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Biodental Engineering IV
Editors
R.M. Natal Jorge, J.C. Reis Campos, Mário A.P. Vaz,
Sónia M. Santos & João Manuel R.S. Tavares
Universidade do Porto, Porto, Portugal
CRC Press/Balkema is an imprint of the Taylor & Francis Group, an informa business
All rights reserved. No part of this publication or the information contained herein may be repro-
duced, stored in a retrieval system, or transmitted in any form or by any means, electronic, mechanical,
by photocopying, recording or otherwise, without written prior permission from the publisher.
Although all care is taken to ensure integrity and the quality of this publication and the information
herein, no responsibility is assumed by the publishers nor the author for any damage to the property or
persons as a result of operation or use of this publication and/or the information contained herein.
Table of contents
Preface vii
Acknowledgements ix
Scientific committee xi
v
Convergence angle of prepared teeth for full crowns 75
I. Meireles Silva, A. Matos Oliveira, P. Vaz, P. Rocha-Almeida, C. Silva & J.C. Sampaio-Fernandes
Dermal zygomatic peri-implant reaction—gene expression? 79
M.A. Sampaio-Fernandes, L. Tovim, L. Rau, C. Silva, J.C. Sampaio-Fernandes & P. Vaz
Palatal obturators for cleft palate patients 81
M. António Silva, A. Correia, H. Figueiral, V. Campos, T. Pereira Leite, T. Tavares & R. Campos
Linkage between denture’s conditions and oral lesions 87
J. Carvalho, L. Vitorino, S. Félix & R. Campos
Influence of selective etching on marginal filtration of self-etching adhesives 93
S. Arroyo Bote, J. Martínez Arroyo, C. Bucchi & M.C. Manzanares Céspedes
Mandible anomalies—how can two-dimensional ultrasound help? 97
I. Côrte-Real, A. Felino, P. Vaz, R. Nogueira, A.C. Braga, V. Campos & F. Valente
Influence of porosity and cell density on tissue engineering of mandibular condylar cartilage 101
S. Cortez, J.L. Alves & A. Completo
Effects of dynamic compression on cells in tissue engineering of mandibular condylar cartilage 107
S. Cortez, J.L. Alves & A. Completo
Three-dimensional scaffold in bone regeneration 111
M.B. Sordi, I.C. Encarnação, A. Aragones, C.A.M. Benfatti & R.S. Magini
Experimental study of a new biomembrane (MES) for guided bone regeneration 117
R.Z. Gomes, I. Guerra, A. Afonso, M. Helena Fernandes, M. Vasconcelos, A. Felino & J. Cavalheiro
Image processing techniques and orthodontic related apical root resorption prediction models 123
S. Alves, H. Silva, L. Mesquita, N. Lavado & M. Lopez
Effect of drill speed on bone damage during drilling 129
M.G.A. Fernandes, R. Natal, E.M.M. Fonseca, J.E.P.C. Ribeiro & L. Azevedo
Determination of optimal parameters in drilling composite materials to minimize
the machining temperature using the Taguchi method 135
A.C. Lopes, M.G.A. Fernandes, J.E.P.C. Ribeiro & E.M.M. Fonseca
vi
Biodental Engineering IV – Natal Jorge et al. (Eds)
© 2018 Taylor & Francis Group, London, ISBN 978-1-138-05737-1
Preface
Dentistry is a branch of medicine with peculiarities and diverse areas of action, being commonly consid-
ered as a very interdisciplinary area. The development, validation and clinical use of more competently
techniques and technologies have been of great demand and interest.
The purpose of these BIODENTAL Conferences on Biodental Engineering, initiated in 2009, is to
solidify knowledge in the field of bioengineering applied to dentistry promoting a comprehensive forum
for discussion on the recent advances in the related fields in order to identify potential collaboration
between researchers and end-users from different sciences.
This book contains the full papers presented at the 4th International Conference on Biodental Engi-
neering (BIODENTAL 2016), which was held in Vila Nova de Famalicão, Porto, Portugal, in June 21–23.
The conference had 1 Invited Lectures, and 50 contributed presentations, which were selected by the
conference scientific committee.
During BIODENTAL 2016, several topics and applications were addressed, including biomechanical
disorders, numerical simulation, orthodontics, implantology, aesthetics, dental medicine, medical devices
and medical imaging.
The conference co-chairs would like to take this opportunity to express their gratitude to the confer-
ence sponsors, all members of the conference scientific committee, invited lecturers, session-chairs and to
all authors for submitting and sharing their knowledge.
