Standard Operating Procedure

Effective Date : 09/01/2024 SOP No. : 2607

Review Date : 08/01/2027 SOP for IVAREZ ISRO Department :Production(FCD)
Supersedes : New RESIN Dept. Code : 06
Revision No. : 00 Page No. : 1 of 22
1. Objective : Objective of this SOP is to lay down a procedure for manufacturing of IVAREZ
ISRO RESIN.
2. Scope : This SOP is applicable for procedure for manufacturing of IVAREZ ISRO
RESIN material in production department in IVP Limited.
3. Responsibilit : Manager – Production, Executive – Production,
y Officer – Production.
4. References : In-House.
5. Equipment’/ : Reactor, Blender.
Instruments
6. Annexure : Annexure I: Batch Card for IVAREZ ISRO RESIN R-4 Page no. 8 of 23
7. Precaution :
7.1 Raw material availability on shop floor.
7.2 Vacuum pump operates properly.
7.3 Reactor /charging pot is empty and clean properly before Charging.
7.4 Bottom valve of reactor / charging pot closed properly.
7.5 Check transfer line from reactor to blender.
7.6 Check load cell of charging pot is working properly.
7.7 Stirrer operates properly.
7.8 Check all tank farm pumps are working properly
7.9 Check all utilities like cooling tower, steam boiler, nitrogen plant, chiller and air
compressor are working properly.
7.10 Wear Safety PPE during operation. (Helmet, hand gloves, safety goggles & shoes)
7.11 Ensure that all the manual supply and return valves are open.
8. Activity Details /Procedure-

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Date : Date : Date:

 Standard Operating Procedure
Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department :Production(FCD)
Supersedes : New RESIN Dept. Code : 06
Revision No. : 00 Page No. : 2 of 22
8.1 Procedure for IVAREZ ISRO Resin:
8.1.1 FORMULATION:
Sr.no Raw material name Remark
A. Solid Phenol 100%
B. Formaldehyde 37 % 37%
C. Caustic Soda Flakes -
D. Spirit -
E. Water -
F. Acetic Acid -

8.1.2 Keep given amount of solid phenol drums in oven with 750 C set point for melting
for 8 hrs.
Check and record temperature of oven after every one hours.
a) Ensure XV-1068, XV-1070, XV-1067, XV-1083, XV-1075, XV-1077A, XV-
1077B, XV-1074, XV-1073, XV-1071, XV-1072, XV-1076A, XV-1086,
b) PCV-106B, XV-1078, HV-110, XV-130, XV-1079 and TCV-108 are closed.
8.1.3 Take out phenol drums from oven and ensure that the phenol melted completely
then check the clarity of phenol and record in log sheet
8.1.4 Now, open XV1083, Close PCV106B and start vacuum pump XMR4_VACUUM
to take vacuum up to -0.8 bar into reactor.
8.1.5 Charge given quantity of molten phenol into reactor under vacuum.
8.1.6 Start the stirrer XMR4 after charging minimum stirrable volume of 1000 Kgs,
Once given qty. of phenol charging completed, Stop vacuum pump XMR4 _
VACUUM and open PCV106B to release vacuum.

Prepared By Reviewed By Authorized By

Date : Date : Date:

 Standard Operating Procedure
Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department :Production(FCD)
Supersedes : New RESIN Dept. Code : 06
Revision No. : 00 Page No. : 3 of 22
8.1.7 Charging of formaldehyde from tank form, (1) If select T-7003
8.1.8 Open XV1059, XV130, XV_721 and XV_725, start pump P-711 to take given
amount of formalin 37% from tank farm to R-4 charging pot through PLC.
8.1.9 If select T-7004 open XV1059, XV130, XV_722, and XV_725, start pump P-711
to take given amount of formalin 37% from tank farm to R-4 charging pot through
PLC.
8.1.10 Now open XV-1068, HV-110 and charge formalin from charging pot to reactor.
Close PCV106B and start vacuum pump XMR4_VACUUM to take vacuum up to -
0.5 bar into reactor & charge 50% caustic solution (Caustic water ratio- 1:1) into
reactor, then Stop vacuum pump XMR4 _ VACUUM and open PCV106B to
release vacuum
8.1.11 Let reaction mass to mix well for 10 mins and take out sample for checking pH it
shall be 8.3 to 8.7
8.2 Sensible Heating Phase:
8.2.1 Confirm XV 1083 & PCV 106B open then open condensate valve XV-1076A,
bottom steam supply inlet XV-1072 and Start heating the reactor by opening TCV-
108 and give set point at 520 C with temperature ramp rate 0.50 C/min.
8.2.2 At 520 C exotherm will start. Wait until temperature of the reaction mass reaches to
600 C.
8.2.3 After 600 C if rate of temperature rise is at 0.3 C/min then open XV-1077A and
apply cooling through bottom coil and if rate of temperature rise is at 0.6 C/min
then open XV-1077B and apply cooling through both top & bottom coils. If
temperature is getting down by 1 C/min then stop cooling.
8.2.4 If temperature is not controlled with both coil cooling then apply vacuum in total

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Date : Date : Date:

 Standard Operating Procedure
Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department :Production(FCD)
Supersedes : New RESIN Dept. Code : 06
Revision No. : 00 Page No. : 4 of 22
reflux.
8.2.5 Let reaction mass temperature to rise with the rate of 0.20 C/min up to 82 C and
maintain the temperature at 82-840 C for 5 hrs.
8.3 Sample Checking Phase:
8.3.1 While maintaining at 840 C, check sample droplets test after every 1 hours
Once droplet test is okay (visual testing) then go for cloud point testing after every
5 mins, base on earlier result.
8.3.2 If cloud point (cloud point: 24.5-25.50C) test is ok, then start cooling to both top
and bottom coil and start vacuum pump XMR4_VACUUM also to apply vacuum
simultaneously.
8.3.3 As soon as temperature of reaction mass drops to 600 C then release vacuum by
stopping vacuum pump XMR4_VACUUM and now allow reaction mass
temperature to cool down up to 450 C.
8.3.4 Now apply vacuum (up to -400 mbar) to reactor by starting vacuum pump
XMR4_VACUUM and add acetic acid at 450 C. Then stop vacuum pump
XMR4_VACUUM.
8.3.5 Mix well for 15 min and take sample for PH test (PH=6.5-7.5).
8.3.6 If PH is not within in range then inform to senior authority.
8.4 8.4.1
Settling Phase:
8.4.1 If PH test is ok, then stop reactor stirrer and allow reaction mass for phase
separation for 10 hrs. under cooling. Keep stirrer out of service mode.
8.5 8.4.2
Layer Separation Phase:
8.5.1 After completion of 10 hrs, open reactor manhole and check phase separation
visually.

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Date : Date : Date:

 Standard Operating Procedure
Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department :Production(FCD)
Supersedes : New RESIN Dept. Code : 06
Revision No. : 00 Page No. : 5 of 22
8.5.2 Ensure R4 blender is clean and empty.
8.5.3 Ensure R4 charging pot bottom valve XV107, nitrogen valve XV1081, R4 reactor
bottom valve XV1075, vent valve XV1080 and blender bottom valve XV1082 are
closed.
8.5.4 Start vacuum pump XMR4_VACUUM and take vacuum in R4 blender and collect
upper layer water (by confirming visually) of reaction mass with flexible hose
through manhole into R4 blender and stop vacuum pump and release vacuum by
opening vent valve XV1080.
8.5.5 Now remove flexible hose, close manhole and remove stirrer from out of service
and start R4 reactor stirrer XMR4.
8.6 8.4.1
Vacuum Dehydration Phase:
Keep distillate valve XV1086 open and reflux valve XV1083 close, then close
8.6.1 PCV106B and start vacuum pump XMR4_VACUUM to take vacuum up to -0.93
bar into reactor
8.6.2 After achieving desire vacuum, open condensate valve XV1076A and bottom coil
valve XV1072, then start heating with steam by giving 550C set point to TCV108.
Temperature should not cross 560C.
8.7 8.4.2
Sample Checking Phase:
8.7.1 Continue vacuum dehydration and maintain above parameter for 1 hr. and check
sample for RI.
8.7.2 Continue vacuum dehydration till desire RI achieve (RI=1.5710 to 1.5720).
8.7.3 Once RI achieve within given range, then close steam control valve TCV108,
bottom coil steam valve XV1072 and condensate valve XV1076A.
8.8 8.4.3
Cooling and Solvent Addition Phase:

