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Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020

Project Name: Date: 14 Jan 2011


Contract Number: Page: 1 of 22
Revision: 1

SPECIFICATION – GAS CHROMATOGRAPHS

This specification has been revised as indicated below and described in the revision record on the following
page. Please destroy all previous revisions.

Revision Date Originator's Reviewed/Checked By Pages


No. Name & Initials Name & Initials
A 7/28/2010 Cory A. Haynes Vincent E. Mezzano 23
0 11/04/2010 Cory A. Haynes Anna M. Pham 21
1 1/14/2011 Cory A. Haynes Anna M. Pham 22

APPROVALS SIGNATURES DATE

Lead Engineer Thomas B. Robinson


Project Manager: Russell Shulz
Client Approval:

ISSUED FOR : Construction X Other Approved


Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

Record of Revisions
Revision
No. Date Description

A 7/28/2010 Issued for Approval, Table of Contents Only

0 11/04/2010 Issued for Review/Approval

1 1/14/2011 Issued Approved


Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
Contract Number: Page: 3 of 22
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SPECIFICATION – GAS CHROMATOGRAPHS

TABLE OF CONTENTS

Section

1.0 GENERAL......................................................................................................................................................... 5
1.1 SCOPE OF SPECIFICATION ........................................................................................................ 5
1.2 EXCLUSIONS.................................................................................................................................... 5
1.3 REFERENCES................................................................................................................................... 5
1.4 SUPPLIER RESPONSIBILITES .................................................................................................... 7
1.5 SAFEGUARDING ............................................................................................................................. 7
1.6 TECHNICAL REQUIREMENTS................................................................................................... 7
1.7 CONFLICTING REQUIREMENTS .............................................................................................. 8
1.8 TRAINING ......................................................................................................................................... 8
2.0 PRODUCTS ...................................................................................................................................................... 8
2.1 GENERAL DESIGN REQUIREMENTS....................................................................................... 8
2.2 REQUIREMENTS FOR ELECTRICAL AND ELECTRONIC DEVICES.............................. 9
2.3 FUNCTIONAL DESIGN ................................................................................................................10
2.4 MATERIALS ...................................................................................................................................10
2.5 DETAILED SPECIFICATIONS....................................................................................................11
2.6 SAMPLE CONDITIONING SYSTEMS (SCS) ...........................................................................11
2.7 ANALYZER......................................................................................................................................12
2.8 PROGRAMMER / CONTROLLER .............................................................................................12
2.9 MAINTENANCE.............................................................................................................................13
2.10 OUTPUT SIGNALS ........................................................................................................................13
2.11 CARRIER, FUEL GAS, AND CALIBRATION STANDARD CYLINDERS .........................16
2.12 COMMUNICATION DATA HIGHWAY....................................................................................16
2.13 PERIPHERAL EQUIPMENT .......................................................................................................16
3.0 EXECUTION ..................................................................................................................................................17
3.1 DOCUMENTATION ......................................................................................................................17
3.2 SPARE PARTS ................................................................................................................................17
3.3 QUALITY ASSURANCE ...............................................................................................................18
3.4 INSPECTION AND TESTING......................................................................................................18
3.5 INDENTIFICATION AND TAGGING........................................................................................21
3.6 PREPARATION FOR SHIPPING................................................................................................22
4.0 ATTACHMENTS...........................................................................................................................................22
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

4.1 Process Industry Practices (PIP)....................................................................................................22


4.2 Datasheets .........................................................................................................................................22
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

1.0 GENERAL

1.1 SCOPE OF SPECIFICATION

A. This Specification, together with Instrument Data Sheets, and Procurement


Documents, details MARAFIQ’s minimum requirements for engineering, design,
supply and/or fabrication, inspection, testing, storage, shipment, training and
maintenance of Process Gas Chromatograph Systems and associated services.

1.2 EXCLUSIONS

A. Sample conditioning systems, shelters, calibration standards, zero and span gases are
to be provided by others.

1.3 REFERENCES

A. This Specification is based on and incorporates by direct reference and/or inference


accepted documents pertinent to control systems engineering and designs, including
but not limited to:

1. Industry codes, standards, and practices prepared and issued by, engineering
societies, industry associations, manufacturer's associations, and insurance
company groups.

2. Laws, regulations, directives prepared and issued by national and local


governing agencies.

3. Engineering and/or design specifications prepared and issued by other


engineering divisions.

B. Any other codes, standards, or practices in addition to or instead of those listed in


this specification that are required for a project will be listed in an attachment to this
specification.

C. Latest edition of publications listed below, form part of this Specification.

D. Industry Association Codes, Standards and Recommended Practices

Applicable industry association codes, standards, and practices referenced in and/or


pertinent to this specification are:
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Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

1. Process Industry Practices (PIP)

 PCTPA001 : Testing of Process Analyzer Systems.

 PCEPA003 : Process Analyzer System Field Installation Guideline.

 PCEPA002 : Process Analyzer Project Implementation Guidelines.

 PCEPA001 : Process Analyzer System Engineering Guidelines.

 PCCPA001 : Process Analyzer System Design Criteria.

2. American Petroleum Institute (API)

 RP-500 : Recommended Practice for Classification of Locations for


Electrical Installations at Petroleum Facilities Classified as Class
I, Division 1 and Division 2

 RP-555 : Process Analyzers

3. National Association of Corrosion Engineers (NACE)

 NACE MR-0175 : Sulfide Stress Cracking Resistant Metallic Materials for


Oil Field Equipment

4. Instrumentation, Systems, and Automation Society (ISA)

 ISA 12.01.01 : Electrical Instruments in Hazardous Areas

 ISA RP 12.4 : Pressurized Enclosures

5. National Electrical Manufacturers Association (NEMA)

 NEMA ISC6 : Enclosures for Industrial Controls and Systems

6. National Fire Protection Association (NFPA)

 NFPA 70 : National Electrical Code (NEC)

7. Underwriters Laboratories, Inc. (UL)

 UL 698 : Standard for Industrial Control Panels Relating to Hazardous


(Classified) Locations
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
Contract Number: Page: 7 of 22
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SPECIFICATION – GAS CHROMATOGRAPHS

1.4 SUPPLIER RESPONSIBILITES

A. The primary responsibility of the analyzer Seller is to provide the equipment and
services as detailed in this specification in such a manner that ensures the safety of
personnel during the construction, commissioning, routine operation, maintenance
and troubleshooting of the analyzer system.

1.5 SAFEGUARDING

A. The analyzer design shall make provision to minimize personnel exposure to toxic,
corrosive or otherwise hazardous substances and cold and hot materials.

B. Safeguarding (e.g., relief valves) shall be incorporated into analyzer design to resolve
the dangerous consequences of an analyzer system component (e.g., pressure
regulator) or subsystem failure and to provide for the detection and alarm of such
failures as specified herein.

1.6 TECHNICAL REQUIREMENTS

A. The analyzer Seller shall provide the following:

1. The analyzers listed in the Instrument Data Sheet(s).

2. The submittals listed in the Process Analyzer Submittal Requirements List.

3. The associated additional equipment listed in the Process Analyzer Additional


Equipment List.

4. The services to be provided as per the Process Analyzer Service Requirements


List subject to the following additional requirements:

a. All equipment and services identified above, to be provided by the analyzer


Seller, shall meet the requirements of this Specification and any
specifications and/or standards referenced herein.
b. All equipment design and installation, in no way abrogates any equipment
manufacturers warrantees or guarantees.
c. The analyzers that are provided shall be fully functional regardless of
whether or not MARAFIQ has reviewed and approved the design or
documentation.

5. The analyzer systems Seller shall base the design upon the data specified in the
Process Analyzer Data Sheet(s).
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

6. It is further the responsibility of the analyzer Seller to identify and resolve


conflicts between the data sheets, requirement lists, and the remainder of this
Specification and between any requirements which in the Seller’s opinion are not
cost effective or technically feasible.

1.7 CONFLICTING REQUIREMENTS

A. Although advantageous, innovative technical designs by the analyzer Seller are


encouraged, any deviation from the requirements of this Specification or the
applicable codes, requires the written approval of MARAFIQ.

B. At the proposal stage of the project, such alternative designs shall only be offered as
options and shall be identified as such. The base proposal shall meet all the
requirements of this specification.

C. At the execution stage of the project, the analyzer Seller shall report to the
MARAFIQ such conflicts for clarification in order to avoid delays in completion of
the work.

1.8 TRAINING

The training requirements of the site analyzer technicians, technologists, and


supervisors with respect to the proper operation, maintenance, and trouble-shooting
of the equipment to be provided shall be identified and provided as part of the
analyzer Sellers proposals. These training requirements shall be detailed in terms of
costs, schedules, and pre-requisites (if any).

2.0 PRODUCTS

2.1 GENERAL DESIGN REQUIREMENTS

A. The analyzers provided shall meet the following:

1. Analyzers shall be suitable for process and upset conditions as well as process
design conditions as detailed in the Process Analyzer Data Sheets.
2. Analyzers shall utilize materials of construction and components with the proper
pressure, temperature, and corrosion ratings
3. The analyzer system, as a whole, shall be capable of providing the desired
measurement as specified in the Analyzer Data Sheets with regard to the proper
format, time response, precision, and accuracy, while doing so in a safe and
maintainable manner.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

4. Equipment design shall follow good engineering practice and meet the
requirements of this specification, in addition to, all applicable codes and
standards.
5. Equipment shall be suitable for the environmental conditions to be encountered
during its fabrication, assembly, job-site storage, and after installation.
6. Components of any analyzer subassembly that require removal for maintenance
shall be removable without having to disassemble any other components.

2.2 REQUIREMENTS FOR ELECTRICAL AND ELECTRONIC DEVICES

A. The requirements of this Section shall apply to all electrical or electronic devices,
components and materials utilized in analyzer systems whether this Section is
referenced explicitly or not.

B. All electrical equipment shall be suitable for the power supplies identified in the
Process Analyzer Data Sheet.

C. The overall electrical design of analyzers as well as all electrical and electronic
devices, their associated components, and materials shall conform to NEC
requirements, as dictated by NFPA 70.

D. For hazardous locations as defined in NFPA 70, the devices shall be approved for the
classification of the particular area in which they are to be installed and shall be so
indicated.

E. The use of non-incendive equipment is preferred. If this is not possible, the use of
purging to meet the area classification requirements of the installation is permitted.

F. Approvals

1. Electrical components or devices which may produce arcs, sparks, or high


temperatures and are intended for operation in locations classified as hazardous
under NFPA 70, Article 500, shall be listed and labeled by the appropriate
approval agencies (i.e.: UL, FM, or CSA).

2. The Seller is responsible for obtaining the appropriate agency approvals for
components that do not meet necessary requirements.

3. Provided the Seller has first obtained written approval from MARAFIQ, the Seller
may obtain special approval for components for which it may be impractical to
obtain typical agency approvals.

G. Area Classifications
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

1. The specific area class, zone, and group(s) for each analyzer system shall be as
specified in the Analyzer Data Sheets for the analyzers and/or the area
classification plot plan for each enclosure.

H. Purging

1. Analyzers or other electrical or electronic components that require air purges to


reduce the classification within an electrical enclosure from either Zone One or
Zone Two to General Purpose, shall be provided with air purges, in accordance the
guidelines contained in ISA 12.01.01 and ISA RP12.4.