vii
Biodental Engineering IV – Natal Jorge et al. (Eds)
© 2018 Taylor & Francis Group, London, ISBN 978-1-138-05737-1
Acknowledgements
The editors and the Conference co-chairs acknowledge the support towards the organization of the 4th
International Conference on Biodental Engineering BIODENTAL 2016 and the publishing of this Book
of Proceedings to the following organizations:
– Universidade do Porto (UP)
– Faculdade de Engenharia da Universidade do Porto (FEUP)
– Faculdade de Medicina Dentária da Universidade do Porto (FMDUP)
– Instituto de Ciência e Inovação em Engenharia Mecânica e Engenharia Industrial (INEGI)
– Laboratório de Biomecânica do Porto (LABIOMEP)
– Fundação para a Ciência e a Tecnologia (FCT)
– Project NORTE-01-0145-FEDER-000022 – SciTech – Science and Technology for Competitive and
Sustainable Industries, cofinanced by Programa Operacional Regional do Norte (NORTE2020),
through Fundo Europeu de Desenvolvimento Regional (FEDER)
– Associação Portuguesa de Mecânica Teórica Aplicada e Computacional (APMTAC)
– Câmara Municipal da Vila Nova de Famalicão
– Casa das Artes de Vila Nova de Famalicão
– Centros auditivos Widex
ix
Biodental Engineering IV – Natal Jorge et al. (Eds)
© 2018 Taylor & Francis Group, London, ISBN 978-1-138-05737-1
Scientific committee
All works submitted to BIODENTAL 2016 were evaluated by an International Scientific Committee
composed by 69 expert researchers from recognized institutions:
xi
Biodental Engineering IV – Natal Jorge et al. (Eds)
© 2018 Taylor & Francis Group, London, ISBN 978-1-138-05737-1
Rui Machado, Orlando F. Lino, César Silva & João Carlos Sampaio-Fernandes
Department of Prosthodontics, Faculty of Dental Medicine, University of Porto, Portugal
ABSTRACT: The aim of this study was to quantify and compare the most frequently type of teeth
required fixed rehabilitation by undergraduate students in Fixed Prosthodontics’ clinical appointments at
the Faculty of Dental Medicine of the University of Porto, in two periods (1990–1994 and 2010–2014),
defining new goals for pre-clinical practice. This study was based on a retrospective review of two-hundred
patient reports, divided into two equal samples. A total of 357 teeth had been prepared, and the major-
ity involved fixed bridge rehabilitation. No significant differences were found between quadrants. The
maxillary teeth were the most frequently prepared and remained constant or increased between peri-
ods. Regarding the lower jaw, a significant difference was observed: the most frequently prepared teeth
in 1990–1994 were molars, whereas in 2010–2014 were the canines and premolars. Pre-clinical practical
teaching should thus focus on all the upper teeth and on lower premolars.
1
The aim of this study is to quantify and com- Table 1. Types of fixed prosthetic restorations by
pare the types of teeth that most frequently require period of years.
rehabilitation with crowns and fixed bridges per-
formed by undergraduate students in Fixed Pros- Prepared Total of
Prepared bridge prepared
thodontics’ clinical appointments at FMDUP, in crowns abutments teeth
two different decades (1990–1994 and 2010–2014), Period (N) (N) (N)
and define new goals for the pre-clinical practice.
1990–1994 83 86 169
2010–2014 91 97 188
2 MATERIAL AND METHODS Total 174 183 357
2
A statistically significant correlation was found molars. These results are close to those published in
between each period and type of prepared teeth in by other authors (Fejérdy et al., 2007; Näpänkan-
the lower jaw (p<0.0005). In the period between gas et al., 2001; Al-Rafee et al., 1996; Barrero
1990 and 1994 the most frequently prepared teeth et al., 2015).
were molars, while in the 2010–2014 period were However, this finding was not as significant in
incisors, canines and premolars (p = 0.011). No the period of 2010–2014, having the number of
significant variation was observed amongst quad- prepared molars and premolars decreased between
rants (p = 0.894). the two periods (twenty-five to nine molars and
sixteen to twelve premolars). These statistically
significant results may be related to the decreas-
4 DISCUSSION ing early loss of first molars due to decay, possibly
explained by the increasing rates of oral hygiene in
In a review article about oral rehabilitation across the Portuguese population. Another explanation
thirteen European countries published in 2007, may be the introduction of implantology in prac-
Zitzmann et al. concluded that half of the Euro- tice classes of master degrees in FMDUP, which is
pean population had some type of oral rehabili- now the first choice for replacing molars.
tation (fixed or removable), which is less common In the 2010–2014 period, the most frequently
in countries where the GDP (Gross Domestic prepared mandibular teeth were canines. This can
Product) is lower, despite the need of rehabilita- be explained by the fact that canines are commonly
tion being higher. They also found that, at younger used for abutments in fixed rehabilitations due to
ages, and if the number of missing teeth was being strong teeth that have a long root with a very
smaller, the likelihood of rehabilitation with fixed powerful bone implantation.
prosthesis was greater. Furthermore, the frequency Bridges abutments preparations were more
of rehabilitation with implants had increased, but frequent although we did not find a significant
it was still low. These results are consistent with difference between them and single crown prepa-
those obtained in the study by Battistuzzi et al. in ration. This finding could be unexpected due to
1987, where they also referred that molars were the the introduction of implantology in the university
first teeth to be lost in all socio-economical classes clinical practice. Many factors can be pointed out
(Zitzmann et al., 2007; Battistuzzi et al., 1987). like the exclusivity clinical learning of implantol-
Valderhaug et al. reported that fixed prosthe- ogy in postgraduate education or some published
sis rehabilitation in the maxilla represented 74% evidence on the survival rates between implants vs
of all, with no difference between right and left bridges pointing out that bridges could give a bet-
sides. They also indicated that upper incisors and ter longevity (Müller et al., 2008; Holm-Pedersen
premolars represented almost 70% of all abutment et al., 2008).