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Date : Date : Date:

 Standard Operating Procedure
Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department :Production(FCD)
Supersedes : New RESIN Dept. Code : 06
Revision No. : 00 Page No. : 6 of 22
8.8.1 Then open XV1073, XV1074, XV1077A and XV1077B to start cooling upto temp
350C.
8.8.2 Close distillate XV1086 and open reflux valve XV1083 to keep the system in total
reflux position.
8.8.3 Now Close PCV106B and start vacuum pump XMR4_VACUUM to take vacuum
(max. -0.5 bar) into reactor.
8.8.4 After achieving desire vacuum, charge given quantity spirit into reactor through
flexible hose.
8.8.5 After 30 mins. of mixing, give sample for viscosity check.(Viscosity: 50 to 51 Sec
in B4 CUP at 300C)
If desire viscosity not achieve, then add extra spirit.
8.9 8.4.4
Discharge for Packing:
8.9.1 Once viscosity achieve within range, stop agitator XMR4 and open reactor bottom
valve XV1075.
8.9.2 Now fill the batch in 50 kg pack through electronic weighing balance.
8.9.3 Close reactor bottom valve XV1075 after batch filling.

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Date : Date : Date:

 Standard Operating Procedure
Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 7 of 22
ANNEXURE – I
IVP Ltd., D-19/20, Tarapur.
Production Foundry Department
Effective Date Ref. SOP No. : 2607
SOP for IVAREZ ISRO
Review Date Department : Production (F)
Format No. : D-19/20/PP/F/014 Rev. No. : 00
BATCH CARD FOR IVEREZ ISRO – R4
FG Code: FG1087 Batch No. Reactor No. R4
Customer Name: Quantity Product IVEREZ ISRO
Work Ins. No. Start Date Completion Date

Material Description RM Code Purity Ratio Qty. Batch/Lot Purity % Actual Input Name of Person I/P Material
(Kg) No. Used Qty (Kg) Charged Variance
SOLID PHENOL RM1068 100.00% 36.83% 1505
FORMAL DEHYDE 37% RM1029 37% 48.70% 1990
CAUSTIC SODA FLAKES RM1016 100.00% 0.35% 14.3
WATER RM1269 0.35% 14.3
ACETIC ACID RM1001 0.56% 22.7
SPRIT RM001434 13.21% 540

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Date :
 Standard Operating Procedure
Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 8 of 22
Material Description RM Code Purity Ratio Qty. Batch/Lot Purity Actual Input Name of Person I/P Material
(Kg) No. Used % Qty (Kg) Charged Variance
IVAREZ ISRO

PVC 50 Liter PM1015

PLASTIC LABEL IVP
PM0066
BLUE 4"*9"
PLASTIC LABEL IVP
PM0067
RED 4"*9"

RM Total Input 100.00 4086.30

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Date : Date : Date:

 Standard Operating Procedure
Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 9 of 22

Material Balance
Expected Output Qty. (Kg) Actual Output Qty. (Kg) Lose weight (Kg)

Output Qty. (Kg)

Yield % Filling Person Name

Equipment Checks
Description Tick whichever applicable Description Tick whichever applicable
Reactor/Vessel inner clean Yes / No Belt are OK Yes / No
Oil in Gas box is above mark level Yes / No Bottom valve are closed Yes / No
Agitator working Yes / No Required Pump are working Yes / No

REMARK: Please ensure when ever Power Failure and resume, start vacuum pump pit circulation pump and also ensure pump suction by confirmation of
water overflow from top 10 kl syntax tank.

