Professional Documents
Culture Documents
Imad L. Al-Qadi, Zhen Leng, Jongeun Baek, Hao Wang, Matthew Doyen,
and Steven L. Gillen
Warm-mix asphalt (WMA) is gaining attention in the pavement indus- for an extended construction season. Three WMA techniques have
try because of its environmental benefits. WMA would be especially been commonly used to facilitate the mixing of binder and aggre-
useful if it could be applied to heat-sensitive mixes, such as stone mastic gates: organic additives, foaming techniques, and chemical addi-
asphalt (SMA). However, before these SMA mixes are used with warm tives. Use of organic additives and foaming techniques reduces
mix additives, the performance of the mixes must be examined. A study the effective viscosity of the binder, and chemical additives serve
was conducted to verify the early-age performance of a warm SMA with as a surface-active agent to reduce friction at bitumen–aggregate
an Evotherm 3G additive. An Evotherm SMA and a conventional SMA interfaces. Table 1 is a list of some of the most typical WMA prod-
were evaluated and compared with in situ lightweight deflectometer ucts used in the United States and shows the degree to which each
testing and comprehensive laboratory tests, including complex modulus, reduces a mixture’s production temperature (1). However, because
wheel track, indirect tensile strength, and semicircular bending fracture. there are various WMA preparation techniques, the physical and
Gyratory-compacted specimens made with fresh plant mixtures were chemical properties of the mixture can be altered, which can result
tested in the lab at various curing periods; lightweight deflectometer in different short-term and long-term mechanical behaviors of the
tests were conducted in the field directly on an Illinois expressway over- mixture. Therefore, many studies evaluated the performance of
lay immediately after compaction up to 24 h. The results showed that mixtures produced with various WMA techniques (2–5). Most of
at the same curing period, the early-age performance of the Evotherm these studies reported equivalent performance of WMA with respect
SMA was generally comparable to that of the conventional SMA. The to HMA. However, because the WMA technology is relatively
curing process increased the dynamic modulus of both Evotherm SMA new, many questions remain about WMA’s characteristics, such as
and conventional SMA but did not significantly affect other laboratory increased susceptibility of permanent deformation caused by early-
test results. The onsite modulus of the Evotherm SMA was found to age traffic, unknown long-term field performance, higher risk of
be less than that of the conventional SMA at the same temperature. moisture susceptibility, and unclear traffic opening time.
However, because of the lower compaction temperature, the pavement WMA could provide significant benefits to the industry and in
constructed with the Evotherm SMA could be opened to traffic earlier northern states if it could be applied to heat-sensitive mixes, such as
than could the pavement constructed with the conventional SMA while polymer or ground tire rubber modified stone mastic asphalt (SMA)
providing the same modulus. mixes designed for high traffic volume or heavy load pavements.
Because these SMA mixes must be produced and compacted at high
temperatures, placing them during colder temperatures in the fall or
The use of warm-mix asphalt (WMA) in the United States has grown
early spring is not practical. Use of warm-mix additives with these
rapidly in recent years because of its significant environmental ben-
mixes would allow for a significantly extended construction season.
efits. Compared with traditional hot-mix asphalt, production of
Before SMA mixes with warm-mix additives are used, however,
WMA consumes less energy, emits less greenhouse gas, and allows
their early-age performance must be determined to be comparable
to that of the conventional SMA mixes.
The early-age performance of WMA is a concern mainly because
I. L. Al-Qadi, Illinois Center for Transportation and Department of Civil and Envi- of the curing process. Within a relatively short period after construc-
ronmental Engineering, and Z. Leng and M. Doyen, MC-250, Department of
tion, time-dependent hardening, or curing, may occur in WMA as the
Civil and Environmental Engineering, University of Illinois at Urbana–Champaign,
205 North Mathews Avenue, Urbana, IL 61801. J. Baek, Department of Civil asphalt binder regains its original viscosity or as a certain amount of
and Environmental Engineering, Sejong University, 98 Gunja-Dong, Kwangjin-Gu, entrapped moisture is evaporated from the WMA. Insufficient cur-
Seoul, 143–747, South Korea. H. Wang, Department of Civil and Environmental ing time may cause deterioration of WMA at an early stage, which
Engineering, Rutgers University, 623 Bowser Road, Piscataway, NJ 08854.
could consequently affect its long-term performance. Therefore, the
S. L. Gillen, Illinois State Toll Highway Authority, 2700 Ogden Avenue, Downers
Grove, IL 60515. Current affiliation for Z. Leng: Department of Civil and Structural early-age performance of WMA must be investigated, especially
Engineering, Hong Kong Polytechnic University, Hung Hom, Kowloon, Hong Kong. within the first 24 h of placement to ensure the roadway is not
Corresponding author: Z. Leng, zleng2@illinois.edu. opened to traffic too soon.