crowns. Moreover, they found that upper first Fejérdy et al. reported that, in Hungary, the
premolars were the teeth most frequently replaced teeth that were most often used as abutments for
with bridges. The canines were the teeth most fixed prosthesis were canines in both jaws. They
commonly replaced with abutments in both jaws also referred that the most often replaced teeth
(Valderhaug et al., 1976). in the maxilla were premolars, and in the mandi-
In our study, the most frequently prepared ble were first molars and second premolars. They
upper teeth were the anterior ones in both periods, found no significant differences between the right
since about half of the rehabilitations involved the and the left side (Fejérdy et al., 2007).
incisors and nearly 87% (N = 109 in 1990–1994 Näpänkangas et al., regarding metal-ceramic
and N = 135 in 2010–2014) of the total number of bridges in the Finnish population, concluded
fixed prosthesis placed in the upper arch involved that more fixed prosthesis had been prepared in
incisors, canines, and premolars. These teeth are the upper arch than in the lower arch. The most
more exposed in the smile, having great aesthetic often replaced teeth were first premolars, followed
and social importance, and thus this region has by upper lateral incisors and lower first molars
highly aesthetical and functional requirements. (Näpänkangas et al., 2001).
Our results are consistent with those obtained by Al-Rafee et al. and Leempoel et al., in stud-
Valderhaug (Valderhaug et al., 1976). ies regarding bridges conducted in Saud Arabia
The results of our study show no significant dif- and The Netherlands, respectively, reported that
ference between quadrants, which is in agreement more bridges were placed in the maxilla, and that
with the results of Fejérdy et al. lower first molars were the teeth that needed to be
We also did not find significant differences replaced most often. The most common places for
between periods, with the exception of the lower abutments were the maxillary second premolars
jaw. In the lower arch, the teeth most frequently and the mandibular second premolars and second
involved in rehabilitations were premolars and molars (Al-Rafee et al., 1996; Leempoel et al., 1989).
3
Our study on prepared teeth cannot be easily and 2010–2014) the number of prepared maxil-
compared to other studies, since we included all lary teeth remained constant or increased;
preparations and not only abutments of bridges. − In the lower jaw, we observed a significant dif-
Our primary objective was to understand which ference between the two periods. The most fre-
teeth required a more intensive training of under- quently prepared teeth in the 1990–1994 period
graduate students. However, the results seem to were the molars, while during the 2010–2014
be close to those obtained by Valderhaug et al., period were the canines and premolars;
regarding the maxilla, and to those obtained by − Pre-clinical practical teaching should focus on
Al-Rafee et al. or Müller et al. concerning the all of the upper teeth and on lower canines and
mandible (Valderhaug et al., 1976; Al-Rafee et al., premolars.
1996; Müller et al., 2008).
In this study, it was also clear that fixed pros-
theses performed in FMDUP involved mainly the REFERENCES
upper teeth. This trend has slightly increased, since
the use of upper teeth surpassed 82% in the 2010– Al-Rafee MA, Fayyad MA. Failure of dental bridges.
2014 period. These results are consistent with Age and sex of patients and distribution of replaced
those obtained by Barrero et al. It seems clear that and abutment teeth. J Oral Rehabil 1996; 23: 280–282.
the predominant use of upper teeth, and, amongst Barrero C, Duqum I, Petrola F. Dental students’ per-
ceived preparedness to treat patients in clinic after a
these, the anterior ones, is related to the higher fixed prosthodontics course: survey results of a case
aesthetic demands of this region (Holm-Pedersen study. J Dent Educ 2015: 79(4) p 409–16.
et al., 2008; Barrero et al., 2015). Battistuzzi P, Kayser A, Peer P. Tooth loss and remaining
Another interesting point is the fact that the occlusion in a Dutch population. J Oral Rehabil 1987;
number of preparations involving every type of teeth 14: 541–547.
of the upper jaw remained constant or increased in Brand HS, Kamell H, Kharbanda AK, et al. Students’
the 20-year period between the two samples. perceptions of materials and techniques used at Euro-
Thus, it seems that pre-clinical teaching of the pean dental schools in the education of fixed prostho-
dental preparation technique in the upper arch dontics. J Dent Educ 2013; 77(9): 1140–6.
Fejérdy P, Tollas OL, Fejérdy L, et al. Monitoring trends
should focus on all teeth. Regarding the lower jaw, in fixed partial denture design based on national sur-
currently, premolars are the teeth whose prepa- veys. Fogorv Sz 2007; 100(6): 279–88.
ration technique should have a more intensive Holm-Pedersen P, Lang NP, Müller F. What are the lon-
training. gevities of teeth and oral implants? Clin Oral Implants
Res. 2008;19(3): 326–8.
Müller F, Naharro M, Carlsson GE. What are the preva-
5 CONCLUSION lence and incidence of tooth loss in the adult and eld-
erly population in Europe? Clin Oral Implants Res.
The study on the rehabilitation of fixed prosthesis 2008; 19(3): 326–8.