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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 10 of 22

Activity Actual Qty I/P Person Date Start Finish Rec. Colum Press Vacu Conde Remark
Time or O/P Time Time n ure um nser
Kg/c nmh Vent
m2 g on/off
1.Check clarity of melted Phenol and ensure
that Solid Phenol is melted completely before
charging.(Put given Qty. Solid Phenol in drum
heating oven for melting at 105°Ctemp. set
point for 10-12 hrs)
2. Charge given quantity previously melted
Phenol.
3. Start Stirrer and Charge given Qty.37%
Formaldehyde.
4. Charge given Qty. Caustic Soda solution(Mixing
with water in 1:1 ratio)
5. Mix well for 10 min and remove sample for pH=
pH(Desired pH: 8.3-8.7)
6. Start steam heating with ramp of 0.5°c/min.
7. Stop steam heating at Reactor Temp 52°C
8. Apply cooling at Reactor Temp 60°c

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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 11 of 22
Activity Actual Qty Person Date Start Finish Rec Colu Press Vacu Con Remark
Time I/P or Time Time mn ure um dens
O/P Kg/c mmh Vent
m2 g/Ba on/
r Off
9. Apply vacuum if exotherm is not controlled
by cooling.
10. Stop vacuum or vacuum and cooling both if
temp rising stopped or gradually drop down.
11. Again apply cooling at Reactor Temp.
70°Cto maintain Reactor Temp. 83-84°c.
12. Apply vacuum if exotherm is not controlled
by cooling to maintain Reactor Temp. 83-84°C.
13. Release vacuum if Reactor Temp. 83-
84°Cis maintained by cooling only.
14. Remove sample for Droplet Test after 1 Hr
of 83-84°Cmaintaining.
15. Remove sample for Droplet Test after 2 Hrs
of 83-84°Cmaintaining.

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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP for IVAREZ ISRO SOP No. : 2607
Review Date : 08/01/2027 Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 12 of 22

Activity Actua Qty Person Date Start Finish Rec Colum Pressu Vacuu Conde Remark
l Time I/P or Time Time n re m nser
O/P Kg/cm mmhg/ Vent
2
Bar on/Off
16. Remove sample for Droplet Test after
3Hrs of 83-84°Cmaintaining.
17. Remove sample for Droplet Test after
3Hrs and 30 min of 83-84°Cmaintaining.
18. Remove sample for Cloud Point and
Droplet Test after 4Hrs of 83-
84°Cmaintaining.(Desired Cloud
Point:25-26°c)
Cloud Point:
19. Remove sample for Cloud Point
(Desired Cloud Point: 25-26°c)
20. Remove sample for Cloud Point Cloud Point:
(Desired Cloud Point: 25-26°c)
21. Remove sample for Cloud Point Cloud Point:
(Desired Cloud Point: 25-26°c)

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Date : Date : Date:

Standard Operating Procedure
Effective Date : 09/01/2024 SOP for IVAREZ ISRO SOP No. : 2607
Review Date : 08/01/2027 Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 13 of 22

Activity Actual Qty Perso Date Start Finish Rec Colu Press Vacuu Cond Remark
Time I/P or n Time Time mn ure m enser
O/P Kg/c mmhg/ Vent
m2 Bar on/Of
f
22. Remove sample for Cloud Point (Desired Cloud
Point:
Cloud Point: 25-26°c)
23. Remove sample for Cloud Point (Desired Cloud
Point:
Cloud Point: 25-26°c)
24. Once desired Cloud Point is achieved, then
immediately start cooling and apply vacuum also
to drop Reactor Temperature.
25. Release vacuum when Reactor Temp. drop
down to 60°Cand continue cooling.
26. Charged given Qty. of Acetic Acid at Reactor
Temp. 45°c
27. Remove sample for PH after 15 min of PH:
mixing.
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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 14 of 22
 Activity Actual Qty I/P Person Date Start Finish Rec Colu Press Vacuu Conde Remark
Time or O/P Time Time mn ure m nser
Kg/c mmhg/ Vent
m2 Bar on/Off
28.Keep Stirrer off after sampling and keep the
batch under settling for 10Hrs

29.After 10Hrs of settling, remove upper layer Layer

water by taking vacuum at blender.(Qty. of Separatio
n
Water to be removed in layer separation: 730- Distillate
750 KG) Qty:

30. After completing layer separation, close

manhole, start stirrer and turn the system into
dehydration mode.

