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GURUGRAM
BARGARH
SOFT DRINKS
”
And completed the same successfully
during academic year 2021-2022
External examiner
CERTIFICATE
External examiner
ACKNOWLEDGEMENT
I am extremely grateful to my learned guide Mrs.
Kusum Mishra (PGT CHEMISTRY) of JNV
gurugram under whose guidance I am privilege to
do this work. I am thankful to Principal Mr. R
K P A N W A R who always inspired me during
this project work. In this I am always indebted to
Mrs. Kusum mishra.
“PREPARATION OF RAYON
THREAD
F R O M FILTER P A P E R ’’
INTRODUCTION
Rayon is a synthetic fibre produced from cellulose.
CHEMICALS
REQUIRED:-
% CuSO4
% NaOH solution
% Liquor ammonia
solution
% Dilute H 2 SO 4
% Whatman paper
% Distilled H 2 O
THEORY:-
Rayon can be obtained in 2 ways :-
[Cu (NH 3 )4 ](OH )2 + pieces of filter paper left for 10-15 days give a
viscous solution called VISCOSE.
Weigh 20 gm of CuSO 4 .5H 2 O .transfer this to beaker having 100 ml distilled
water and 15 ml dil.NaOH to prevent hydrolysis of CuSO 4 . Stired it with a glass
rod till a clear solution is obtained. Add 11ml of liquor ammonia drop by
drop with slow stirring. The precipitate of cupric hydroxide is separated out.
Filter the solution containing cupric hydroxide through a funnel with filter
paper. Wash the precipitate of cupric hydroxide with water until the
filtrate fails to give a positive test for sulphate ions with barium chloride
solution. Transfer the precipitate to beaker that contains 50ml of liquor
ammonia or wash it down the funnel. The precipitate when dissolved in liquor
ammonia gives a deep blue solution of cuprammonium hydroxide.
This is known as SCHWEITZER’S SOLUTION.
The viscose solution was taken in a syringe and was squeezed out keeping
the hand in motion into a 5M H 2 SO 4 solution .It was then kept for one
day till blue colour of the rayon filament became white. Rayon filaments
were then removed out from the acid bath and were washed with water
dried by keeping then on the filter paper
O B S E R VAT I O N
dressing.
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