Näpänkangas R, Salonen MA, Raustia AM. Treat-
on teeth performed by undergraduate students in ment need for fixed metal ceramic bridge prostheses
FMDUP patients in the periods of 1990–1994 and in patients treated by dental students in 1984–1996.
2010–2014 lead us to conclude that: J Oral Rehabil. 2001; 28(12): 1101–5.
− Tooth preparations for fixed bridge rehabilita- Scott J. Dental education in Europe: the challenges of
variety. J Dent Educ 2003; 67(1): 69–78.
tion were slightly more common than for single Valderhaug J, Karlsen K. Frequency and location of arti-
crowns; ficial crowns and fixed partial dentures constructed at
− No difference was observed between right and a dental school. J Oral Rehabil 1976: 3(1): 75–81.
left quadrants; Zitzmann NU, Hagmann E, Weiger R. What is the preva-
− The most frequently prepared teeth were the lence of various types of prosthetic dental restorations
maxillary ones, and between periods (1990–1994 in Europe? Clin Oral Impl Res 2007; 18: 20–33.
4
Biodental Engineering IV – Natal Jorge et al. (Eds)
© 2018 Taylor & Francis Group, London, ISBN 978-1-138-05737-1
M.E.R. Dotto
Department of Physics, Federal University of Santa Catarina (UFSC), Florianópolis/SC, Brazil
ABSTRACT: The aim of this study was to evaluate the changes on implant-abutment surfaces after
immersion systems in 2% chlorhexidine or 1% citric acid. Implant-abutment systems were embedded in
epoxy resin and cross-sectioned at delimited areas to be immersed in 2% Chlorhexidine (CG) or 1% Citric
Acid (CAG) Gel for 4 and 2 min, respectively. The surfaces were analyzed by profilometry and Scanning
Electron Microscopy (SEM). SEM analysis revealed changes on the test surfaces after immersion in chlo-
rhexidine or citric acid. Signs of corrosion were more evident for CAG. Before immersion, Ra roughness
mean values were at 0.035 μm for GC implant and at 0.022 μm for GC abutment; while Ra mean values
were at 0.038 μm for CAG implant and 0.016 μm for CAG abutment. After immersion, Ra roughness
mean values were at 0.041 μm for GC implant and 0.033 μm for GC abutment; while Ra mean values were
at 0.49 μm for CAG implant and 0.031 μm for CAG abutment. All groups showed statistically significant
differences when compared (p < 0.05). It was concluded that both gels applied caused change on dental
implant systems being more intense when immersed in 1% citric acid.
5
However, the titanium surface behavior in con- Different areas within the critical zone were
tact with some substances used in the treatment of inspected at magnification ranging from 1000 to
perimplantitis is not entirely understood in the lit- 2000 X at 10 kV.
erature. Therefore, such potential titanium degra-
dation risk should be clarified, revealing the effects 2.3 Topographic analysis by optical profilometry
of these common therapeutic procedures in dental
clinical practice for patients with oral rehabilita- The roughness of the abutment and the dental
tions implant supported. implant was analyzed using optical profilometry
The aim of this study was to evaluate the changes (DektakXT Profilometer, Germany) at three six
on implant-abutment surfaces after immersion in different areas within the critical zone in all sam-
two therapeutic gels, namely 2% chlorhexidine or ples (n = 18). For optical profilometry, the following
1% citric acid. parameters were considered: length measurement
at 2 mm, cut off at 0.25 mm and speed of 30s
before and after immersion in both gels.
2 MATERIALS AND METHODS The roughness values were obtained regard-
ing Ra roughness parameter that consists in the
2.1 Sample preparation arithmetic mean value between the peak and valley
height values in the effective roughness profile.
Dental implant systems (Titamax, Neodent®,
Curitiba, Brazil) were used in this study. Abut-
ments were torqued at 15 Ncm on their respec- 2.4 Statistical analysis
tive implants using a Lutron digital torquemeter Results were statistically analyzed by analysis t-stu-
(Lutron TQ8800, Taiwan). Then, the abutment- dent test, at a significance level of p < 0.05 by using
implant assemblies were embedded in acrylic resin the SPSS 17.0 software.
(Technovit 7200 VLC. Kulzer, Wehrheim, Ger-
many) and cross-sectioned along the vertical axis
of the implant using a precise cutting machine 3 RESULTS
(Isomet 1000, Germany).
The cross-sectioned samples were wet ground 3.1 Morphological analysis of cross-sectioned
down to 2400 Mesh using silicon carbide sandpa- areas
pers followed by polishing with alumina particles
Micrographs of cross-sectioned areas obtained by
(1 and 0.03 μm at diameter). After that, the samples
SEM revealed scratches from sample preparation
were ultrasonically cleaned in isopropyl alcohol for
by grinding and polishing (Fig. 1).
10 min, and then in distilled water for 5 min.
The micrographs obtained after immersion
The cross-section method allowed the analysis
in chlorhexidine did not show clear signs of the
along the implant-abutment connection by micros-
abutment implant system degradation, although a
copy and profilometry.
slight change was noted on the surfaces (Fig. 2).
After preparation, samples were divided into
Samples immersed in a 1% citric acid revealed
two groups, for all samples, an area has been
significantly greater changes when compared with
selected (0.8 × 0.8) mm at the level of critical
abutment region and implant considering the
interaction of substances. The delimited area was
analyzed after contact with the solutions accord-
ing to the specifications suggested in the literature
(Ungvári et al., 2010) for chemical disinfection.