2. As a minimum requirement, enclosures shall conform to NEMA ICS6, Type 4,


unless otherwise specified by the Analyzer Data Sheets.

I. Non-Incendive Equipment

1. Electrical equipment and associated circuits designated as suitable for installation


in a Zone 2 hazardous area, by virtue of it being non-incendive, shall meet the
requirements of the NEC, as dictated in NFPA 70, for non-incendive devices. Non-
incendive electrical equipment shall not be used for an area rated as Class I / Zone
1.

2. Cables and wiring for non-incendive circuits shall also meet NEC requirements, as
dictated by NFPA 70.

2.3 FUNCTIONAL DESIGN

A. Functional design of an analyzer system to meet the requirements detailed in this


specification and/or specified in the instruments data sheets taking into account the
listed process conditions rests with the Seller.

2.4 MATERIALS

A. General

1. All wetted parts shall be constructed of 316L stainless steel, unless otherwise
specified, or if stainless steel is deemed an unsuitable material.

2. Thermal insulation (e.g., glass fibre, mineral wool) used for insulation of stainless
steel components such as heat traced tubing shall be free of water soluble chlorides
(i.e., not to exceed 10 mg/kg).

3. For corrosive service, other materials should be considered with preference given
to materials such as Incoloy, Monel, and Hastelloy.

4. The use of any material other than stainless steel in wetted service requires the
written approval of MARAFIQ.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
Contract Number: Page: 11 of 22
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SPECIFICATION – GAS CHROMATOGRAPHS

B. Compression Fittings

1. All components shall be selected so that only Swagelok compression fittings


are used.

2. Provisions shall be made for the use of Teflon tape (PTFE) for those
applications where prevention of seizing and leakage of NPT threaded
connections is required, provided the design temperature of these connections
is in the range of -100C to 200C. The Teflon tape shall not be applied to the
first two threads. Anaerobic pipe thread sealant is to be used only where
absolutely required and then in minimum amounts. Any excess should be
wiped clean with a solvent.

2.5 DETAILED SPECIFICATIONS

A. Specific requirements for each analyzer, such as stream components, stream


temperature and pressure, stream physical properties (i.e., specific gravity, dew point,
etc.), and analysis time, shall be as specified on the instrument data sheets.

B. The analyzer system shall be engineered, designed, and assembled in such a manner
as to perform continuous, automatic, unattended analysis in the minimum cycle time,
without compromising maintainability.

2.6 SAMPLE CONDITIONING SYSTEMS (SCS)

A. The sample handling and conditioning subassembly shall be furnished by others.

B. It is the Sellers responsibility to review MARAFIQ’s SCS design for functionality


and satisfactory operation with the proposed analyzer. The Sellers responsibilities
will include:

1. Review process data contained on analyzer data sheets,


2. Review MARAFIQ’s SCS design and recommend improvements based on
applicable experience or changes where required to ensure the sample
conditioning system will prepare the sample for the analyzer inlet conditions and
accept the analyzer effluent at the analyzer outlet conditions.
3. Provide required analyzer inlet and outlet operating conditions including
temperature, pressure and flow.

C. Where liquid sample injection is specified or proposed by the Seller. The Seller shall
carry out the necessary flash calculations to verify that the sample remains in the
liquid state at the chromatograph injection valve. If required the Seller shall provide
the necessary components to control backpressure on the valve, above the vapor
pressure of the sampled product, in order to prevent flashing.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

2.7 ANALYZER

A. The analyzer shall be furnished with all the necessary equipment to meet the
performance requirements as specified in the attached data sheets.

B. The selection of columns shall be of a type that will provide adequate separation of
components, minimize analysis time, minimize maintenance time, and meet the
performance requirements of this specification. Baseline separation of all measured
components is preferred to other chromatographic methods. Detector selection shall
be based upon the type required to accurately measure all components at their
specified range.

C. Analyzer system temperature shall be controlled by an electric, air sparging heating


system to ensure proper sample separation and minimum analysis time. Accuracy of
the electric heating system shall be such as to ensure compliance with the specified
performance of the system.

D. A shutdown switch shall be provided to protect the analyzer from loss of carrier gas
or fuel gas, should such loss of utility gas result in damage to the analyzer.

E. Solenoid/air operated multifunction valves for sample inject and column switching
shall be provided.

F. All Fire Ionization Detector (FID) based analyzers shall be provided with a catalytic
air treater, for combustion air.

G. Provisions to adjust column and detector flows without the need to open the oven
compartment shall be provided.

H. The analyzer shall be of a stand-alone, wall mounted design with an integral


microprocessor capable of performing the required control, data collection, data
reduction and communication functions independent of a central controller.

I. Column/detector life shall be a minimum of twelve months.

J. Electronic Pressure Control (EPC) shall be provided as a standard on all gas


chromatographs.

2.8 PROGRAMMER / CONTROLLER

A. The programmer/controller shall be microprocessor-based and shall be furnished


with all the equipment necessary to properly control the analysis cycle, the automatic
zero adjustment circuit, the calibration of the analyzer and programmer systems and
the transmission of data to a distributed control system or digital computer and any
required peripheral equipment as specified on the instrument data sheets.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

B. Visual readout shall be provided to identify each component being analyzed and each
step in the program as well as displaying the latest readings.

C. All program data tables shall be capable of field modification without user
knowledge of higher level programming. A key-lock switch or field alterable
password shall be provided to limit access to system software by unauthorized
personnel.

D. The application program in the analyzer shall be retained for a minimum of six
months without external power by the use of E2PROM, flash PROM or battery
backup. Alternate methods of long-term program storage may be submitted by the
Seller for consideration.

E. Maintenance diagnostics shall be included in the software system to allow rapid


troubleshooting in the event of system malfunction. Alarms shall be provided to
notify the operator in the event of a malfunction. A low carrier flow alarm shall be
included.

F. Data reduction capabilities within the programmer/controller software shall be


available as specified on the instrument data sheets.

2.9 MAINTENANCE

A. Analyzer systems shall incorporate designs and components that utilize


microprocessors based controllers with self-diagnostic capability to facilitate the
maintenance of analytical systems.

B. The analyzer systems Seller shall identify any special tools and materials (excludes
common tools and materials) required to maintain the analyzers or associated
equipment to be provided as part of the proposal.

2.10 OUTPUT SIGNALS

A. Analyzer analog, alarm signal and serial communications equipment shall meet the
requirements detailed in the Process Analyzer Data Sheets and also the requirements
of this section.

B. The use of supplementary, signal conditioning devices should be avoided whenever


possible.

C. For the purpose of brevity and clarity, in this sub-section of this Specification, the
term "host computer" shall signify all or any of the devices that might be interfaced
to an analyzer for the purpose of unidirectional or bi-directional data or analyzer
command transfer (e.g., distributed control system computer, trend recorder, loop
controller, PLC, printer or personnel computer).
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

D. All components and equipment utilized in the analyzer communications system shall
meet the requirements of the analyzer manufacturer and of the manufacturer of the
host computer to which the analyzer is to interface.

E. The Seller shall identify in the bid documents the following:

1. All software (if applicable), components (e.g., interface boards), materials (e.g.,
conductors) and the specifications and prices of same that would be required to
fulfil the functional and other communication requirements of the project
specification;
2. For digital links, the communications protocol and effective data transfer rate;
3. Any incompatibilities between the analyzers and the host computer to which the
analyzers are to interface;
4. Any limitations of the communications equipment with regard to radio
frequency (RFI) or electromagnetic interference (EMI).
F. Separate 4-20 milliamp isolated analog outputs to the distributed control system shall
be provided for each measurement or calculated value, when specified on the
analyzer data sheets. External load capability shall be at least 1000 ohms.

G. Digital serial data transmission outputs to a host computer shall be available via a
serial interface link as specified on the instrument data sheets. The serial data
transmission shall be available from any point on the chromatograph system or data
highway. Modbus and/or Modbus Plus protocols shall also be available. All
applicable data including but not limited to component analyses, calculated values,
alarms, stream identification, date and time, shall be available for transmission on the
serial data link.

H. If required, contact closures of the SPDT contact type shall be provided to identify
the stream being analyzed by multi-stream analyzers. Contact ratings shall be as
shown on the instrument data sheets.

I. A built-in dual high and low setpoint alarm with SPDT contacts unless otherwise
specified shall be available for each component of interest. Contact ratings shall be
as shown on the instrument data sheets.

J. Analog Signals

1. Analyzer analog output signals shall meet the following requirements:

a. Utilize a 4-20 mA dc signal


b. Capable of driving an external load of 1 000 ohms minimum
c. Long term (six months) drift of 0.1% of full scale maximum
d. Accuracy of 0.05% of full scale, minimum, including the effects of
precision and temperature
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Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

e. Calibration capability for zero and full scale outputs of +/- 1% of full scale
f. Under-range capability of -2% of full scale and over-range capability of
+2% of full scale.

K. Digital Signals

1. Digital data transfer systems shall meet the following requirements:

a. Utilize standard communication protocols and specifications


b. Utilize interface devices at both the analyzer and host computer terminations
that are standard products of the respective manufactures
c. Utilize a controlling device and protocol which ensures that data flows in an
orderly manner and is capable of detecting and responding to malfunctions
related to the data link or highway
d. Preferably utilize proven software (e.g., drivers and data handlers)
e. Utilize wiring that meets the requirements of the analyzer Seller and the host
computer Seller.

L. Discrete Signals

1. Discrete outputs shall fail upon power loss or open circuit to a predictable state
(preferably to an open circuit state) consistent with the design of the analyzer
system.

2. Interposing relays, if required, shall be of plug-in, sealed type construction with


SPDT arrangement minimum.

3. All discrete outputs and inputs shall be hermetically sealed and electrically
isolated from each other and from the system circuitry and shall have provision
for arc suppression circuitry on all contacts.

M. Fieldbus Foundation

1. Analyzers outputs shall preferably conform to Fieldbus Foundation H1


specifications, ITK4.x certified tested , or being capable of providing 2 wire loop
powered 4-20 mA HART addressable signal from 24 VDC input with external
loop resistance of no more than 600 ohms, scalable within the operating limits of
the transmitter or measurement device. Each analyzer shall have independent
and non-interactive zero and span adjustment and shall be capable of, as a
minimum, being remotely configured, allow checking of output signal without
interrupting the loop operation, user selectable failure mode, as well as to allow
entry of operating parameters and transmitter identification.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
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SPECIFICATION – GAS CHROMATOGRAPHS

2.11 CARRIER, FUEL GAS, AND CALIBRATION STANDARD CYLINDERS

A. The Seller shall detail in the quotation the quality of span and zero gases that the
analyzer requires to meet the performance specification. An estimate of annual usage
of each type of gas per analyzer shall also be provided.

B. All carrier, fuel and calibration gases will be purchased by others.

C. The Seller shall detail in the quotation the time period over which each calibration
cylinder contents will be stable.

