0
14,0
(ml)
7,5
15,0
30,0
2,5
1,5
3,5
7,5
V mu (ml)
16 x 100 mm
20 x 150 mm
25 x 150 mm
ng chun 10
ml
V mu
Dung dch
H2SO4 reagent
(ml)
2,5
5,0
10,0
2,5
K2Cr2O7 (ml)
1,5
3,0
6,0
1,5
(ml)
3,5
7,0
14,0
3,5
Tng V (ml)
7,5
15,0
30,0
7,5