A group of samples was immersed in 2% chlo-
rhexidine gel for 4 min (group CG) and another
one (group CAG) was immersed in 1% citric acid
for 2 min. After ultrasonic cleaning, the surfaces
were analyzed again by profilometry and scanning
electron microscopy (SEM).
6
the results obtained after immersion in chlorhexi- Chlorexidine Group Ra roughness h1m)
dine. Morphological aspects resultant from degra- (Jlm)
dation by corrosion were noticed on the surfaces ,041
,045
immersed in 1% citric acid, mainly on the implant
region (Fig. 3). ,040
,035
,030
3.2 Roughness analysis by optical profilometry
,025
The mean values of Ra roughness for implant and ,020
abutment before and after immersion in 2% chlorhex- ,015
idine and 1% citric acid are shown in Figures 4 and 5. ,010
Before immersion in chlorhexidine, the mean ,005 Before
values of Ra roughness for implant and abut- ,000 • After
Abutment
ment surfaces were different due to the grinding Implant
(Jlm)
,050
,045
,040
,035
,030
,025
,020
,015
,010
,005 • Before
•After
,000 Implant Abutment
7
Table 1. Statistical analysis of the results on Ra rough- citric acid or 2% chlorhexidine. We can conclude
ness (μm) before and after immersion in 2% chlorhexi- that there were changes on the surface of the den-
dine (CG). tal implant systems after both gels; although, signs
of corrosion were clearly detected after immersion
Mean (μm) Std. deviation p
in 1% citric acid.
CG Abutment 0.022 0.0013 <0.05 Roughness slightly increased on the implant
before surface after immersion in 2% chlorhexidine for
CG Abutment 0.033 0.0078 5 min. However, chlorhexidine gel can adhere to
after the surface of the titanium; leading to changes in
CG Implant 0.035 0.0087 <0.05 the roughness.
before Considering the changes observed on the sur-
CG Implant 0.041 0.012 face of the samples, the clinician should be aware
after on the application timer of chlorhexidine or citric
acid in contact with titanium-based dental implant
systems.
Table 2. Statistical analysis of the results of Ra rough-
ness (μm) before and after immersion in 1% citric acid.
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the effect of a commercial chlorhexidine gel form of hydrogen peroxide and other oxidizing agents:
which is more viscous and difficult to remove differences between liquid and gas forms. Journal of
after rising or ultra-sonic bath concerning a clini- Antimicrobial Chemotherapy 65: 2108–2115.
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GC samples can thus be assigned to a substance implantitis disinfection methods on in vivo human
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8
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ferent pHs on commercially pure titanium-based national Journal of Oral Maxillofacial Implants 27:
implants. Journal of Prosthodontics 18: 130–134. 1043–1054.
Schwarz, F., Hegewald, A., John, G., Sahm, N. & Becker, Ungvári K, Pelsöczi IK, Kormos B, Oszkó A, Rakonczay
J.L. (2013) Four-year follow-up of combined surgi- Z, Kemény L et al. Effects on titanium implant sur-
cal therapy of advanced peri-implantitis evaluating faces of chemical agents used for the treatment of
two methods of surface decontamination. Journal peri-implantitis. J Biomed Mater Res B Appl Bio-
of Clinical Periodontology 40: 962–967. mater. 2010; 94(1): 222–9.
Sjögren, LDS, Sletten, Jon E. Cytotoxicity of dental Valderrama, P., Blansett, J., Gonzalez, M.G., Cantu,
alloys, metals, and ceramics assessed by Millipore fil- M.G. & Wilson, T.G. (2014) Detoxification of
ter, agar overlay, and MTT tests. Scandinavian Insti- implant surfaces affected by peri-implant disease:
tute of Dental Materials, Haslum, Norway, 2000. an overview of non-surgical methods. Open Dental
Souza JCM, Barbosa SL, Ariza E, Celis J-P, Rocha LA. Journal 8: 77–84.
Simultaneous degradation by corrosion and wear
9
Biodental Engineering IV – Natal Jorge et al. (Eds)
© 2018 Taylor & Francis Group, London, ISBN 978-1-138-05737-1
F.S. Silva
MEMS, Universidade do Minho, Guimarães, Portugal
ABSTRACT: Zirconia is widely used as ceramic material, mainly because of its high mechanical prop-
erties, accounted by a martensitic phase transformation. However, a combination of events can affect
zirconia properties, reducing and making hard to predict its lifetime under wet environments. To prevent
this behavior some strategies have been developed, including using new materials and new processing
techniques. This document will give a brief explanation about zirconia-based materials and the future of
this oxide ceramic as material for dental applications.
11
(>3 mol.%) or by other stabilizers might be signifi-
cantly reduced. Ceria, for instance, can stabilize
the tetragonal phase of zirconia with still appreci-
ated fracture toughness and without aging sensitiv-
ity, Figure 1 (Palmero et al. 2016; Fornabaio et al.
2015; Chevalier 2006).
