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  • Perhitungan Oleo

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    AnnisaAfrillaAdraf
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    This document contains calculations for the transesterification of palm oil to produce biodiesel. It details the volumes of palm oil, methanol and sulfuric acid catalyst used. It then shows the calculations to determine the initial free fatty acid content of the palm oil at 1.85%, and the final free fatty acid contents after reactions at 45 minutes (9.34%), 70 minutes (1.1%) and 80 minutes (0.74%). The percentage conversions of free fatty acids after each reaction are also reported.

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    This document contains calculations for the transesterification of palm oil to produce biodiesel. It details the volumes of palm oil, methanol and sulfuric acid catalyst used. It then shows the calculations to determine the initial free fatty acid content of the palm oil at 1.85%, and the final free fatty acid contents after reactions at 45 minutes (9.34%), 70 minutes (1.1%) and 80 minutes (0.74%). The percentage conversions of free fatty acids after each reaction are also reported.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
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    21 views4 pages

    Perhitungan Oleo

    Uploaded by

    AnnisaAfrillaAdraf
    This document contains calculations for the transesterification of palm oil to produce biodiesel. It details the volumes of palm oil, methanol and sulfuric acid catalyst used. It then shows the calculations to determine the initial free fatty acid content of the palm oil at 1.85%, and the final free fatty acid contents after reactions at 45 minutes (9.34%), 70 minutes (1.1%) and 80 minutes (0.74%). The percentage conversions of free fatty acids after each reaction are also reported.

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    © All Rights Reserved
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    of 4

    LAMPIRAN B

    PERHITUNGAN

    A. Perhitungan volume minyak, metanol, dan katalis H2SO4


    B. Diket : Mr minyak kemasan
    = 256
    C.
    minyak kemasan
    = 0,8 gr/ml
    D.
    Mr metanol
    = 32
    E.
    metanol
    = 0,793 gr/ml
    F.

    Minyak : Metanol

    = 1 mol : 6 mol

    1. Volume minyak kemasan =

    G.
    H.
    I.

    Mol minyak kemasan =

    100 gr
    0,8 gr /ml

    = 125 ml
    Vx
    Mr

    J.

    125 ml x 0,8
    = 256 gr /mol

    K.

    = 0,39
    2. Mol metanol

    = 6 x 0,39

    L.

    = 2,34
    M. Volume metanol

    Mr x mol

    32 x 2,34
    0,793 gr /ml

    N.

    O.

    = 94,57 ml

    3. Volume katalis (H2SO4) = 3% x Volume Minyak


    P.
    = 3% x 125 ml
    Q.
    = 3,75 ml
    R.
    S. Analisa kadar berat asam lemak bebas reaktan
    T. N KOH
    = 0,365 N
    U. Mr asam lemak
    = 256
    V. Berat sampel minyak
    = 3 gr
    W. Volume KOH yang terpakai = 0,5 ml
    X.
    ml KOH x N KOH x Mr asamlemak
    Y. Kadar ALB =
    Berat sampel x 1000
    Z.

    0,5 ml x 0,492 N x 228


    3,03 gr x 1000

    AA.
    AB.
    AC.

    = 0,0185 = 1,85%
    Analisa kadar berat asam lemak bebas produk
    ALB : Metanol

    =1:3

    AD.
    Waktu
    = 45 menit
    AE.
    N KOH
    = 0,365 N
    AF.Mr asam lemak
    = 256 gr/mol
    AG.
    Berat sampel minyak
    = 3 gr
    AH.

    Volume KOH yang terpakai = 3 ml

    AI. Kadar ALB

    ml KOH x N KOH x Mr asamlemak


    Berat sampel x 1000

    AJ.

    3 ml x 0,365 N x 256
    3 gr x 1000

    AK.

    = 0,09344
    = 9,34%

    AL.
    AM.
    AN.
    AO.
    AP.
    AQ.
    AR.
    AS.
    AT.
    AU.
    AV.

    Analisa kadar berat asam lemak bebas produk


    ALB : Metanol
    Waktu
    N KOH
    Mr asam lemak
    Berat sampel minyak
    Volume KOH yang terpakai
    Kadar ALB
    =

    AW.
    AX.

    =1:6
    = 45 menit
    = 0,365 N
    = 256 gr/mol
    = 3 gr
    = 2 ml

    ml KOH x N KOH x Mr asamlemak


    Berat sampel x 1000

    2 ml x 0,365 N x 256
    3 gr x 1000
    = 0,062
    = 6,2%

    AY.
    AZ.

    Konversi ALB =

    BA.

    KAdar ALB AwalKadar ALB Akhir


    Kadar ALB Awal
    1,851,46
    x 100
    1,85

    BB.
    = 21,08 %
    BC.
    BD.
    Analisa kadar berat asam lemak bebas produk (70 menit)
    BE.
    Waktu
    = 70 menit
    BF.N KOH
    = 0,492 N
    BG.
    Mr asam lemak (miristat)
    = 228
    BH.
    Berat sampel minyak
    = 3,02 gr
    BI. Volume KOH yang terpakai = 0,3 ml
    BJ.

    BK.

    Kadar ALB

    BL.
    BM.
    BN.

    ml KOH x N KOH x Mr asamlemak


    Berat sampel x 1000

    0,3 ml x 0,492 N x 228


    3,02 gr x 1000

    = 0,011 = 1,1%
    KAdar ALB AwalKadar ALB Akhir
    Konversi ALB =
    Kadar ALB Awal

    BO.

    1,851,1
    x 100
    1,85

    BP.
    = 40,5%
    BQ.
    BR.
    Analisa kadar berat asam lemak bebas produk (80 menit)
    BS.Waktu
    = 80 menit
    BT.N KOH
    = 0,492 N
    BU.
    Mr asam lemak (miristat)
    = 228
    BV.
    Berat sampel minyak
    = 3,01 gr
    BW.
    Volume KOH yang terpakai = 7 ml
    BX.
    ml KOH x N KOH x Mr asamlemak
    BY.
    Kadar ALB =
    Berat sampel x 1000
    BZ.

    =
    CA.
    CB.

    0,2ml x 0,492 N x 228


    3,01 gr x 1000

    = 0,74%
    KAdar ALB AwalKadar ALB Akhir
    Kadar ALB Awal

    CC.

    Konversi ALB =

    CD.

    CE.

    = 60 %

    CF.
    CG.

    1,850,74
    x 100
    1,85

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