2.12 COMMUNICATION DATA HIGHWAY

A. A communication data highway consisting of a network interface unit and cable


termination devices shall be provided when specified on the instrument data sheets.
This data highway shall provide an interface between the analyzer and various
external intelligent devices. These devices may include the following:

1. Other analyzers
2. Electronic controllers
3. Operator interface units
4. Personal computers or Work Stations
5. Printers
6. Modems
7. Distributed Control System or Digital Computer
8. Programmable Logic Controller
9. Local Area Networks

B. The data highway shall be provided with redundant communication capabilities as


well as intelligent device failure detection capabilities.

2.13 PERIPHERAL EQUIPMENT

A. Peripheral equipment, such as printers, PC’s etc., shall be provided by the Seller,
when specified on the analyzer Data Sheet.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
Contract Number: Page: 17 of 22
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SPECIFICATION – GAS CHROMATOGRAPHS

3.0 EXECUTION

3.1 DOCUMENTATION

A. Documentation shall meet the requirements as detailed in the SDDC - Seller


Drawing and Data Commitment form and shall also meet the requirements of this
section.

B. Approval of drawings by MARAFIQ does not release the analyzer systems Seller
from the responsibility for proper design and functionality of the analyzer system.

C. The component labeling on all drawings shall be consistent with the labeling on the
component hardware nameplates of the analyzer system and other related drawings.

D. In addition to specifying equipment to be provided by the analyzer systems Seller, all


drawings shall also specify and identify as such, any equipment that is part of the
analyzer system but will be provided or installed by others.

E. Final Drawings, Manuals and Records

1. Analyzer data books shall contain the following for each analyzer.

 Any certificates or licenses required to operate all equipment and


components that comprise the analyzer.
 Recommended priced spare parts list detailing manufacture, model number
of analyzer (if applicable), part or catalogue number, item description,
address and telephone number of supplier, and number to stock.
 Calibration and/or Test Reports
 Analyzer Data and Specification Sheets
1. Instruction manuals detailing the following aspects (as applicable) of the
installed analyzers and associated equipment shall also be provided:

 Installation Details.
 Routine Calibration, Maintenance, and Operation Procedures
 Internal Mechanical and Electrical Details
 Complete Parts List.

3.2 SPARE PARTS

A. Seller shall supply with each quotation; a list of recommended spare parts, which
MARAFIQ should maintain as a minimum at the plant site. The list shall include
descriptions and indicate the cost of each item. Quoted costs shall be current list
prices of the parts as purchased on an individual basis.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
Contract Number: Page: 18 of 22
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SPECIFICATION – GAS CHROMATOGRAPHS

3.3 QUALITY ASSURANCE

A. The Seller shall warrant that the analyzer quoted meets the specifications as outline
in this document and the attached data sheet(s).

B. Any deviation from this specification shall be clearly noted in the Seller’s quotation.

3.4 INSPECTION AND TESTING

A. Inspection of the analyzer and ancillary devices shall be at the discretion of


MARAFIQ or their designated agent.

B. Seller shall be responsible for supplying the inspection and test certificates as part of
the purchase price of the analyzer.

C. Examinations and/or tests may be reviewed and/or witnessed by MARAFIQ or their


authorized agent at the Manufacturer’s or Sellers facility.

D. Each analyzer shall be tested for repeatability for an eight-hour period. The analyzer
will be tested with a calibrated sample that closely resembles the actual process
conditions. The analyzer must meet the quoted repeatability for the entire eight-hour
test period. Any deviations from the repeatability test will require a complete re-
testing of the analyzer for another eight-hour period.

E. Testing shall include all analyzers and ancillary devices interconnected together
simulating a plant environment.

F. General Requirements

1. The analyzer manufacturer and/or analyzer Seller shall meet the inspection and
testing requirements as detailed in the in the Process Analyzer Inspection and
Testing Requirements List and shall also meet the requirements of this section.

2. Leak and pressure testing of all fluid lines and components shall be carried out
utilizing a testing fluid which does not compromise the subsequent operation of
the analyzer or analyzer subsystem.

3. Pressure testing shall be performed at 1.5 times the design pressure of the
system.

G. Detailed Inspection and Testing Requirements

1. For factory acceptance testing, the analyzer Seller shall provide the following
requirements:

 At least two weeks advance notice of scheduled factory testing and


inspections.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
Contract Number: Page: 19 of 22
Revision: 1

SPECIFICATION – GAS CHROMATOGRAPHS

 Details of proposed testing procedures.


 Details of proposed testing documentation.
 All the equipment and materials including calibration/test samples required
to perform the specified inspection and testing at their respective facilities.
 Timely access for MARAFIQ to perform said inspections and witness
testing.

2. When specified, the test program to be completed at the analyzer Seller's facility
shall consist of the following tests as a minimum:

 An eight-hour (minimum) performance test of the analyzer including the


sample conditioning system (if supplied with the analyzer).
 Performance test of all optional equipment (e.g., printers, remote I/O
interfaces, PC’s).
 Performance test of all analog and digital communication links and
transmitters.
 Verification of all analyzer functions (e.g., auto-ranging, alarming) and
capabilities (e.g., diagnostics).

3. When specified, a record of the eight-hour performance test in the form of


charts, reports or trends can be submitted by the analyzer Seller to MARAFIQ in
lieu of the witnessed eight hour performance test. This record shall be fully
documented with time, date, chart speed and where applicable settings, flows,
temperatures and any other information to properly define the operating
conditions.

H. Quality Control Requirements

1. The Seller shall be responsible for all Quality Assurance and Quality Control
activities in carrying out the work. The Seller shall at all times provide
adequate, competent, and qualified supervision and inspection personnel to
ensure that the specified quality of the work is met for the Seller’s scope and all
sub-contracted items.

2. MARAFIQ shall have free access to the Seller’s files at all times, including after
completion of the contract. Equipment may also be subject to random audits by
MARAFIQ or MARAFIQ’s representatives.

3. The following information is required to be submitted with the bid package, and
will be used as part of the bid evaluation process:

 Completed “Quality System Questionnaire”, complete with copies of all


Quality Accreditation (form is provided with bid package).
 Typical Quality Control Plan / Inspection and Test Plan.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
Contract Number: Page: 20 of 22
Revision: 1

SPECIFICATION – GAS CHROMATOGRAPHS

 Proposed Sub-supplier listing complete with Sub-supplier’s Locations and


Quality Accreditation.
 Procedure for Control of Sub-Suppliers, detailing the procedures used to
ensure Sub-suppliers meet purchase order requirements, the level of
Inspection carried out at Sub-supplier’s premises, etc.
 Copy of last period Audit Summary from assessing body.

I. Project Quality Plan

1. The Seller’s Quality Plan shall describe the system that shall determine how the
work is to be undertaken, including but not limited to the following:

 Seller’s Quality Policies


 Description of the Seller’s management system
 Seller’s Organization / Organizational Chart
 Planning and setting of standards
 Measurement of performance
 Audit and review
 Hydrotest Procedures
 Material Certificates
 Material Identification System / Traceability
 Visual Inspection procedures
 Fabrication dimensional measurements procedures / report
 Final Inspection procedures / report
 Painting procedures and reports
 Non-conformance reports

2. The project Quality Plan shall include a Quality Control Plan / Inspection & Test
Plan to control the quality practices and special process procedures relevant to
the manufacturing process. The main part of this Quality Plan will be a schedule
of inspection and test activities.

3. The Seller’s project Quality Plan shall be submitted to MARAFIQ for review
after award of the contract.
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
Contract Number: Page: 21 of 22
Revision: 1

SPECIFICATION – GAS CHROMATOGRAPHS

J. Sub-Seller’s Quality Requirements

1. The Seller shall be responsible for ensuring that its Sub-suppliers comply fully
with the Owner’s quality requirements and that the sub-suppliers management
systems comply with the requirements of the project specifications. This shall,
as a minimum, include review of Sub-supplier’s Quality Control Plans /
Inspection & Test Plans for compliance with Purchase Order and Specification
requirements.

3.5 INDENTIFICATION AND TAGGING

A. Each analyzer shall be furnished with two (2) nameplates fastened with stainless
steel screws.

1. Tag Number Plate - Lamacoid Type

a. Plate shall be clearly engraved with the tag number assigned by MARAFIQ.

b. Nameplates shall comply with the following requirements:

 Be of the engraved type, weatherproof, and resistant to any process


fluids present.
 Be constructed of laminated plastic, 4 mm thick with beveled edges
 Utilize white plastic with black core (i.e., lettering) for general
applications and red plastic with white core (i.e., lettering) for safety
related applications
 Utilize lettering which is a minimum of 3 mm high for general use and
10 mm minimum height for safety related nameplates

c. For those applications where plastic labels are not suitable for reasons of
temperature or chemical compatibility, labels shall be fabricated from
stainless steel.

2. Manufacturer’s Descriptive Nameplate - Stainless Steel

a. Nameplate shall be clearly engraved with the following information:

 Manufacturer’s name
 Model number
 Serial number
 Operating voltage
 Operating current
 CSA designation
Power and Water Utility Company for Jubail and Yanbu (MARAFIQ) Master Specification: MQ-SP-I-7020
Project Name: Date: 14 Jan 2011
Contract Number: Page: 22 of 22
Revision: 1

SPECIFICATION – GAS CHROMATOGRAPHS

B. Individual accessories, such as, system computers, board chassis, external


programming devices, etc. shall be clearly and separately identified with lamacoid
tags bearing instrument tag numbers as shown on the data sheets.

3.6 PREPARATION FOR SHIPPING

A. Threaded and tube openings shall be plugged with suitable protectors to prevent
damage to threads or tubing and prevent the ingress of dirt or packing material.

B. Analyzers shall be prepared for shipment in a manor to avoid damage or atmospheric


corrosion to interior or exterior surfaces while in transit or during storage.

C. Analyzers shall be crated or boxed, at the suppliers discretion unless specified on the
data sheets, in such a fashion to preclude, within reason, damage in transit. The
analyzers shall be isolated from the packing material by means of a plastic vapor
barrier.

D. The crate or box shall be clearly marked with an arrow indicating the correct side up.
If the orientation of the analyzer in transit is critical, the crate shall be provided with
“tip and tell” indicators.

E. Documents, tags or instructions necessary for proper unpacking and protection after
unpacking shall be enclosed and their location marked on the outer covering.

F. Glass columns and electronic boards shall be removed for shipping to prevent
breakage during transit. Items are to be placed in the original boxes, properly packed,
and shipped with the analyzer.

4.0 ATTACHMENTS

4.1 Process Industry Practices (PIP)

A. PCTPA001 Testing of Process Analyzer Systems

B. PCEPA003 Process Analyzer System Field Installation Guideline

C. PCEPA002 Process Analyzer Project Implementation Guidelines

D. PCEPA001 Process Analyzer System Engineering Guidelines

E. PCCPA001 Process Analyzer System Design Criteria

4.2 Datasheets

A. MQ-DS-I-7628 – Gas Chromatographs


COMPLETE REVISION
August 2006

Process Industry Practices


Process Control

PIP PCTPA001
Testing of Process Analyzer Systems
PURPOSE AND USE OF PROCESS INDUSTRY PRACTICES

In an effort to minimize the cost of process industry facilities, this Practice has
been prepared from the technical requirements in the existing standards of major
industrial users, contractors, or standards organizations. By harmonizing these
technical requirements into a single set of Practices, administrative, application, and
engineering costs to both the purchaser and the manufacturer should be reduced. While
this Practice is expected to incorporate the majority of requirements of most users,
individual applications may involve requirements that will be appended to and take
precedence over this Practice. Determinations concerning fitness for purpose and
particular matters or application of the Practice to particular project or engineering
situations should not be made solely on information contained in these materials. The
use of trade names from time to time should not be viewed as an expression of
preference but rather recognized as normal usage in the trade. Other brands having the
same specifications are equally correct and may be substituted for those named. All
Practices or guidelines are intended to be consistent with applicable laws and
regulations including OSHA requirements. To the extent these Practices or guidelines
should conflict with OSHA or other applicable laws or regulations, such laws or
regulations must be followed. Consult an appropriate professional before applying or
acting on any material contained in or suggested by the Practice.