Hence, there are nowadays three main ways to
avoid zirconia aging:
Yttria fully stabilized microstructure modifi-
cation, using precipitates as alumina, to obtain
small microstructural grains and, as a conse-
quence, ceramic-ceramic composite materi-
als. This approach was mainly used to improve
mechanical properties of hip implants, with the
drawback, for oral applications, of increasing the
Young’s Modulus of the composite (Tebaldo &
Gautier 2013; Perrichon et al. 2016; Nevarez-
Rascon et al. 2009).
Dopant changing, where the mainly challenge
is to obtain good mechanical properties with- Figure 2. Composite of 3 mol.% yttria stabilized zirco-
nia and alumina [13].
out using yttrium oxide (yttria). Here two oxides
have been shown good potential: Cerium oxide
(ceria), with studies coming from hip materials
designs; and magnesium oxide (magnesia), where
a partially stabilized microstructure gives inter-
esting aesthetics along with suitable mechanical
properties to use as crowns (Palmero et al. 2016;
Fornabaio et al. 2015).
Avoid the Y-TZP contact with water, or mois-
ture, by a surface protection layer, using glass
or a codopant, for example, in the surface of
the piece (Marro et al. 2011; Camposilvan et al.
2015). The challenge in this approach is to cre-
ate a homogeneous layer with good mechani-
cal properties, considering that cracks start to
propagate from the surface and that it may dra-
matically impact the mechanical strength of the
materials.
'
NO LTD
1200
m-
a.
~ 1000
.c
c;,
c:
~ 800
u;
600
400
5 9 10 11 12 13 16
Toughness (MPa" m)
12
3 FUTURE TRENDS REFERENCES
As zirconia is still being one of the most reliable Basu, B., 2005. Toughening of yttria-stabilised tetrago-
ceramics, in terms of fracture toughness (KIC), and nal zirconia ceramics. International Materials Reviews,
its properties are also really appreciated, one may 50(4): 239–256.
foresee further improvements based on the strate- Camposilvan, E. et al., 2015. Acta Biomaterialia
Enhanced reliability of yttria-stabilized zirconia for
gies previously described, with more studies being dental applications. Acta Biomaterialia, 17: 36–46.
conducted. Chevalier, J. et al., 2009. The tetragonal-monoclinic
Thinking about dental applications, is possible transformation in zirconia: Lessons learned and
to split the material requirements in two different future trends. Journal of the American Ceramic Soci-
categories: the ones with aesthetical demands and ety, 92(9): 1901–1920.
the others that do not. Chevalier, J., 2006. What future for zirconia as a biomate-
In the first one, where dental prosthesis is the rial? Biomaterials, 27(4): 535–543.
main example, the challenge is how to obtain a Chevalier, J., Gremillard, L. & Deville, S., 2007. Low-
translucent zirconia without losing in mechanical Temperature Degradation of Zirconia and Impli-
cations for Biomedical Implants. Annual Review of
properties and aging resistance. Moreover, because Materials Research, 37(1): 1–32.
of such aesthetical requirements, is not possible Chevalier, J., Olagnon, C. & Fantozzi, G., 1999. Subcriti-
to use ceria as stabilizer, once it has a yellowish cal crack propagation in 3Y-TZP ceramics: static and
color. cyclic fatigue. Journal of American Ceramic Society,
In these aesthetical applications (dental resto- 82(11): 3129–3138.
rations) is also usual to apply a porcelain veneer, Denry, I. & Kelly, J.R., 2014. Emerging Ceramic-based
which masks the white color of zirconia. The Materials for Dentistry. Journal of Dental Research,
future in this application is go for monolithic zir- 93(12): 1235–42.
conia restorations without a surface layer of glass Fornabaio, M. et al., 2015. Zirconia-based composites
for biomedical applications: Role of second phases
or feldspathic porcelain, once most of failures in on composition, microstructure and zirconia trans-
this prosthesis are regarded to fracture and exfo- formability. Journal of the European Ceramic Society,
liation of the veneering material (Denry & Kelly 35(0): 4039–4049.
2014). Monolithic zirconia restorations, exhibiting Marro, F.G. et al., 2011. Surface modification of 3Y-TZP
a gradient in translucency given by the presence of with cerium oxide. Journal of the European Ceramic
different stabilizers over the volume of the zirconia Society, 31(3): 331–338.
part is also being attempted. Miyazaki, T. et al., 2013. Current status of zirconia res-
The second category gives more freedom to toration. Journal of Prosthodontic Research, 57(4):
work with different zirconia based materials, once 236–261.
Nevarez-Rascon, A. et al., 2009. On the wide range of
no teeth—like color or translucency are required. mechanical properties of ZTA and ATZ based dental
In this way, ceria stabilized zirconia is one of the ceramic composites by varying the Al2O3 and ZrO2
most promising materials, especially as a ceramic- content. International Journal of Refractory Metals
ceramic compound. Nevertheless, yttria stabilized and Hard Materials, 27(6): 962–970.
zirconia will be continuously investigated, espe- Palmero, P. et al., 2015. Towards long lasting zirconia-
cially to produce ceramic-ceramic composites, based composites for dental implants. Part I : Innova-
which can have the highest strength for ceramic tive synthesis, microstructural characterization and in
materials. vitro stability. Biomaterials, 50: 38–46.