31.Apply vacuum into Reactor for vacuum

dehydration(Desired Vacuum: -0.92 to -0.94
Bar)

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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 15 of 22
Activity Actual Qty I/P Person Date Start Finish Rec Colu Pres Vacuu Conde Remark
Time or O/P Time Time mn sure m nser
Kg/ mmhg/ Vent
cm2 Bar on/Off
32. Once desired vacuum (Desired Vacuum: -
0.92 to -0.94 Bar) achieved, then start heating
at bottom coil and maintain Reactor Temp. 55-
58°Cduring vacuum dehydration.

33.Remove Sample for RI after 2Hrs of RI:

vacuum dehydration (Desired RI: 1.5700- Distillate
:
1.5720)
34. If desired RI not achieved, then again apply
vacuum to achieve desired RI and maintain
Reactor Temp. 55-58°Cduring vacuum
dehydration(Desired RI: 1.5700-1.5720)

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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 16 of 22
Activity Actual Qty I/P Person Date Start Finish Rec Colu Press Vacuu Conde Remark
Time or O/P Time Time mn ure m nser
Kg/c mmhg/ Vent
m2 Bar on/Off
35. Remove Sample for RI after 1Hr of RI:
vacuum dehydration (Desired RI: 1.5700- Distillate
1.5720).
36. If desired RI not achieved, then again apply
vacuum to achieve desired RI and maintain
Reactor Temp. 55-58°Cduring vacuum
dehydration(Desired RI: 1.5700-1.5720)
37. Remove Sample for RI after 30 Min of RI:
vacuum dehydration (Desired RI: 1.5700- Distillate:
1.5720)

38. If desired RI not achieved, then again apply

vacuum to achieve desired RI and maintain
Reactor Temp. 55-58°Cduring vacuum
dehydration(Desired RI: 1.5700-1.5720)

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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 17 of 22
Activity Actual Qty I/P Person Date Start Finish Rec Colum Pre Vacu Con Remark
Time or O/P Time Time n ssu um dens
re mmh er
Kg/ g/ Vent
cm2 Bar on/O
ff
39. Remove Sample for RI after 15 Min of RI:
Distillate:
vacuum dehydration (Desired RI: 1.5700-
1.5720)
40. If desired RI not achieved, then again apply
vacuum to achieve desired RI and maintain
Reactor Temp. 55-58°Cduring vacuum
dehydration(Desired RI: 1.5700-1.5720)
41. Remove Sample for RI (Desired RI: RI:
1.5700-1.5720) Distillate
42. Once desired RI is achieved, then start
cooling, turn the system into reflux mode and
Drain water hold up from reflux U-loop, then
add given Qty. of Spirit.(apply max vacuum= -
0.5 bar).

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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page o. : 18 of 22
Activity Actual Qty I/P or Person Date Start Finish Rec Colu Pre Vacu Con Remark
Time O/P Time Time mn ssur um dens
e mmh er
Kg/ g/ Vent
cm2 Bar on/O
ff
43. Remove Sample for Viscosity after 30 Min Viscosity in
B4 CUP:
of mixing (Desired Viscosity : 50-51 Sec in
B4 CUP)
44.If desired Viscosity not achieved, then add
required quantity of Spirit to achieve desired
Viscosity (Desired Viscosity: 50-51 Sec in B4
CUP)
45. Remove Sample for Viscosity after 30 Min Viscosity in
of mixing (Desired Viscosity : 50-51 Sec in B4 CUP:
B4 CUP)
46.If desired Viscosity not achieved, then add
required quantity of Spirit to achieve desired
Viscosity (Desired Viscosity: 50-51 Sec in B4
CUP)

