SYSTEM PRECISION REPORT

AC Q U I SI TI O N I N F O R M ATI O N

System Name: Del_Patrol2 Acquired By: Jennb

Project Name: SQT_PATrol_TUV_CM_rev C Column serial Number: 11581505610K
Sample Set Method: 020 System Precision Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
Processing Method System Precision PM Sample Kit 1 Lot Number: N070015
Report Method Name: System Precision Report Build Version: Empower 2 Software Build 2154 SPs
User Name: System Installed:
Sample Set Feature Release 5
Id: 10377 DB ID:
Result 847558692
Set Id 10390
Sample Set Name: System Precision Sample Set Start Date: 10/25/2010 5:51:34 PM

In the System Precision qualification, six (6) injections of Caffeine are made.

The SD for the Caffeine peak RT should be < or = 1.0 seconds, the %RSD for Area should be < or = 0.5 %
and the %RSD for Height should be < or = 1.1 %.

Caffeine Area and Height Results Table

Area %RSD Area Area %RSD Height %RSD Height Height %RSD
Specification %RSD Pass Fail Specification %RSD Pass Fail
1 %RSD < or = 0.5 0.1 PASS %RSD < or = 1.1 0.2 PASS

Caffeine Retention Time (RTsec) Results Table

Retention time (sec) Retention time (sec)

Retention time (sec)
Standard Deviation Standard Deviation
Standard Deviation
Specification Pass Fail
1 SD RT < or = 1.0sec 0.0 PASS

Printed 8:30:17 AM US/Eastern 11/17/2010 Page: 1 of 3

 SYSTEM PRECISION REPORT

AC Q U I SI TI O N I N F O R M ATI O N

System Name: Del_Patrol2 Acquired By: Jennb

Project Name: SQT_PATrol_TUV_CM_rev C Column serial Number: 11581505610K
Sample Set Method: 020 System Precision Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
Processing Method System Precision PM Sample Kit 1 Lot Number: N070015
Report Method Name: System Precision Report Build Version: Empower 2 Software Build 2154 SPs
User Name: System Installed:
Sample Set Feature Release 5
Id: 10377 DB ID:
Result 847558692
Set Id 10390
Sample Set Name: System Precision Sample Set Start Date: 10/25/2010 5:51:34 PM

System Precision Chromatograms

Caffeine - 0.953

1.00
AU

0.00
Caffeine - 0.952

1.00
AU

0.00
Caffeine - 0.952

1.00
AU

0.00
Caffeine - 0.953

1.00
AU

0.00
Caffeine - 0.952

1.00
AU

0.00
Caffeine - 0.951

1.00
AU

0.00
0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20
Minutes

Printed 8:30:17 AM US/Eastern 11/17/2010 Page: 2 of 3

 SYSTEM PRECISION REPORT

AC Q U I SI TI O N I N F O R M ATI O N

System Name: Del_Patrol2 Acquired By: Jennb

Project Name: SQT_PATrol_TUV_CM_rev C Column serial Number: 11581505610K
Sample Set Method: 020 System Precision Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
Processing Method System Precision PM Sample Kit 1 Lot Number: N070015
Report Method Name: System Precision Report Build Version: Empower 2 Software Build 2154 SPs
User Name: System Installed:
Sample Set Feature Release 5
Id: 10377 DB ID:
Result 847558692
Set Id 10390
Sample Set Name: System Precision Sample Set Start Date: 10/25/2010 5:51:34 PM

System Precision Peak Results

Name: Caffeine
Inj Vol RT Retention time Height Points
Vial Injection Name Area Result Id
(ul) (min) (sec) (µV) Across Peak
1 6 1 10 Caffeine 0.953 57.18 2495668.59 1611216.77 54 10424
2 6 2 10 Caffeine 0.952 57.13 2492075.36 1610091.17 54 10425
3 6 3 10 Caffeine 0.951 57.07 2497832.71 1615197.14 54 10426
4 6 4 10 Caffeine 0.953 57.18 2491935.83 1609450.82 54 10427
5 6 5 10 Caffeine 0.952 57.09 2497452.47 1612504.54 53 10428
6 6 6 10 Caffeine 0.952 57.09 2490695.24 1606722.34 53 10429
Mean 57.12 2494276.70 1610863.80
Std. Dev. 0.04 3092.59 2875.40
% RSD 0.12 0.18

Printed 8:30:17 AM US/Eastern 11/17/2010 Page: 3 of 3