Several previous studies reported on the effects of curing time on
Transportation Research Record: Journal of the Transportation Research Board,
No. 2306, Transportation Research Board of the National Academies, Washington,
the strength of WMA. The earliest references to WMA in the United
D.C., 2012, pp. 86–94. States focused on the way in which curing conditions affected the
DOI: 10.3141/2306-10 moisture content and stability of WMA prepared with foaming tech-
86
Al-Qadi, Leng, Baek, Wang, Doyen, and Gillen 87
TABLE 1 Typical WMA Products and Temperature Reductions TESTING MATERIAL AND EXPERIMENTAL PLAN
A 1/2-in. (12.5-mm) SMA, one of the typical SMAs that have been
niques (6–8). These investigations discovered a strong correlation used by contractors in the Chicago, Illinois, area on many large-
between moisture content and strength of the mixtures. Consider- scale expressway overlay projects, was selected as the control for
able strength gain was observed for the specimens subjected to short this study. As Table 2 shows, the Evotherm SMA and the control
(within 1 day) and intermediate (1 to 7 days) curing periods. The SMA share a mixture design, although the Evotherm SMA con-
effect of curing for WMA prepared with organic and chemical addi- tains 0.5% Evotherm 3G by weight of binder. Both mixtures use
tives has also been investigated (3). However, no strong evidence PG 64-22 asphalt binder with 12% ground tire rubber and 8% fine
was found to support that curing time affects the tensile strength of fraction of fractionated recycled asphalt pavement. The compac-
Sasobit WMA and Evotherm WMA. Hence, depending on the type tion temperatures of the control SMA and the Evotherm SMA were
of warm-mix technique and asphalt mixture, the curing effects of 305°F and 260°F (152°C and 127°C), respectively. The volumet-
WMA may vary. ric properties of the control SMA, which meet the standard Illi-
nois Department of Transportation requirements for SMA mixture
design, as modified by Illinois Tollway special provisions are as
RESEARCH OBJECTIVE AND SCOPE follows:
This study determined the early-age performance of the warm-mix • Ndes: 80,
SMA containing an Evotherm 3G additive with both laboratory per- • Asphalt content: 6.2%,
formance testing and on-site stiffness measurement. The following • Bulk specific gravity: 2.440,
research tasks were conducted: • Maximum specific gravity: 2.529,
• Air void: 3.5%,
1. Evaluate the early-age mechanical properties of the Evotherm • Voids in mineral aggregate: 15.7%,
SMA with respect to a control conventional SMA through labora- • Voids filled with asphalt: 77.7%, and
tory performance testing. Laboratory tests were conducted on both • Tensile strength ratio: 0.94.
the Evotherm SMA mixture and the control SMA mixture. These
tests included complex modulus, loaded wheel track, indirect ten-
sile (IDT) strength, and semicircular bending (SCB) fracture.
2. Evaluate the effect of curing time on various mechanical prop-
erties of the Evotherm SMA based on the laboratory test results. For
both the Evotherm SMA and the control SMA, each performance
test was conducted at curing periods of between 3 h and 7 days after
compaction. Because the fracture property is not time critical, the
SCB fracture tests were conducted at curing times of between 12 h
and 12 weeks after compaction.
3. Compare the in situ stiffness of the field Evotherm SMA pave-
ment section and the control SMA pavement section with a light-
weight deflectometer (LWD) test. The LWD test was conducted at
various periods after compaction to monitor the change in pavement
surface modulus as the pavement cooled and continued to cure.
4. Determine the appropriate traffic opening time for the Evo-
therm SMA on the basis of the field LWD testing results. For
determining the traffic opening time for the Evotherm SMA, it was
decided that the Evotherm SMA and control SMA should provide
the same in situ stiffness at traffic opening. FIGURE 1 Injection of Evotherm 3G.
88 Transportation Research Record 2306
Compaction
NMAS Warm Mix Temperature
Mix Ndes [in. (mm)] Binder FRAP (%) Additive [°F (°C)]
NOTE: NMAS = nominal maximum aggregate size; FRAP = fractionated recycled asphalt pavement; GTR = ground tire rubber;
na = not applicable.