As a component with higher mechanical Perrichon, A. et al., 2016. A testing protocol combining
shocks, hydrothermal ageing and friction, applied to
requirements than dental crowns, and also because Zirconia Toughened Alumina (ZTA) hip implants.
of their traumatic replacement, dental implants Journal of the Mechanical Behavior of Biomedical
need to be tested under compatible in-service con- Materials, 65(July 2016): 600–608.
ditions, namely those where zirconia have shown Schubert, H. & Frey, F., 2005. Stability of Y-TZP dur-
special problems: the LTD and subcritical crack ing hydrothermal treatment: Neutron experiments
growth, which is like stress corrosion for some and stability considerations. Journal of the European
oxides ceramics. Ceramic Society, 25(9): 1597–1602.
For both applications (aesthetical and mechani- Tebaldo, V. & Gautier, G., 2013. Influences of evalua-
cal), it is likely that zirconia will be, in few years, tion methods and testing load on microhardness and
Young’s modulus of ZTA and ATZ ceramics. Ceram-
the gold standard material, replacing titanium ics International, 39(3): 2683–2693.
alloys and disilicates. However, to make it possi-
ble, researchers and scientists have to handle some
of the challenges previously reported, using new
materials and processing techniques.
13
Biodental Engineering IV – Natal Jorge et al. (Eds)
© 2018 Taylor & Francis Group, London, ISBN 978-1-138-05737-1
E. Correia
DDS, Faculty of Dental Medicine of the University of Porto (FMDUP), Portugal
P. Vaz
Fixed Prosthodontics, Medical and Orofacial Genetics, FMDUP, Portugal
ABSTRACT: Tooth preparation for fixed prosthesis should take into account some principles in order
to obtain regular surfaces and smooth textures on the cervical surface. This way it will be possible to
achieve uniform prosthesis seating on the tooth structure and the best marginal adaptation, contribut-
ing to the fixed prosthesis durability. The surface regularization (that allows the surface finishing) may
be performed by different methods and instruments, which may show different results. Eleven teeth were
embedded in epoxy resin and finished with different instruments: ultrasonic tip, fine grain diamond burs
assembled to turbineand to a multiplier handpiece. The samples were analyzed with SEM and the results
subjected to Mann-Whitney test to determine statistical significance. The best results for this surface
preparation were obtained using fine grain diamond burs assembled to a multiplier handpiece or through
an ultrasonic tip.
15
3 RESULTS AND DISCUSSION
4 CONCLUSIONS
REFERENCES
16
Another random document with
no related content on Scribd:
The Project Gutenberg eBook of Knights and
their days
This ebook is for the use of anyone anywhere in the United
States and most other parts of the world at no cost and with
almost no restrictions whatsoever. You may copy it, give it away
or re-use it under the terms of the Project Gutenberg License
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laws of the country where you are located before using this
eBook.
Language: English
A N D T H E I R D AY S
BY DR. DORAN
AUTHOR OF “LIVES OF THE QUEENS OF ENGLAND OF THE HOUSE OF HANOVER,”
“TABLE TRAITS,” “HABITS AND MEN,” ETC.
REDFIELD
3 4 B E E K M A N S T R E E T, N E W Y O R K
1856
TO
Is inscribed
BY HIS VERY SINCERE FRIEND,
THE AUTHOR.
CONTENTS.
PAGE
A FRAGMENTARY PROLOGUE
9
THE TRAINING OF PAGES 30
KNIGHTS AT HOME 36
LOVE IN CHEVALIERS, AND CHEVALIERS IN LOVE 51
DUELLING, DEATH, AND BURIAL 65
THE KNIGHTS WHO “GREW TIRED OF IT” 78
FEMALE KNIGHTS AND JEANNE DARC 104
THE CHAMPIONS OF CHRISTENDOM 113
SIR GUY OF WARWICK, AND WHAT BEFELL HIM 133
GARTERIANA 148
FOREIGN KNIGHTS OF THE GARTER 170
THE POOR KNIGHTS OF WINDSOR, AND THEIR DOINGS 184
THE KNIGHTS OF THE SAINTE AMPOULE 194
THE ORDER OF THE HOLY GHOST 200
JACQUES DE LELAING 208
THE FORTUNES OF A KNIGHTLY FAMILY 228
THE RECORD OF RAMBOUILLET 263
SIR JOHN FALSTAFF 276
STAGE KNIGHTS 295
STAGE LADIES, AND THE ROMANCE OF HISTORY 312
THE KINGS OF ENGLAND AS KNIGHTS; FROM THE NORMANS TO
THE
STUARTS 329
“THE INSTITUTION OF A GENTLEMAN” 351
THE KINGS OF ENGLAND AS KNIGHTS; THE STUARTS 358
THE SPANISH MATCH 364
THE KINGS OF ENGLAND AS KNIGHTS; FROM STUART TO
375
BRUNSWICK
RECIPIENTS OF KNIGHTHOOD 388
RICHARD CARR, PAGE, AND GUY FAUX, ESQUIRE 410
ULRICH VON HUTTEN 420
SHAM KNIGHTS 439
PIECES OF ARMOR 455
THE
Dr. Lingard, when adverting to the sons of Henry II., and their
knightly practices, remarks that although chivalry was considered the
school of honor and probity, there was not overmuch of those or of
any other virtues to be found among the members of the chivalrous
orders. He names the vices that were more common, as he thinks,
and probably with some justice. Hallam, on the other hand, looks on
the institution of chivalry as the best school of moral discipline in the
Middle Ages: and as the great and influential source of human
improvement. “It preserved,” he says, “an exquisite sense of honor,
which in its results worked as great effects as either of the powerful
spirits of liberty and religion, which have given a predominant
impulse to the moral sentiments and energies of mankind.”