This Practice is subject to revision at any time.

© Process Industry Practices (PIP), Construction Industry Institute, The


University of Texas at Austin, 3925 West Braker Lane (R4500), Austin,
Texas 78759. PIP member companies and subscribers may copy this Practice
for their internal use. Changes, overlays, addenda, or modifications of any
kind are not permitted within any PIP Practice without the express written
authorization of PIP.

PRINTING HISTORY
January 2001 Issued
August 2006 Complete Revision

Not printed with State funds


COMPLETE REVISION
August 2006

Process Industry Practices


Process Control

PIP PCTPA001
Testing of Process Analyzer Systems
Table of Contents

1. Introduction................................. 2
1.1 Purpose ............................................. 2
1.2 Scope................................................. 2

2. References .................................. 2
2.1 Process Industry Practices ................ 2
2.2 Industry Codes and Standards .......... 2
2.3 Other References .............................. 3

3. Definitions ................................... 3

4. Requirements.............................. 3
4.2 Original Equipment Manufacturer
(OEM) Tests ...................................... 4
4.3 Factory Acceptance Tests (FAT)....... 5
4.4 Site Acceptance Tests (SAT) ............ 9

Process Industry Practices Page 1 of 9


PIP PCTPA001 COMPLETE REVISION
Process Analyzer System Acceptance Testing August 2006

1. Introduction

1.1 Purpose
This Practice provides requirements for inspection and acceptance testing of process
analyzer systems and field enclosures.

1.2 Scope
This Practice describes requirements inspection and acceptance tests for process
analyzer systems performed as follows:
a. on process analyzer(s) performed by the OEM
b. on the fabricated process analyzer systems and shelter(s) performed by the
ASV
c. on the installed systems on site as a requirement for turnover to the owner.

2. References
Applicable parts of the following Practices, industry codes and standards, and references
should be considered an integral part of this Practice. The edition in effect on the date of
contract award should be used, except as otherwise noted. Short titles will be used herein
where appropriate.

2.1 Process Industry Practices (PIP)


– PIP PCCPA001 - Process Analyzer System Design Criteria
– PIP PCEPA001 - Process Analyzer System Engineering Guidelines
– PIP PCEPA002 - Process Analyzer Project Implementation Guidelines
– PIP PCSPA001 - Process Analyzer Project Documentation Data Sheet
Instructions
– PIP PCSPA01D - Process Analyzer Project Documentation Data Sheet
– PIP PCSPA002 - Process Analyzer System Data Sheet Instructions
– PIP PCSPA02D - Process Analyzer System Data Sheet
– PIP PCSPA003 - Process Analyzer Shelter Data Sheet Instructions
– PIP PCSPA03D - Process Analyzer Shelter Data Sheet
– PIP PCSPA004 - Process Analyzer System Bid Proposal Data Sheet
Instructions
– PIP PCSPA04D - Process Analyzer System Bid Proposal Data Sheet
– PIP PCIPA001 - Process Analyzer System Field Installation

2.2 Industry Codes and Standards

• National Fire Protection Association (NFPA)


– NFPA 30 - Flammable and Combustibles Liquids Code

Page 2 of 9 Process Industry Practices


COMPLETE REVISION PIP PCTPA001
August 2006 Process Analyzer System Acceptance Testing

– NFPA 70 - National Electrical Code - Latest Edition


– NFPA 496 - Standards for Purged and Pressurized Enclosures for Electrical
Equipment
– NFPA 497 - Classification of Flammable Liquids, Gases, or Vapors and of
Hazardous (Classified) Locations for Electrical Installations in Chemical
Process Areas

2.3 Other References


– Clevett, K.J., Process Analyzer Technology, John Wiley & Sons, NY, NY
– Cornish, D. C. Jepson, G. Smurthwaite, M.J., Sampling Systems for Process
Analyzers, Butterworths, London, England
– Houser, E.A., Principles of Sample Handling and Sample System Design for
Process Analysis, Instrument Society of America, Research Triangle Park, NC
– Lipták, B.G., Instrumentation in the Processing Industries, Chilton Book Co.,
Radnor, PA
– Sherman, R. E., Analytical Instrumentation Practices Guide for Measurement
and Control, Instrument Society of America, Research Triangle Park, NC

3. Definitions
owner: The party who owns the facility wherein the process analyzer systems will be used

4. Requirements

4.1 General

4.1.1 Inspection and acceptance testing of process analyzer systems on a major


capital project can require the participation of only one or several of the
following resource groups:
a. Owner company personnel
b. Engineering & Construction contractor personnel
c. Analyzer System Vendors (ASV)
d. Analyzer Original Equipment Manufacturer (OEM)
4.1.2 Physical inspections shall be performed by both the ASV and the OEM.
4.1.3 Acceptance testing shall be performed at each stage of acquisition and
integration.
4.1.4 Before performing an acceptance test, statistical quality control (SQC)
performance data shall be provided.
4.1.5 If specified on purchaser’s process analyzer system data sheet,
PIP PCSPA02D, system-specific inspections and tests shall be performed
before final inspection.

Process Industry Practices Page 3 of 9


PIP PCTPA001 COMPLETE REVISION
Process Analyzer System Acceptance Testing August 2006

4.2 Original Equipment Manufacturer (OEM) Tests


4.2.1 General
4.2.1.1 OEM tests are acceptance tests performed at the analyzer OEM’s
facility.
4.2.1.2 OEM tests shall have defined and measurable parameters with
repeatability factors or tolerance factors stated in the data sheets or
in engineering notes.
Comment: Examples of these tests are baseline drift,
repeatability, resolution, signal ranges, etc.
4.2.1.3 The analyzer manufacturer shall provide all testing equipment
required.
4.2.1.4 Inspection and acceptance tests at an analyzer OEM shall be limited
to “complex analyzers” or analyzers that require specific
applications engineering or development beyond that which is
normally defined in an OEM’s literature.
4.2.1.5 All analyzers and peripheral support hardware for each analyzer
shall be powered and operational during inspections and tests.
4.2.1.6 The tasks outlined in Sections 4.2.2 through 4.2.4 shall be completed
during this stage of the testing and inspection
4.2.2 Hardware Inspection
4.2.2.1 Visually inspect and verify that the each analyzer meets stated,
specified, or approved outline mounting and dimensions.
4.2.2.2 Visually inspect and verify fit and finish of each analyzer housing,
cabinet, or enclosure.
4.2.2.3 Visually inspect and verify type and location of all electrical and
tubing penetrations of each analyzer housing or cabinet.
4.2.2.4 Visually inspect and verify conformance to approved
interconnecting diagrams for electrical and signal wiring.
4.2.2.5 Visually inspect and verify conformance to specified materials of
construction.
4.2.2.6 Visually inspect and verify conformance to specified utility and
safety alarm relay and indication systems.
4.2.2.7 Visually inspect and verify conformance of equipment to specified
electrical specifications.
4.2.2.8 Visually inspect and verify conformance of equipment to specified
electrical area classification to include, e.g., Underwriter Laboratory
(UL) labeling, Factory Mutual (FM), and Canada Safety Association
(CSA) approvals.
4.2.2.9 Verify presence of all required accessories and options.

Page 4 of 9 Process Industry Practices


COMPLETE REVISION PIP PCTPA001
August 2006 Process Analyzer System Acceptance Testing

4.2.2.10 Visually verify presence and conformance to specified wire tags,


labels, and equipment tag numbers.
4.2.3 Analyzer Performance Tests
4.2.3.1 Witness and verify operation and calibration of all inputs and
outputs.
4.2.3.2 Witness and verify zero and span calibration with known standards.
a. Witness and verify acceptable or specified signal-to-noise ratio.
b. Witness and verify stability (drift) and reproducibility runs
against stated specifications.
c. Witness and verify that the analyzer meets required linearity.
d. Witness and verify analyzer response time against
specification.
4.2.3.3 Witness and verify acceptable compensation for stated background
interferences.
4.2.3.4 Witness and verify operation and performance of internal
diagnostics.
4.2.3.5 Verify operating software version number against specifications.
4.2.3.6 Functionally test all alarm and alarm indication circuits.
4.2.3.7 Verify SQC data against performance requirements.
4.2.4 OEM Test Documentation
4.2.4.1 Review and verify that all required documentation is complete and
in acceptable format.
4.2.4.2 Obtain signoff by owner, or by owner-authorized agent, of
inspection discrepancies (punch list).
a.. The punch list shall define items for correction, acknowledged
exceptions, or deficiencies.
b. The signoff shall include timing for satisfactory resolution of
all items by responsible organization.
4.2.4.3 Re-inspect as required to ensure compliance and note all deficiencies
on the punch list.

4.3 Factory Acceptance Tests (FAT)


4.3.1 General
4.3.1.1 FATs are performed at the ASV’s facility after complete fabrication
and assembly of the analyzer system(s).
4.3.1.2 These tests shall have defined and measurable parameters that
encompass the complete analyzer system including any support
peripherals such as analyzer shelters or buildings and all ancillary
equipment.

Process Industry Practices Page 5 of 9


PIP PCTPA001 COMPLETE REVISION
Process Analyzer System Acceptance Testing August 2006

4.3.1.3 Reviewing documentation and conducting physical inspection for


compliance to codes and standards plus adherence to the analyzer
system engineering specification shall be part of this acceptance test.
4.3.1.4 The ASV shall supply all equipment required for testing, e.g., air
velocity, shelter interior sound levels, steam generators, etc.
4.3.1.5 Sample transport and sample conditioning systems are normally
custom engineered and fabricated by the analyzer OEM or ASV and
shall require inspection and acceptance testing.
4.3.1.6 Analyzer system shelters are normally custom-engineered and
fabricated by the analyzer OEM or an ASV and shall require
inspection and acceptance testing.
4.3.1.7 All analyzers and peripheral support hardware for each analyzer
shall be powered and operational during inspections and tests.
4.3.1.8 All analyzer enclosure or shelter utility and alarm systems shall be
powered, fully operational, and demonstrated.
4.3.1.9 The tasks outlined in Sections 4.3.2 through 4.3.6 shall be completed
during this stage of the testing and inspection.
4.3.2 Shelter
4.3.2.1 Review all required certificates of analyzer OEM to ensure
compliance with specifications, e.g., welding certifications,
electrical area classification compliance, Professional Engineer (PE)
certification of base support structure.
4.3.2.2 Visually inspect and verify conformance to shelter dimensional and
mounting specifications.
4.3.2.3 Visually inspect and verify conformance to specified shelter
materials of construction and fabrication requirements.
4.3.2.4 Visually inspect and verify conformance to specified/approved
sample system enclosure type, materials of construction, location,
and mounting.
4.3.2.5 Visually inspect and verify conformance to specified electrical
components, piping and valves, and mounting hardware.
4.3.2.6 Visually inspect and verify conformance to specified electrical
grounding requirements.
4.3.2.7 Visually inspect and verify conformance of HVAC system to
specification, including issuance of a certificate of compliance to the
electrical area classification.
4.3.2.8 Visually inspect and verify conformance of HVAC to specified
dimensional and mounting specifications.
4.3.2.9 Visually inspect and verify size and location of all utility and
process connection points.