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Date: Date: Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP for IVAREZ ISRO SOP No. : 2607
Review Date : 08/01/2027 Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 19 of 22
Activity Actual Qty Person Date Start Finish Rec Colu Pre Vacuu Conde Remark
Time I/P or Time Time mn ssur m nser
O/P e mmhg/ Vent
Kg/ Bar on/Off
cm2
47.Remove Sample for Viscosity after 30 Viscosity in
B4 CUP:
Min of mixing (Desired Viscosity : 50-51
Sec in B4 CUP)
48.If desired Viscosity not achieved, then
add required quantity of Spirit to achieve
desired Viscosity (Desired Viscosity: 50-51
Sec in B4 CUP)
49.Remove Sample for Viscosity after 30 Viscosity in
Min of mixing(Desired Viscosity : 50-51 B4 CUP:
Sec in B4 CUP)
50. If desired viscosity achieved, then Solid
check solid content, point of trouble and BF Content
Point of
viscosity. Then fill the batch in PVC Trouble
carboy. Viscosity

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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP for IVAREZ ISRO SOP No. : 2607
Review Date : 08/01/2027 Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 20 of 22
Activity Actual Qty Person Date Start Finish Rec Colu Press Vacuu Conde Remark
Time I/P or Time Time mn ure m nser
O/P Kg/c mmhg/ Vent
m2 Bar on/Off
51.If desired viscosity achieved, then check Solid
solid content, point of trouble and BF Content
Point of
viscosity. Then fill the batch in PVC Trouble
carboy. Viscosity

SPECIAL INSTRUCTION FOR BATCH

Stage No.: NOTE:- Please ensure when ever Power Failure and resume, start vacuum pump pit circulation pump and also ensure pump
suction by confirmation of water overflow from top 10 kl syntax tank.
Stage No.:

QC Check
Stage No. Description UOM Standard Specification QC Results Remark
Stage No.:5 PH 8.3-8.7
Stage No.:19 Cloud Point °c 25-26°c
Stage No.:20 Cloud Point °c 25-26°c
Stage No.:21 Cloud Point °c 25-26°c

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Date : Date : Date:

Standard Operating Procedure

Effective Date : 09/01/2024 SOP for IVAREZ ISRO SOP No. : 2607
Review Date : 08/01/2027 Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 21 of 22
.

QC Check
Stage No. Description UOM Standard Specification QC Results Remark
Stage No.:22 Cloud Point °c 25-26°c
Stage No.:23 Cloud Point °c 25-26°c
Stage No.:23 Cloud Point °c 25-26°c
Stage No.:23 Cloud Point °c 25-26°c
Stage No.:27 Ph - 6-6.5
Stage No.:33 RI - 1.5700-1.5720
Stage No.:35 RI - 1.5700-1.5720
Stage No.:37 RI - 1.5700-1.5720
Stage No.:39 RI - 1.5700-1.5720
Stage No.:41 RI - 1.5700-1.5720
Stage No.:43 Viscosity @ 30°Cin B4 Sec
CUP 50-51
Stage No.:45 Viscosity @ 30°Cin B4 Sec
CUP 50-51
Stage No.:47 Viscosity @ 30°Cin B4 Sec
CUP 50-51
Stage No.:49 Viscosity @ 30°Cin B4 Sec
CUP 50-51

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Date : Date : Date:

Standard Operating Procedure
Effective Date : 09/01/2024 SOP No. : 2607
Review Date : 08/01/2027 SOP for IVAREZ ISRO Department : Production (F)
Supersedes : New Dept. Code : 06
Revision No. : 00 Page No. : 22 of 22
.

QC Check
Stage No. Description UOM Standard Specification QC Results Remark
Stage No.:51 Solid Content % 60-65
Stage No.:51 Point of Trouble ML 08—12
Stage No.:51 Viscosity in BF CPS 100-150

Variance Description Remark

I/P Material Variance
Time Variance
Quality Variance
Production In charge

End of SOP no. 2607

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