Laboratory Testing and Specimen Preparation crete Mixtures. For each mix and curing period, three replicates
were prepared for testing. Dynamic modulus tests were con-
As shown in Figure 2, four laboratory performance tests were con- ducted at room temperature [77°F (25°C)] with frequencies of
ducted in this study: dynamic modulus test, loaded wheel track test, 25, 10, 5, 1, 0.5, and 0.1 Hz. The measured dynamic modulus and
IDT strength test, and SCB fracture test. Table 3 is a summary of phase angle for each test were reported as defined by the following
the laboratory testing matrix. equations:
σ0
Dynamic Modulus Test E* = (1)
ε0
The dynamic modulus test was conducted according to AASHTO
TP-62, Determining Dynamic Modulus of Hot-Mix Asphalt Con- σ = σ 0 sin ( ωt ) (2)
(a) (b)
(c) (d)
FIGURE 2 Laboratory test setup: (a) dynamic modulus test, (b) loaded wheel track test, (c) IDT strength test, and (d) SCB
fracture test.
Al-Qadi, Leng, Baek, Wang, Doyen, and Gillen 89
Material property |E*|, phase angle Rut depth Strength Work of fracture
Temperature, °F (°C) 77 (25) 86 (30) 77 (25) 10 (−12)
Specimen dimension, 3.94 (100) (D) 2.44 (62) (H) 5.91 (150) (D) 2.96 (75) (R)
in. (mm) 5.91 (100) (H) 1.97 (50) (H) 1.97 (50) (H)
Condition 25, 10, 5, 1, 0.5, 0.1 Hz Up to 20,000 cycles (dry) Max. 2,248 lbf (10 kN) CMOD control at 0.028 in./mm
(0.7 mm/min)
Curing period 3 h, 6 h, 12 h, 1 day, 3 3 h, 6 h, 12 h, 1 day, and 3 h, 6 h, 12 h, 1 day, 3 12 h, 1 day, 3 days, 7 days, 3 weeks,
days, and 7 days 3 days days, and 7 days 6 weeks, and 12 weeks
where
On-Site LWD Test
St = tensile strength,
P = maximum applied load, Concurrent with the laboratory performance tests, LWD tests were
d = diameter of specimen, and conducted in the field for monitoring of the early-age on-site stiff-
b = thickness of specimen. ness of the SMA mixtures. As Figure 3 shows, an LWD is a type of
90 Transportation Research Record 2306
120 15
Deflect
Load
Deflection (micron)
12
90
Load (kN)
9
60
6
30
3
0 0
0 10 20 30 40 50 60
Loading time (ms)
(a) (b)
field testing equipment that determines the stiffness of pavement construction, the test was repeated every 30 min until 3 h and then
material. The basic principle of the LWD is to use geophones to every 3 h until 24 h. Before each test, an infrared temperature gun was
measure surface deflections induced by dropping weight. The cal- used to measure the pavement surface temperature.
culation of the pavement surface deflection modulus is based on the
Boussinesq solution:
TESTING RESULTS AND DISCUSSION
f (1 − µ 2 ) σ 0 a
E0 = (6) Results of Laboratory Performance Test
d0
Air Void Contents of Prepared Specimens
where
E0 = surface deflection modulus (MPa), The air void contents of the compacted gyratory specimens were
f = factor for stress distribution (2 is a standard value for flexible measured before each test. Table 4 is a summary of the measured
plate), air void contents of the specimens prepared for various tests. The
µ = Poisson’s ratio (normally 0.35 for asphalt mixture), data show that the air void contents are generally within the range
σ0 = stress under plate (kPa), of 6.0% ± 0.5%, with only one exception: the control SMA for the
a = radius of plate (mm), and wheel track test.
d0 = center deflection (µm).
Figure 4a shows the construction site on I-355 in the Chicago area, Complex Modulus Test
where the Evotherm SMA and control SMA used in laboratory testing
were placed. The underlying structures of both SMA layers contain a Figure 5 shows the dynamic modulus test results at 25 Hz and 0.1 Hz.
1.9-mm (0.75-in.) leveling binder course, a 30.5-cm (12-in.) cement At both frequencies, the modulus of both mixtures increases with
concrete layer, and a 30.5-cm (12-in.) aggregate subbase on top of the the curing time. However, at the same curing time, no significant
subgrade. For each mixture, a leveled area was selected for the LWD difference was found between the Evotherm SMA and the control
test to eliminate the effect of the surface slope on the testing results. SMA, as supported by the overlapped error bars at all curing times.