Page 6 of 9 Process Industry Practices


COMPLETE REVISION PIP PCTPA001
August 2006 Process Analyzer System Acceptance Testing

4.3.2.10 Visually inspect and verify shelter layout against specifications and
approved drawings.
4.3.2.11 Visually inspect and verify accessibility and maintainability of all
utility and analyzer systems and peripheral support hardware
components.
4.3.2.12 Visually inspect and verify presence of all enclosure utility and
safety alarm sensors and indicators.
4.3.2.13 Visually inspect and verify specification compliance for all “bolt on”
or field-mounted accessories, e.g., awnings, cylinder racks, and
sample recovery systems.
4.3.2.14 Visually inspect and verify shelter lift points against approved lifting
drawings.
4.3.3 Sample System
4.3.3.1 Visually inspect and verify sample system against approved flow
diagrams.
4.3.3.2 Visually inspect and verify accessibility, operability, and
maintainability of as-built sample system.
4.3.3.3 Visually inspect and verify sample system components against
approved manufacturer lists.
4.3.3.4 Visually inspect and verify sample-wetted materials of construction
against specifications, e.g., o-rings, diaphragms, floats, rotameter
tubes, and similar components.
4.3.3.5 Visually inspect and verify all sample system component tagging
and labeling.
4.3.3.6 Visually inspect and verify presence, size, and range of all sample
system and utility support indicators and control devices, e.g.,
pressure gauges, cabinet heater, dial thermometer, temperature
controller, cabinet purge flowmeter, heat exchangers, insulation, and
heat tracing.
4.3.3.7 Visually inspect and verify presence of all sample system safety
alarm and indicating systems.
4.3.3.8 Visually inspect and verify proper cabinet penetrations for all
electrical, utility, and sample line penetrations.
4.3.3.9 Visually inspect and verify sample probe assemblies for
conformance to specified requirements. Inspection should include
verification of proper sizing, materials of construction, tagging,
flange bolt patterns, welds, and weld certifications.
4.3.3.10 Visually inspect and verify proper labeling (externally and
internally) of all sample cabinet penetrations.
4.3.3.11 Verify total sample flow to analyzer house interior against stated
design parameters.

Process Industry Practices Page 7 of 9


PIP PCTPA001 COMPLETE REVISION
Process Analyzer System Acceptance Testing August 2006

4.3.4 Shelter Performance Testing


4.3.4.1 Verify proper operation of all electrical utility functions, e.g.,
interior and exterior lighting, HVAC, analyzer power, sample system
power, UPS power feeds, switches, and breakers.
4.3.4.2 Verify proper operation and calibration of all shelter alarm and
shutdown systems, e.g., oxygen deficiency, smoke detectors,
combustible gas detectors, toxic gas detectors, shelter
pressurization/flow sensors, visual and audible alarms, analog, and
digital outputs.
4.3.4.3 Functionally check and verify total airflow and velocity against
stated pressurization and air change requirements.
4.3.4.4 Verify total utility flows, e.g., N2, H2, to analyzer shelter interior.
4.3.5 Analyzer and Sample System Performance Testing
4.3.5.1 Pressure-test and leak-check all sample systems.
4.3.5.2 Functionally check the operation of all manual and automatic
stream-switching valves, calibration valves, automatic system
isolation valves, and valve position indicators.
4.3.5.3 Functionally check the operation and calibration of the sample
temperature controls, heating/cooling system controllers, and
indicators.
4.3.5.4 Functionally check the operation and calibration of all sample
system alarm and/or shutdown systems, e.g., toxic gas leak detectors,
and combustible gas detectors.
4.3.5.5 Verify sizing and calibration, and functionally check the operation
of all sample system flow indicators and controllers.
4.3.5.6 Verify sizing and calibration, and functionally check the operation of
all sample pressure regulators, indicators, and pressure relief valves.
4.3.5.7 Check and verify all terminal connections for stated analog/digital
I/O interconnections to owner data highway, host computer, and
control room interface.
4.3.6 FAT Test Documentation
4.3.6.1 Review and verify that all required documentation is complete and
in acceptable format.
4.3.6.2 Obtain signoff by owner, or by owner-authorized agent, of
inspection discrepancies (punch list). The punch list shall define
items for correction, acknowledged exceptions, or deficiencies. The
signoff shall include timing for satisfactory resolution of all items by
responsible organization.
4.3.6.3 Re-inspect as required to ensure compliance with all deficiencies
noted on the punch list.

Page 8 of 9 Process Industry Practices


COMPLETE REVISION PIP PCTPA001
August 2006 Process Analyzer System Acceptance Testing

4.4 Site Acceptance Tests (SAT)


4.4.1 General
4.4.1.1 The SAT demonstrates analyzer system performance following a
defined period of uninterrupted, on-line operation and shall be in
accordance with the performance test requirements.
4.4.1.2 SATs, including the documentation requirements and standards
compliance, shall be fully defined at the bidding stage of an analyzer
project.
Comment: See Section 4.6 of PIP PCEPA002.
4.4.1.3 The tasks outlined in Section 4.4.2 shall be completed during this
stage of the testing and inspection
4.4.2 Performance Tests
4.4.2.1 Check and verify proper installation of sample probes, sample lines,
calibration gas tubing runs, and all utility and vent headers.
4.4.2.2 Check and verify operation of heat-traced sample lines and
controller operation.
4.4.2.3 Verify total system (analyzer and sample system) response time with
introduction of known zero and span calibration standards.
4.4.2.4 Verify sample system flow, temperature, and pressure operation
against stated design parameters.
4.4.2.5 Verify calibrated analyzer on-stream analytical response against
plant lab or grab sample analysis.
4.4.2.6 Verify analog/digital I/O to owner data highway, host computer, and
control room interface.
4.4.2.7 Verify operation and performance of each analytical system against
specified turnover criteria, e.g., 5 days continuous operation.
4.4.2.8 Verify performance of all shelter and sample system alarm
functions.

Process Industry Practices Page 9 of 9


COMPLETE REVISION
August 2006

Process Industry Practices


Process Control

PIP PCEPA003
Process Analyzer System
Field Installation Guideline
PURPOSE AND USE OF PROCESS INDUSTRY PRACTICES

In an effort to minimize the cost of process industry facilities, this Practice has
been prepared from the technical requirements in the existing standards of major
industrial users, contractors, or standards organizations. By harmonizing these
technical requirements into a single set of Practices, administrative, application, and
engineering costs to both the purchaser and the manufacturer should be reduced. While
this Practice is expected to incorporate the majority of requirements of most users,
individual applications may involve requirements that will be appended to and take
precedence over this Practice. Determinations concerning fitness for purpose and
particular matters or application of the Practice to particular project or engineering
situations should not be made solely on information contained in these materials. The
use of trade names from time to time should not be viewed as an expression of
preference but rather recognized as normal usage in the trade. Other brands having the
same specifications are equally correct and may be substituted for those named. All
Practices or guidelines are intended to be consistent with applicable laws and
regulations including OSHA requirements. To the extent these Practices or guidelines
should conflict with OSHA or other applicable laws or regulations, such laws or
regulations must be followed. Consult an appropriate professional before applying or
acting on any material contained in or suggested by the Practice.

This Practice is subject to revision at any time.

© Process Industry Practices (PIP), Construction Industry Institute, The


University of Texas at Austin, 3925 West Braker Lane (R4500), Austin,
Texas 78759. PIP member companies and subscribers may copy this Practice
for their internal use. Changes, overlays, addenda, or modifications of any
kind are not permitted within any PIP Practice without the express written
authorization of PIP.

PRINTING HISTORY
August 2000 Issued as PCIPA001
August 2006 Complete Revision

Not printed with State funds


COMPLETE REVISION
August 2006

Process Industry Practices


Process Control

PIP PCEPA003
Process Analyzer System
Field Installation Guideline
Table of Contents

1. Introduction................................. 2
1.1 Purpose............................................ 2
1.2 Scope ............................................... 2

2. References .................................. 2
2.1 Process Industry Practices............... 2
2.2 Industry Codes and Standards......... 3

3. Definitions ................................... 3

4. Pre-Installation............................ 3
4.1 General ............................................ 3
4.2 Receiving ......................................... 3
4.3 Civil/Structural .................................. 4

5. Field Installation ......................... 4


5.1 Analyzer Shelter ............................... 4
5.2 Field Hardware................................. 4
5.3 Utility Piping...................................... 4
5.4 Sample Tubing ................................. 5
5.5 Electric Heat-Traced and Pre-
Insulated Tubing............................... 6
5.6 Steam-Traced Tubing Bundles ........ 7
5.7 Sample Probe .................................. 8
5.8 Electrical Equipment ........................ 8

Process Industry Practices Page 1 of 8


PIP PCEPA003 COMPLETE REVISION
Process Analyzer Field Installation Guideline August 2006

1. Introduction

1.1 Purpose
This Practice provides guidelines to individuals responsible for the field installation
of process analyzer systems.

1.2 Scope
This Practice describes guidelines for field installation of process analyzer systems.

2. References
Applicable parts of the following Practices and industry codes and standards shall be
considered an integral part of this Practice. The edition in effect on the date of contract
award shall be used, except as otherwise noted. Short titles will be used herein where
appropriate.

Comment: Although some of the references are not cited in the narrative of this Practice, all
of the references are listed because they can be helpful to the installer of process
analyzer systems.

2.1 Process Industry Practices (PIP)


– PIP CVC01016 - Plant Site and Project Data Sheet
– PIP PCCEL001 - Instrument Electrical Requirements
– PIP PCCIA001 - Instrument Air Systems Criteria
– PIP PCCIP001 - Instrument Piping and Tubing Criteria
– PIP PCCPA001 - Process Analyzer System Design Criteria
– PIP PCEPA001 - Process Analyzer System Engineering Guidelines
– PIP PCEPA002 - Process Analyzer Project Implementation Guidelines
– PIP PCCGN002 - General Instrument Installation Criteria
– PIP PCIEL000 - Instrumentation Electrical Installation Details
– PIP PCSEL003 - Instrument Junction Box Specifications
– PIP PCSPA001 - Process Analyzer Project Documentation Data Sheet
Instructions
– PIP PCSPA01D - Process Analyzer Project Documentation Data Sheet
– PIP PCSPA002 - Process Analyzer System Data Sheet Instructions
– PIP PCSPA02D - Process Analyzer System Data Sheet
– PIP PCSPA003 - Process Analyzer Shelter Data Sheet Instructions
– PIP PCSPA03D - Process Analyzer Shelter Data Sheet
– PIP PCSPA004 - Process Analyzer System Proposal Data Sheet Instructions
– PIP PCSPA04D - Process Analyzer System Proposal Data Sheet

Page 2 of 8 Process Industry Practices


COMPLETE REVISION PIP PCEPA003
August 2006 Process Analyzer System Field Installation

– PIP PCTPA001 - Process Analyzer System Acceptance Testing


– PIP STC01015 - Structural Design Criteria

2.2 Industry Codes and Standards

• National Fire Protection Association (NFPA)


– NFPA 70 - National Electrical Code (NEC)

3. Definitions
owner: The party who owns the facility wherein the process analyzer system will be installed

purchaser: The party who awards the contract to the supplier. The purchaser may be the
owner or the owner’s authorized agent.

supplier: The party responsible for installing the process analyzer system.

