CARRYOVER REPORT

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_TQD Acquired By: sqte
Project Name: SQT_E_BSM_SM_TQD_data Column serial Number:
Sample Set Method: 070 Carryover SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Carryover RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 2694 Result Set Id 3071
Sample Set Name: Carryover SSM Sample Set Start Date: 1/4/2011 11:31:01 PM EST

In the Carryover qualification, three pre-blank injections are performed to determine if the chromatograph is
clean enough to measure carryover. T hose injections are followed by three Sulfadimethoxine calibration injections
at a concentration of (5 ppm) which is 0.005 percent of the Challenge injection concentration (100000 ppm).

T he Challenge injection is made and is followed by three post-blank injections.

Carryover is reported as a percent of the Challenge concentration. If the % Carryover of the first post-blank
injection is less than or equal to 0.005% the qualification passes.

Carryov er Peak Results

Carryover Carryover
SampleName Peak Type % Carryover
Specification Pass Fail
1 PostBlank1 < or = 0.005% Found 0.003 PASS

Printed 8:13:12 PM US/Eastern 4/26/2011 Page: 1 of 4

 CARRYOVER REPORT

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_TQD Acquired By: sqte
Project Name: SQT_E_BSM_SM_TQD_data Column serial Number:
Sample Set Method: 070 Carryover SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Carryover RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 2694 Result Set Id 3071
Sample Set Name: Carryover SSM Sample Set Start Date: 1/4/2011 11:31:01 PM EST

10000.0 10000.0 10000.0

8000.0 8000.0 8000.0

6000.0 6000.0 6000.0

Intensity

Intensity

Intensity
4000.0 4000.0 4000.0

2000.0 2000.0 2000.0

0.0 0.0 0.0

1.00 2.00 1.00 2.00 1.00 2.00
Minutes Minutes Minutes

PreBlank; Vial: 2:F,8; Inj: 1 PreBlank; Vial: 2:F,8; Inj: 2 PreBlank; Vial: 2:F,8; Inj: 3
10000.0 10000.0 10000.0

8000.0 8000.0 8000.0

Sulfadimethoxine
Sulfadimethoxine

Sulfadimethoxine
6000.0 6000.0 6000.0
Intensity

Intensity

Intensity

4000.0 4000.0 4000.0

2000.0 2000.0 2000.0

0.0 0.0 0.0

1.00 2.00 1.00 2.00 1.00 2.00
Minutes Minutes Minutes

Std 0.005%; Vial: 2:E,8; Inj: 1 Std 0.005%; Vial: 2:E,8; Inj: 2 Std 0.005%; Vial: 2:E,8; Inj: 3
10000.0 10000.0 10000.0

8000.0 8000.0 8000.0

Sulfadimethoxine

Sulfadimethoxine

6000.0 6000.0 6000.0

Intensity

Intensity

Intensity

4000.0 4000.0 4000.0

2000.0 2000.0 2000.0

0.0 0.0 0.0

1.00 2.00 1.00 2.00 1.00 2.00
Minutes Minutes Minutes

Stock 100 ng/µL; Vial: 2:F,5; Inj: 1 PostBlank1; Vial: 2:F,6; Inj: 1 PostBlank2; Vial: 2:F,6; Inj: 1

Printed 8:13:12 PM US/Eastern 4/26/2011 Page: 2 of 4

 CARRYOVER REPORT

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_TQD Acquired By: sqte
Project Name: SQT_E_BSM_SM_TQD_data Column serial Number:
Sample Set Method: 070 Carryover SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Carryover RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 2694 Result Set Id 3071
Sample Set Name: Carryover SSM Sample Set Start Date: 1/4/2011 11:31:01 PM EST

10000.0

8000.0
Sulfadimethoxine

6000.0
Intensity

4000.0

2000.0

0.0
1.00 2.00
Minutes

PostBlank3; Vial: 2:F,6; Inj: 1

Printed 8:13:12 PM US/Eastern 4/26/2011 Page: 3 of 4

 CARRYOVER REPORT

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_TQD Acquired By: sqte
Project Name: SQT_E_BSM_SM_TQD_data Column serial Number:
Sample Set Method: 070 Carryover SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Carryover RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 2694 Result Set Id 3071
Sample Set Name: Carryover SSM Sample Set Start Date: 1/4/2011 11:31:01 PM EST

Peak Results
Sample Type: Unknow n
SampleName Sample Type Vial Injection Name RT Area Height Peak Type % Carryover
1 PreBlank Unknown 2:F,8 1 Sulfadimethoxine 1.500 Missing
2 PreBlank Unknown 2:F,8 2 Sulfadimethoxine 1.500 Missing
3 PreBlank Unknown 2:F,8 3 Sulfadimethoxine 1.500 Missing

Peak Results
Sample Type: Standard
SampleName Sample Type Vial Injection Name RT Area Height Peak Type % Carryover
1 Std 0.005% Standard 2:E,8 1 Sulfadimethoxine 1.496 245095 98929 Found 0.0050
2 Std 0.005% Standard 2:E,8 2 Sulfadimethoxine 1.494 237294 93166 Found 0.0050
3 Std 0.005% Standard 2:E,8 3 Sulfadimethoxine 1.495 241367 96797 Found 0.0050

Peak Results
Sample Type: Unknow n
SampleName Sample Type Vial Injection Name RT Area Height Peak Type % Carryover
1 PostBlank1 Unknown 2:F,6 1 Sulfadimethoxine 1.495 125041 48541 Found 0.0026
2 PostBlank2 Unknown 2:F,6 1 Sulfadimethoxine 1.504 36321 14433 Found 0.0008
3 PostBlank3 Unknown 2:F,6 1 Sulfadimethoxine 1.500 19908 8028 Found 0.0004

Printed 8:13:12 PM US/Eastern 4/26/2011 Page: 4 of 4