Three test locations were selected, as illustrated in Figure 4b: one The error bars represent the mean dynamic modulus plus and minus
in the left wheelpath, one between wheelpaths, and one in the right one standard deviation. If the error bars at the same curing time
wheelpath. The LWD test started immediately after the final compac- overlap, the two measurements are considered to be not statisti-
tion pass. To monitor the surface modulus change over time after cally different. Thus the data presented in Figure 5 indicate that the
Right wheelpath
10ft
Between wheelpaths
10ft
Left wheelpath
One lane
(b)
(a)
FIGURE 4 Construction site at I-355 driving lane: (a) compaction and (b) LWD test
locations.
Al-Qadi, Leng, Baek, Wang, Doyen, and Gillen 91
Dynamic Modulus Test Loaded Wheel Track Test IDT Strength Test SCB Fracture Test
Mix Average (%) COV (%) Average (%) COV (%) Average (%) COV (%) Average (%) COV (%)
dynamic moduli of the Evotherm SMA and control SMA are com- cally the same in most cases except at the 72-h curing time, when
parable at the same curing stage. The dynamic moduli of both mixes the Evotherm SMA resulted in a slightly greater rut depth than the
show a trend to increase during the curing process. control SMA.
Figure 6 shows the wheel track test results at 5,000 and 20,000 load- The early-age tensile strengths of the two mixtures were obtained
ing cycles. Because the tests for the specimens with 3-h curing were through the IDT test. Figure 7 shows the tensile strengths of the
terminated before 20,000 loading cycles to start the tests for the Evotherm SMA and the control SMA at various curing stages. The
specimens with 6-h curing, no data were collected at 20,000 loading Evotherm SMA provides statistically higher tensile strength only
cycles for the specimens with 3-h curing time. at 12 h, whereas the control SMA provides equal or higher tensile
Figure 6 shows no clear trend between the rut depth and the cur- strength at all other curing times. In general, the tensile strength of
ing time for the mixtures. This lack of a trend indicates that curing the control SMA is comparable to, or higher than, that of the Evo-
time does not significantly affect the early-age rutting performance therm SMA. The tensile strength of the Evotherm SMA increases
of either Evotherm SMA or control SMA. A comparison of the rut during the first 12 h and then stays relatively constant. The tensile
depth of both mixtures at the same curing time showed that the strength of the control SMA increases at between 24 and 72 h and
rut depths of the Evotherm SMA and the control SMA are statisti- then remains relatively constant.
0.16
1200 Evotherm
SMA
Dynamic Modulus (ksi)
1000 Evotherm
0.12
Rut Depth (in.)
SMA
800
0.08
600
400 0.04
200
0.00
0 3 6 12 24 72
3 6 12 24 72 168 Curing Time (hr)
Curing Time (hr) (a)
(a)
250 0.20
Evotherm Evotherm
Dynamic Modulus (ksi)
SMA SMA
200 0.16
Rut Depth (in.)
150 0.12
100 0.08
50 0.04
0 0.00
3 6 12 24 72 168 6 12 24 72
Curing Time (hr) Curing Time (hr)
(b) (b)
FIGURE 5 Dynamic modulus test results at (a) 25 Hz and FIGURE 6 Loaded wheel track test results after (a) 5,000
(b) 0.1 Hz. cycles and (b) 20,000 cycles.
92 Transportation Research Record 2306
150
500
7 Evotherm
6 SMA 400
Work of Fracture (J)
5 300
4 200
3
100
2
0
1 50 70 90 110 130 150 170 190
0 Surface Temperature (°F)
1 3 7 49 84 (b)
Curing Time (day)
FIGURE 9 Field testing results: (a) pavement surface temperature
FIGURE 8 SCB test results. versus time and (b) surface modulus versus surface temperature.
Al-Qadi, Leng, Baek, Wang, Doyen, and Gillen 93
determine the opening time for WMA based on the surface modulus the traffic opening times of the same mixtures paved in other envi-
measurement. In the criterion used here, the warm mix SMA and ronmental conditions to be determined, the temperature and cooling
the control SMA should provide the same modulus when they are time relations could be obtained with existing cooling model pro-
opened to traffic. grams, such as the MultiCool software developed at the University
The following regression equations between the surface modu- of Minnesota (10). Then the procedure presented in this study could
lus E and the surface temperature T for the control SMA and the be followed to determine the traffic opening times for the two
Evotherm SMA can be obtained from the data in Figure 9b: mixtures in any specific environmental condition.
Traffic Opening
Assumed Traffic Traffic Opening Time (h)
Opening Temperature Surface Modulus Temperature for
for Control [°F (°C)] [ksi (MPa)] Evotherm [°F (°C)] Control Evotherm