4. Pre-Installation

4.1 General
4.1.1 Before installing the analyzer system equipment in the field, a pre-
installation meeting should be held between the owner, purchaser, and
supplier to confirm the requirements of this Practice and all associated
analyzer system installation drawings.
4.1.2 If required to assist with start-up, calibration, and/or initial operation,
analyzer original equipment manufacturer (OEM) service representatives
and/or analyzer system vendor personnel should be scheduled. Analyzer
OEM’s assistance may also be required for warranty validation.
4.1.3 Installation of all analyzer equipment should be performed by trained,
experienced workers.

4.2 Receiving
4.2.1 Personnel should be assigned to coordinate the arrival of equipment on site.
Coordination instructions should include time, location, and date of
scheduled delivery; safety requirements for driver of the delivery truck;
unloading plan; permits; ancillary equipment, etc.
4.2.2 Personnel should be assigned to verify that all equipment required for
unloading and installation is present at the site.
4.2.3 Personnel should be assigned to make provisions for process analyzer
systems that require immediate purging and/or power for climate control.
The provisions and associated field requirements should be communicated to
field construction personnel.

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PIP PCEPA003 COMPLETE REVISION
Process Analyzer Field Installation Guideline August 2006

4.3 Civil/Structural
4.3.1 The analyzer system location should be verified to be in accordance with
area space, elevation, and orientation requirements.
4.3.2 The foundation or platform preparation should be verified to be in
accordance with purchaser’s specifications.
4.3.3 The cylinder rack installation preparation (e.g., ramp access for wheeled
cylinder carts, paving, and elevation of cylinder connections) should be
verified to be in accordance with purchaser’s specifications.

5. Field Installation

5.1 Analyzer Shelter


5.1.1 Field-mounted analyzer enclosure or shelter should be leveled and secured to
support foundation.
5.1.2 Base support structure should be sealed to foundation with appropriate
sealing compound.
5.1.3 For installation of a shelter without a floor, the shelter sealing gasket should
be checked to ensure proper installation.
5.1.4 Ancillary shelter equipment such as awnings/rain shields, detached cylinder
racks, fresh air intake, sample recovery systems, etc., should be installed.
5.1.5 The heating, ventilation, and air conditioning (HVAC) condensate drain line
should be connected to the condensate drain header or sewer. Draining
condensate freely on a concrete pad should not be permitted.

5.2 Field Hardware


5.2.1 Plate- or cabinet-mounted equipment locations should permit maintenance
access.
5.2.2 All components used should be in accordance with purchaser’s
specifications.
5.2.3 Clamps and brackets should be galvanized or stainless steel.
5.2.4 Tubing supports should be provided and installed with fittings, spacers,
clamps, guides, and other accessories as required.
5.2.5 All sample-wetted materials should meet or exceed the materials of
construction described in the purchaser’s piping specifications.

5.3 Utility Piping


5.3.1 Utility piping should be in accordance with the purchaser’s piping
specification.
5.3.2 Utility piping should include local isolation valves, drain valves, and check
valves, as specified.

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COMPLETE REVISION PIP PCEPA003
August 2006 Process Analyzer System Field Installation

5.3.3 Piping to drains should be routed under the slab or in such manner that the
piping is not a tripping hazard and does not limit access around the analyzer
shelter.
5.3.4 The utility piping specification break should be at the connecting flange to
the analyzer shelter.
5.3.5 If steam is required for heating remote analyzer equipment, each user should
have an individual supply with an isolation valve and trap.
5.3.6 Threaded piping connections should be sealed with PTFE sealing tape or
equivalent tape-type sealer.
5.3.7 Piping should be leak-checked according to project/location procedure and
analyzer specification. The piping should be repaired, flushed, and dried as
required.
5.3.8 Utility piping should be cleaned and degreased before final connection to the
utility headers of the analyzer system.

5.4 Sample Tubing


5.4.1 Sample tubing should be in accordance with analyzer data sheet
(PIP PCSPA02-D), purchaser’s specification, size, and material.
5.4.2 Only pre-cleaned tubing should be used for sample-wetted surfaces. Specific
applications may require post-installation cleaning.
5.4.3 Field-tubing runs should be grouped to benefit from use of common support
members and to present a finished installation that is routed in a neat and
orderly manner.
5.4.3 Tubing spacing should be adequate and uniform. Tubes should not be
permitted to cross over one another.
5.4.5 Only industry-standard tools should be used for bending to avoid flat spots
and kinks. Bent tubing should be de-burred to the original internal diameter
and blown free of particles.
5.4.6 Tubing supports should be installed in accordance with specification, tube
material, and service. Tubing trays or perforated angle supports should be
used as needed.
5.4.7 High-quality two-ferrule tube fittings should be used for gas cylinders and
for all sample-wetted lines.
5.4.8 Continuous tubing runs should be used wherever possible to minimize the
number of tubing unions.
5.4.9 If run in trays, tubing should be equally spaced on the same plane leaving a ¼-
inch air gap. If tubing unions are used, the unions should be installed in a
raised and staggered fashion away from the plane, using short 45° bends for
ease of assembly and disassembly. If possible, tubing unions should be visible.
5.4.10 All installed tubing should be pressure-tested and leak-checked.

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PIP PCEPA003 COMPLETE REVISION
Process Analyzer Field Installation Guideline August 2006

5.4.11 Pressure sensitive instrumentation should be isolated before pressure testing.


5.4.12 If a vapor sample can contain liquids or condensables, the sample line should
be sloped. The sample line may slope in two directions (toward the sample
tap and toward the analyzer), but both slopes should be continuous from the
high point. Traps in the sample line should not be permitted.

5.5 Electric Heat-Traced and Pre-Insulated Tubing


5.5.1 Manufacturer’s instructions should be used for proper installation of
electrically heated and/or pre-insulated sample lines and bundles, including
the following:
a. Minimum bending radius
b. Spacing between bundles
c. Maximum spacing of supports
d. Use of terminator kits
e. Connections to electrical supply
f. Penetrations through enclosures, e.g., safety precautions
5.5.2 Both ends of heat-traced sample tubing should be sealed with the
manufacturer’s recommended kits to prevent moisture damage.
5.5.3 The circuit for electrically heat-traced tubing should include equipment for
ground fault protection in accordance with NFPA 70.
5.5.4 Heat-traced and pre-insulated tubing should be installed in accordance with
the purchaser’s specifications.
5.5.5 Tubing trays or perforated angle supports should be used as needed.
5.5.6 Sample lines should be properly secured. To prevent the creation of hot
spots, care should be taken to ensure that the sample line securing devices do
not deform the tube bundle.
5.5.7 Manufacturer’s instructions should be checked before shortening electrically
heated self-regulating sample line.
5.5.8 Heat-treated and pre-insulated tubing should be run directly to the device it
serves.
5.5.9 Bulkhead tubing unions should not be permitted for cabinet or enclosure
penetrations.
5.5.10 Bundle(s) should penetrate the walls of the enclosure using heat-shrink entry
seals to ensure that the sample temperature is uniformly maintained.
5.5.11 Tubing connections for electrically traced tubing should be installed inside
the enclosure.
5.5.12 The power source for traced tubing should be provided at either of the
following locations:

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COMPLETE REVISION PIP PCEPA003
August 2006 Process Analyzer System Field Installation

a. Analyzer enclosure
b. Dedicated heat-tracing panel
5.5.13 Traced sample lines that have exposed surface temperatures exceeding plant
safety standards should, for personnel protection, be shielded or routed away
from normal reach.
5.5.14 Electrically traced tubing bundles should be checked for proper resistance or
continuity before being powered.

5.6 Steam-Traced Tubing Bundles


5.6.1 Manufacturer’s instructions should be used for proper installation of steam-
heated sample lines and bundles, including the following:
a. Minimum bending radius
b. Spacing between bundles
c. Maximum spacing of supports
d. Use of terminator kits
e. Penetrations through enclosures
f. Safety precautions
5.6.2 If steam is used for heat tracing, the sample line should be sloped.
5.6.3 Unions and splices in the steam lines should be minimized.
5.6.4 Steam traps should be located and steam lines should be insulated in
accordance with manufacturer’s recommendations.
5.6.5 Steam-traced tubing should be installed in accordance with the purchaser’s
specifications.
5.6.6 Tubing trays or perforated angle supports should be used as needed.
5.6.7 Sample lines should be properly secured. To prevent the creation of hot
spots, care should be taken to ensure that the sample line securing devices do
not deform the tube bundle.
5.6.8 Steam-traced tubing should be installed directly to the device it serves.
5.6.9 Bulkhead tubing unions should not be permitted for cabinet or enclosure
penetrations.
5.6.10 Bundle(s) should penetrate the walls of the enclosure using heat-shrink entry
seals to ensure that the sample temperature is uniformly maintained.
5.6.11 The steam source should be provided at either of the following locations:
a. Analyzer enclosure
b. Other appropriate source

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PIP PCEPA003 COMPLETE REVISION
Process Analyzer Field Installation Guideline August 2006

5.6.12 Traced sample lines that have the exposed surface temperatures exceeding
specified safety standards should, for personnel protection, be shielded or
routed away from normal reach.
5.6.13 Each steam line should have a dedicated trap located in accordance with
manufacturer’s recommendation. The traps should not be insulated and
should be installed at the lowest convenient point.
5.6.14 Seal kits should be installed on each end of steam-traced sample lines to
prevent corrosion.

5.7 Sample Probe


5.7.1 Flanged sample probes used to extract the sample from the process line
should be installed before hydraulic testing of the lines.
5.7.2 Proper isolations of the analyzer system should be verified.
5.7.3 Retractable insertion probes should be retracted before leak testing.
5.7.4 In-situ analyzer-sensing elements such as pH, conductivity, chlorine,
viscosity, etc., should be installed only after leak testing.
5.7.5 Orientation of the sample probe or sensor installation should be verified.
5.7.6 Sample-conditioning equipment at the sample tap should be close-coupled to
the tap and mounted and installed in accordance with purchaser’s drawings.

5.8 Electrical Equipment


5.8.1 Electrical components should have a nationally recognized testing laboratory
approval.
5.8.2 Conduit, metal-clad, or tray cable wiring can be used.
5.8.3 AC and DC wiring sizes and color codes should be in accordance with
purchaser’s requirements.
5.8.4 Field wiring and connections should be loop-checked for continuity and
conformance to purchaser’s drawings.
5.8.5 Junction box or electrical cabinet penetrations should be through the sides or
bottom only.
5.8.6 If conduit wiring is used, covers on conduit fittings should be checked to
ensure that they are properly secured. After all inspections are complete,
conduit seals should be poured and marked.
5.8.7 Conduit drains should be used at each low point.
5.8.8 The shelter and all electrical equipment should be grounded.

