BO CO THC HNH MN HC QU TRNH THIT B Bi: SY PHUN VITAMIN C H v tn: Bi Vnh Phc Lp: DH09HH Ngy th nghim: 1.

m nguyn liu Khi lng mu trc sy: 4.2436g. Khi lng mu sau sy: 3.822g Tnh m theo cn bng t ta c cng thc:

Trong : m1: khi lng mu trc sy. m2: khi lng mu sau sy. H= = 9.934%

2. m bt vi bc. Khi lng mu trc sy: 4.2376g. Khi lng mu sau sy: 3.8718g Tnh m theo cn bng t ta c cng thc:

Trong : m1: khi lng mu trc sy. m2: khi lng mu sau sy. H= = 8.632%

3. Hiu sut thu hi bt qua my sy phun.

Trong : mB l lng bt thu c sau khi sy phun ton b lng dch(mhh). Ta c : mB = 10.2336g; mhh = 210+90+5 = 305g

4. T l Vitamin C b oxi ho khi sy phun. ( )

Trong : C1% v C2% l nng phn trm ca Vitamin C trong dung dch trc v sau khi sy phun vi cng nng maltodextrin. Xc nh nng vitamin C sau sy (C2%): - Nguyn tc: Vitamin C c chun bng php o iod theo phn ng C6H8O6 + I2 C6H6O6 + 2HI cui nh lng mt lng tha iod s tc dng vi h tinh bt cho mu xanh en. Pha dung dch chun Iod 0,1N

1,3 g Iod + 2 g KI pha nc ct nh mc ln 100 mL Chun bng dd chun Na2S2O3 0,1N Lng Na2S2O3 dng: 24,5 mL K = 24,5/25 = 0.98 Chun vitamin C:

Cn 6g mu pha vi 14ml nc c dung dch c nng maltodextrin l 30% theo khi lng. Sau chia mu thnh 3 phn bng nhau ta c mi mu c khi lng bng 6.67g. Chun bng dung dch iod 0.1N cho n khi xut hin mu xanh bn vng trong 30 giy ( ch th h tinh bt 1%). 1ml dung dch iod 0.1N tng ng vi 8.806mg Vitamin C. Tnh kt qu C% =

Ln 1: lng dd Iod = 11,6 mL => C% = 1.5% Ln 2: lng dd Iod = 11,5 mL => C% = 1.48% Ln 3: lng dd Iod = 11,4 mL => C% = 1.47% => C2% = 1.483% C1% =
T l Vitamin C b oxi ho khi sy phun.

5. Tr li cu hi. - V s cu to v nu nguyn tc hot ng ca my sy phun(bung sy v theo ng t l kch thc ca my tht). - K tn cc loi u phun, nu u v nhc im ca mi loi.