The custom of receiving arms at the age of manhood is supposed,
by the same author, to have been established among the nations
that overthrew the Roman Empire; and he cites the familiar passage
from Tacitus, descriptive of this custom among the Germans. At first,
little but bodily strength seems to have been required on the part of
the candidate. The qualifications and the forms of investiture
changed or improved with the times.
In a general sense, chivalry, according to Hallam, may be referred to
the age of Charlemagne, when the Caballarii, or horsemen, became
the distinctive appellation of those feudal tenants and allodial
proprietors who were bound to serve on horseback. When these
were equipped and formally appointed to their martial duties, they
were, in point of fact, knights, with so far more incentives to
distinction than modern soldiers, that each man depended on
himself, and not on the general body. Except in certain cases, the
individual has now but few chances of distinction; and knighthood, in
its solitary aspect, may be said to have been blown up by
gunpowder.
As examples of the true knightly spirit in ancient times, Mr. Hallam
cites Achilles, who had a supreme indifference for the question of
what side he fought upon, had a strong affection for a friend, and
looked at death calmly. I think Mr. Hallam over-rates the bully Greek
considerably. His instance of the Cid Ruy Diaz, as a perfect
specimen of what the modern knight ought to have been, is less to
be gainsaid.
In old times, as in later days, there were knights who acquired the
appellation by favor rather than service; or by a compelled rather
than a voluntary service. The old landholders, the Caballarii, or
Milites, as they came to be called, were landholders who followed
their lord to the field, by feudal obligation: paying their rent, or part of
it, by such service. The voluntary knights were those “younger
brothers,” perhaps, who sought to amend their indifferent fortunes by
joining the banner of some lord. These were not legally knights, but
they might win the honor by their prowess; and thus in arms, dress,
and title, the younger brother became the equal of the wealthy
landholders. He became even their superior, in one sense, for as Mr.
Hallam adds:—“The territorial knights became by degrees ashamed
of assuming a title which the others had won by merit, till they
themselves could challenge it by real desert.”
The connection of knighthood with feudal tenure was much
loosened, if it did not altogether disappear, by the Crusades. There
the knights were chiefly volunteers who served for pay: all feudal
service there was out of the question. Its connection with religion
was, on the other hand, much increased, particularly among the
Norman knights who had not hitherto, like the Anglo-Saxons, looked
upon chivalric investiture as necessarily a religious ceremony. The
crusaders made religious professors, at least, of all knights, and
never was one of these present at the reading of the gospel, without
holding the point of his sword toward the book, in testimony of his
desire to uphold what it taught by force of arms. From this time the
passage into knighthood was a solemn ceremony; the candidate was
belted, white-robed, and absolved after due confession, when his
sword was blessed, and Heaven was supposed to be its director.
With the love of God was combined love for the ladies. What was
implied was that the knight should display courtesy, gallantry, and
readiness to defend, wherever those services were required by
defenceless women. Where such was bounden duty—but many
knights did not so understand it—there was an increase of
refinement in society; and probably there is nothing overcharged in
the old ballad which tells us of a feast at Perceforest, where eight
hundred knights sat at a feast, each of them with a lady at his side,
eating off the same plate; the then fashionable sign of a refined
friendship, mingled with a spirit of gallantry. That the husbands
occasionally looked with uneasiness upon this arrangement, is
illustrated in the unreasonably jealous husband in the romance of
“Lancelot du Lac;” but, as the lady tells him, he had little right to cavil
at all, for it was an age since any knight had eaten with her off the
same plate.
Among the Romans the word virtue implied both virtue and valor—as
if bravery in a man were the same thing as virtue in a woman. It
certainly did not signify among Roman knights that a brave man was
necessarily virtuous. In more recent times the word gallantry has
been made also to take a double meaning, implying not only courage
in man, but his courtesy toward woman. Both in ancient and modern
times, however, the words, or their meanings, have been much
abused. At a more recent period, perhaps, gallantry was never better
illustrated than when in an encounter by hostile squadrons near
Cherbourg, the adverse factions stood still, on a knight, wearing the
colors of his mistress, advancing from the ranks of one party, and
challenging to single combat the cavalier in the opposite ranks who
was the most deeply in love with his mistress. There was no lack of
adversaries, and the amorous knights fell on one another with a fury
little akin to love.
A knight thus slain for his love was duly honored by his lady and
contemporaries. Thus we read in the history of Gyron le Courtois,
that the chivalric king so named, with his royal cousin Melyadus, a
knight, by way of equerry, and a maiden, went together in search of
the body of a chevalier who had fallen pour les beaux yeux of that