Page 8 of 8 Process Industry Practices


COMPLETE REVISION
August 2006

Process Industry Practices


Process Control

PIP PCEPA002
Process Analyzer Project
Implementation Guidelines
PURPOSE AND USE OF PROCESS INDUSTRY PRACTICES

In an effort to minimize the cost of process industry facilities, this Practice has
been prepared from the technical requirements in the existing standards of major
industrial users, contractors, or standards organizations. By harmonizing these
technical requirements into a single set of Practices, administrative, application, and
engineering costs to both the purchaser and the manufacturer should be reduced. While
this Practice is expected to incorporate the majority of requirements of most users,
individual applications may involve requirements that will be appended to and take
precedence over this Practice. Determinations concerning fitness for purpose and
particular matters or application of the Practice to particular project or engineering
situations should not be made solely on information contained in these materials. The
use of trade names from time to time should not be viewed as an expression of
preference but rather recognized as normal usage in the trade. Other brands having the
same specifications are equally correct and may be substituted for those named. All
Practices or guidelines are intended to be consistent with applicable laws and
regulations including OSHA requirements. To the extent these Practices or guidelines
should conflict with OSHA or other applicable laws or regulations, such laws or
regulations must be followed. Consult an appropriate professional before applying or
acting on any material contained in or suggested by the Practice.

This Practice is subject to revision at any time.

© Process Industry Practices (PIP), Construction Industry Institute, The


University of Texas at Austin, 3925 West Braker Lane (R4500), Austin,
Texas 78759. PIP member companies and subscribers may copy this Practice
for their internal use. Changes, overlays, addenda, or modifications of any
kind are not permitted within any PIP Practice without the express written
authorization of PIP.

PRINTING HISTORY
August 2000 Issued
August 2006 Complete Revision

Not printed with State funds


COMPLETE REVISION
August 2006

Process Industry Practices


Process Control

PIP PCEPA002
Process Analyzer Project
Implementation Guidelines
Table of Contents

1. Introduction................................. 2
1.1 Purpose............................................ 2
1.2 Scope ............................................... 2

2. General References.................... 2
2.1 Process Industry Practices............... 2
2.2 Industry Codes and Standards......... 3
2.3 Information Resources..................... 3

3. General ........................................ 3

4. Tasks and Deliverables.............. 4


4.1 Conceptual Design........................... 4
4.2 Production Design............................ 5
4.3 Implementation ................................ 6
4.4 Detailed Design................................ 8
4.5 Installation ...................................... 11
4.6 Commissioning/Start-up/Turnover . 12
4.7 Project Completion......................... 12

5. Project Scheduling ................... 13

Process Industry Practices Page 1 of 13


PIP PCEPA002 COMPLETE REVISION
Process Analyzer Project Implementation Guidelines August 2006

1. Introduction

1.1 Purpose
This Practice provides guidelines for the design, specification, purchasing, and
installation of process analyzer systems for major capital projects.

1.2 Scope
This Practice describes the guidelines for implementation of process analyzer
systems. The successful implementation of a process analyzer project requires the
knowledge, integration, and management of multi-disciplinary engineering skills and
resources that may bridge several different organizations. The detailed information
on “Tasks and Deliverables” provided in this Practice assumes a typical project.
However, depending upon the scope of a given project and the organizational
structure defined for that project, the tasks defined under the Task s and Deliverables
for participating organizations may change. This Practice should be used to assist in
assessment and definition of roles and responsibilities for those tasks required for a
given project.

2. General References
Applicable parts of the following Practices, industry codes and standards, and references
shall be considered an integral part of this Practice. The edition in effect on the date of
contract award shall be used, except as otherwise noted. Short titles will be used herein
where appropriate.

2.1 Process Industry Practices (PIP)


– PIP PCCPA001 - Process Analyzer System Design Criteria
– PIP PCEPA001 - Process Analyzer System Engineering Guidelines
– PIP PCSPA001 - Process Analyzer Project Documentation Data Sheet
Instructions
– PIP PCSPA01D - Process Analyzer Project Documentation Data Sheet
– PIP PCSPA002 - Process Analyzer System Data Sheet Instructions
– PIP PCSPA02D - Process Analyzer System Data Sheet
– PIP PCSPA003 - Process Analyzer Shelter Data Sheet Instructions
– PIP PCSPA03D - Process Analyzer Shelter Data Sheet
– PIP PCSPA004 - Process Analyzer Bid Proposal Data Sheet Instructions
– PIP PCSPA04D - Process Analyzer Bid Proposal Data Sheet
– PIP PCIPA001 - Process Analyzer System Field Installation
– PIP PCTPA001 - Process Analyzer System Acceptance Testing

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COMPLETE REVISION PIP PCEPA002
August 2006 Process Analyzer Project Implementation Guidelines

2.2 Industry Codes and Standards

• National Fire Protection Association (NFPA)


– NFPA 30 - Flammable and Combustibles Liquids Code
– NFPA 70 - National Electrical Code - Latest Edition
– NFPA 496 - Standards for Purged and Pressurized Enclosures for Electrical
Equipment
– NFPA 497 - Recommended Practice for the Flammable Liquids, Gases, or
Vapors and of Hazardous (Classified) Locations for Electrical Installations in
Chemical Process Areas

2.3 Information Resources


– Clevett, K.J., Process Analyzer Technology, John Wiley & Sons, NY, NY.
– Cornish, D. C., Jepson, G., Smurthwaite, M.J., Sampling Systems for Process
Analyzers, Buttersworth, London, England.
– Houser, E.A., Principles of Sample Handling and Sample System Design for
Process Analysis, Instrument Society of America, Research Triangle Park, NC.
– Lipták, B.G., Instrumentation in the Processing Industries, Chilton Book Co.,
Radnor, PA.
– Sherman, R. E., Analytical Instrumentation Practices Guide for Measurement
and Control, Instrument Society of America, Research Triangle Park, NC.
– Sherman, R.E., Process Analyzer Sample-Conditioning System Technology,
Wiley Interscience, 2002, New York.

3. General
3.1 The implementation of process analyzers on a major capital project can require the
participation of only one or several of the following resource groups:
a. Owner Company personnel.
b. Engineering and Construction Electrical and Instruments (E&I) engineering
section (E&C) contractor
c. Analyzer Systems Vendor (ASV)
d. Analyzer Original Equipment Manufacturer (OEM)
3.2 How these different organizations interact to produce a successful analyzer project
can vary depending upon the expertise of each group and the stage of the project. A
typical capital project includes, but may not be limited to, the following stages:
a. Conceptual design
b. Production design
c. Implementation
d. Detail design
e. Installation

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PIP PCEPA002 COMPLETE REVISION
Process Analyzer Project Implementation Guidelines August 2006

f. Commissioning/startup/turnover
g. Project completion
3.3 Successful implementation of a project requires continuity of personnel throughout
the execution period of a project. In addition to minimizing the overall cost of the
project, all efforts should be taken to align resources and minimize duplication of
effort. A matrix can be prepared in a spreadsheet or word-processing format to show
the tasks required at each stage in the project, along with each party’s agreed role
(i.e., lead, approval, review, and information only).

4. Tasks and Deliverables


A brief explanation of the analyzer project activity associated with each of the project stages
is defined in this section. Specific analyzer-related tasks and deliverables for each design
stage are further detailed for each of the participating organizations.

4.1 Conceptual Design


4.1.1 The conceptual design phase, which may follow piloting activity, is used to
generate process flow diagrams (PFDs).
4.1.2 Piping and instrument drawings (P&IDs) may be started during this stage of
a project.
4.1.3 This activity normally includes the participation of the Owner Company
R&D and Engineering organizations.
4.1.4 If a production-scale pilot plant facility is included in this stage, the services
of an E&C contractor may also be required.
4.1.5 At this stage of a project, the definition of process analyzer needs is often
limited to a conceptual “like to have” or “must have.” However, including
process analyzer resources at this stage of process development and design is
critical. This may be the only opportunity to develop, test, and evaluate
process specific on-line analysis techniques for perceived analysis needs
before implementation.
4.1.6 Owner Company
4.1.6.1 Develop PFDs.
4.1.6.2 Define preliminary analysis requirements.
4.1.6.3 Develop methods for Owner Company proprietary analytical
technology.
4.1.6.4 Develop analysis systems design concepts.
4.1.6.5 Initiate preparation of PIP PCSPA02D utilizing PIP PCSPA002.
4.1.6.6 Specify acceptable analytical technologies and vendors.
4.1.6.7 Develop acceptable vendor lists for ASV, analyzer OEM, and
system components.
4.1.6.8 Develop preliminary of P&IDs (study drawings).

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COMPLETE REVISION PIP PCEPA002
August 2006 Process Analyzer Project Implementation Guidelines

4.1.6.9 Define project Tasks and Deliverables.

4.2 Production Design


4.2.1 During the production phase of a project, PFDs are further refined, the plant
layout or general arrangement is defined, and P&IDs are developed and
completed.
4.2.2 On-line process analyzer requirements, including sample tap locations,
process operating conditions, and specific analysis requirements, are defined
during this stage.
4.2.3 An E&C contractor typically completes the detailed design of a production
facility, in conjunction with designated representatives of Owner Company.
4.2.4 The tasks outlined in the following sections are completed during this stage
of the project. These tasks may not be presented in a timeline sequence
because the project participants often complete them in parallel.
4.2.5 Owner Company Tasks and Deliverables
4.2.5.1 Recommend sample point and sample return requirements.
4.2.5.2 Recommend sample line materials of construction, insulation, and
heating requirements.
4.2.5.3 Recommend acceptable materials of construction for process-
wetted sample-handling components.
4.2.5.4 Recommend analyzer calibration/validation method.
4.2.5.5 List available support utilities.
4.2.5.6 Recommend alarm and signal requirements.
4.2.5.7 Recommend analyzer system host computer interface.
4.2.5.8 Provide typical flow diagrams for sample system.
4.2.5.9 Provide laboratory sample station requirements.
4.2.5.10 Recommend shelter type:
a. Type I - field mounted.
b. Type II - freely ventilated.
c. Type III - climate controlled.
d. Type IV - controlled for area classification reduction.
4.2.5.11 Update PIP PCSPA02D utilizing PIP PCSPA002.
4.2.5.12 Produce PIP PCSPA03D utilizing PIP PCSPA003.
4.2.5.13 Recommend maintenance support peripherals (e.g., cylinder racks,
apron around shelter, walkways, maintenance data highways, etc.).
4.2.5.14 Prepare preliminary process analyzer budgetary cost estimate based
on data available and defined design requirements.

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PIP PCEPA002 COMPLETE REVISION
Process Analyzer Project Implementation Guidelines August 2006

4.2.6 E&C Contractor Tasks and Deliverables


4.2.6.1 Define electrical area classification for each analyzer location.
4.2.6.2 Incorporate maintenance support peripherals.
4.2.6.3 Locate sample point and sample return points on P&IDs.
4.2.6.4 Complete P&ID representation of alarm and signal requirements
between analyzers, sample systems, and host computer.
4.2.6.5 Complete drawing representation or written functional description of
host computer interface and control functions for any automated
sampling, calibration, flushing, inerting operations, and valve
sequencing.
4.2.6.6 Prepare flow diagrams for sample systems.
4.2.6.7 Locate and identify laboratory sample stations on P&IDs.
4.2.6.8 Update PIP PCSPA02D utilizing PIP PCSPA002.
4.2.6.9 Update PIP PCSPA03D utilizing PIP PCSPA003.
4.2.6.10 Locate process analyzer shelter(s) on plot plan or model.
4.2.6.11 Identify all relevant local and industry standards and certification
requirements.
4.2.7 ASV Tasks and Deliverables
Provide budgetary quotations.
4.2.8 Analyzer OEM Tasks and Deliverables
Provide budgetary quotations.

4.3 Implementation
4.3.1 The basic data for the process analysis requirements that are developed
during the conceptual and production design stages are used during
implementation to define sample transport, sample conditioning, and utility
support requirements for each analyzer system installation.
4.3.2 Depending upon the roles and responsibilities that have been defined for a
given project, the Owner Company and/or the E&C contractor typically
assumes the responsibility for developing the analyzer system installation
information.
4.3.3 The tasks outlined in the following sections are completed during this stage
of the project. These tasks may not be presented in a timeline sequence
because the project participants often complete them in parallel.
4.3.4 Owner CompanyTasks and Deliverables
4.3.4.1 Review ASV bid package, drawings, and specifications prepared by
E&C contractor.
4.3.4.2 Review and approve ASV bid package.

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August 2006 Process Analyzer Project Implementation Guidelines

4.3.5 Owner and/or E&C Contractor Tasks and Deliverables


4.3.5.1 Provide physical location information for all analyzer sample taps
and sample return points. Include physical orientation (vertical vs.
horizontal pipe run, nozzle orientation: top vs. side of pipe, etc.) and
accommodate maintenance accessibility.
4.3.5.2 Locate and orient all field-mounted analyzers, pre-conditioning
assemblies, analyzer enclosures, analyzer shelter, and cylinder racks
to assure maintenance accessibility and tie-in to field piping and
utility support.
4.3.5.3 Define interconnection requirements for power, analog/digital, and
fiber optic signals for host computer and process field wiring.
4.3.5.4 Complete PIP PCSPA02D.
4.3.5.5 Complete PIP PCSPA03D utilizing PIP PCSPA003.
4.3.5.6 Compile all applicable standards, codes, or approved supplier lists
that will impact the design, fabrication, and installation of the
analyzer systems, including those listed in the References.
4.3.5.7 Prepare Overview Document to describe the project scope.
4.3.5.8 Prepare and complete PIP PCSPA01D.
4.3.5.9 Define ASV and analyzer OEM installation, start-up, and
commissioning requirements.
4.3.5.10 Prepare bid specification for analyzer system project.
4.3.5.11 Prepare lower sections of PIP PCSPA04D utilizing PIP PCSPA004.
4.3.5.12 Participate together in ASV bid evaluation.
4.3.5.13 Place order to ASV for process analyzer project.
4.3.6 E&C Contractor and/or ASV Tasks and Deliverables
4.3.6.1 Design functional details for sample-handling system:
a. Single vs. multi-point
b. Differential pressure vs. pumped vs. aspirated sample transport
c. Fast loop and analyzer flow requirements.
d. Auto vs. manual stream switching
e. Auto vs. manual calibration and validation
4.3.6.2 Design fabrication details for sample-handling system:
a. Layout
b. Mounting and installation considerations
4.3.6.3 Complete and submit bid proposal for process analyzer package in
accordance with PIP PCSPA04D.

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PIP PCEPA002 COMPLETE REVISION
Process Analyzer Project Implementation Guidelines August 2006

4.3.7 Analyzer OEM(s) Tasks and Deliverables


Complete applications assessment or development for unique analysis
requirements.

4.4 Detailed Design


4.4.1 The data developed during conceptual design, production design, and
implementation stages of the project are transmitted to an ASV and/or an
analyzer OEM for development and production of design documentation for
each analyzer system and installation design details.
4.4.2 Following approvals by both the owner and E&C contractor, the systems are
released for fabrication.
4.4.3 Upon completion of fabrication, the systems are inspected and subjected to
acceptance tests by owner and E&C contractor.
4.4.4 The tasks outlined in the following sections are completed during this stage
of the project. These tasks may not be presented in a timeline sequence
because the project participants often complete them in parallel.
4.4.5 Owner and/or E&C Contractor Tasks and Deliverables
4.4.5.1 Purchase analytical instruments and/or obtain proprietary in-house
instruments. Instruments may be drop-shipped to ASV or others for
modifications as required to meet installation electrical area
classification, all local electrical codes, and sample system
integration.
4.4.5.2 Conduct analyzer systems safety review before final approval for
fabrication.
4.4.5.3 In conjunction with ASV, design and provide foundation and
structural supports required for analyzer shelters, HVAC cylinder
racks, utilities support, etc.
4.4.5.4 Participate in Analyzer OEM acceptance tests of process analyzers.
4.4.5.5 Approve all documentation including:
a. Specifications
b. Drawings
c. Acceptance test procedures
d. Inspections
4.4.5.6 Participate in Factory Acceptance Tests (FAT) of fabricated
analyzer systems.
4.4.5.7 Define maintenance and support training requirements.
4.4.5.8 Use Document Control for tracking all manuals, drawings, etc., for
the analyzer project.

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COMPLETE REVISION PIP PCEPA002
August 2006 Process Analyzer Project Implementation Guidelines

4.4.5.9 Supply ASV with a block of instrument loop numbers for identifying
instruments on analyzer system P&IDs and other drawings as
required.
4.4.5.10 Review and approve all specifications, drawings, and documents that
require interfaces/interconnections to process equipment or services
as required to ensure that systems supplied by Owner Company or
ASV will meet all site design and installation criteria.
4.4.5.11 Design and provide to the ASV all sample and sample return line
routings and lengths.
4.4.5.12 For Type III and Type IV shelters, design and provide to the ASV
the routing, distance, and support needs for the fresh air intake stack.
4.4.5.13 Design signal and alarm cabling and routings.
4.4.5.14 Design and provide utility support requirements as defined by
Owner Company and/or the ASV.
4.4.5.15 Complete PIP PCSPA01D utilizing PIP PCSPA001.
4.4.5.16 Owner shall supply certificates of manufacture written in the
destination language and authenticated by the local embassy,
consulate, or commercial attachés for countries outside the European
Community. The owner should be responsible for U.S.-purchased
equipment.
4.4.6 ASV Tasks and Deliverables
4.4.6.1 Analyzer Shelter
1. Design, purchase, and fabricate analyzer shelter(s) including
a. HVAC
b. Orientation
c. Utility connections
d. Location
e. Layout
f. Sizing
g. Mounting and orientation of analyzers
h. Sample probes
i. Sample systems
j. Pre-conditioning assemblies
k. Other supplied accessories in accordance with bid
specification, installation criteria, electrical area classification,
and any other related project requirements.
2. Prepare written specifications for all major equipment and
system components that are not being purchased by owner
and/or E&C contractor (e.g., HVAC system).

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PIP PCEPA002 COMPLETE REVISION
Process Analyzer Project Implementation Guidelines August 2006

3. Provide shelter pressurization and airflow calculations required


to purge for toxic gas, combustible gas, or asphyxiant gas leaks
into the interior of the shelter.
4. Design sample return interface including sample recovery
systems, vents, drains, process headers, etc.
5. Design for all utility requirements including load and
consumption calculations.
6. Design for all cabling requirements.
7. Provide required certifications.
8. Prepare and provide detailed documentation for the installation
by the E&C contractor for all analyzer systems shelters and
ancillary equipment.
9. If required, provide preliminary drawings for outline and
mounting dimensions and interconnections.
4.4.6.2 Analyzer Systems
1. Design and provide calculations for sample line size in
accordance with sample loop residence and analyzer response
time requirements.
2. Ensure that sample system design includes the following:
a. Calibration and validation systems with standards as defined
on the data sheets.
b. Temperature, pressure, flow indication, and control.
c. Suitable materials of construction to meet process tap and
return conditions.
3. Prepare and issue all drawings in accordance with
PIP PCSPA01D utilizing PIP PCSPA001.
4. Purchase all analyzers not included in owner alliance
agreements and associated hardware required to fabricate and
mount all analyzer sample system enclosures, shelters, and
racks.
5. Fabricate all process analyzers systems, shelters, and racks.
6. Provide all material, test equipment, and personnel to conduct
the Factory Acceptance Tests, including calibration gases and
standard generators.
7. Host and conduct Factory Acceptance Tests for all process
analyzers and associated hardware purchased by the ASV.
Provide preliminary system test results to owner and E&C
contractor.
8. Provide a list of start-up and commissioning spares and a list of
spare parts for 2-year operation.

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COMPLETE REVISION PIP PCEPA002
August 2006 Process Analyzer Project Implementation Guidelines

9. Identify any consumable or limited shelf-life items that may


require special shipping requirements (e.g., pH electrodes).
4.4.7 Analyzer OEM Tasks and Deliverables
4.4.7.1 Provide the process analyzers as defined by the owner and E&C
contractor or the ASV in accordance with PIP PCSPA02D.
4.4.7.2 Provide all information, documentation, software, and ancillary
equipment as required for a fully operational and functional
analyzer.
4.4.7.3 Provide dimensional outline, electrical, and utility interconnection
diagrams.
4.4.7.4 Provide all material and personnel to conduct the Analyzer OEM
acceptance test.

4.5 Installation
4.5.1 The E&C contractor or a contractor designated by the owner normally
handles the field installation of the analyzer systems.
4.5.2 The tasks outlined in the following sections are to be completed during this
stage of the project. These tasks may not be presented in a timeline sequence
because the project participants often complete them in parallel.
4.5.3 Owner and/or E&C Contractor Tasks and Deliverables
4.5.3.1 Complete site preparation
4.5.3.2 Install concrete foundations
4.5.3.3 Set major equipment
4.5.3.4 Install analyzer systems, including sample lines
4.5.3.5 In accordance with ASV installation detail drawings, purchase
required materials for mounting and installing analyzer shelters and
all field-mounted hardware, including sample lines and sample line
heat trace termination kits.
4.5.3.6 Connect all interface points (e.g., piping, utilities, electrical, and
instrumentation).
4.5.4 ASV Tasks and Deliverables
4.5.4.1 May provide on-site supervision for off-loading and site installation
of all analyzers, shelters, or systems, including HVAC ductwork,
sample probes, sample lines, and calibration systems in their supply.
This may also include providing supervision for termination of field
power, signal cabling, connection of all utilities, and mounting of all
systems and ancillary equipment.
4.5.4.2 Prepare data books and training program for the operation,
calibration, start-up, shutdown, maintenance, troubleshooting, and
analyzer system diagnostics of the process analyzer systems,

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PIP PCEPA002 COMPLETE REVISION
Process Analyzer Project Implementation Guidelines August 2006

shelters, alarms, and safety systems. Provide copies of the data


books as specified.

4.6 Commissioning/Start-up/Turnover
4.6.1 Commissioning is the demonstrated operation of the analyzer systems and all
associated hardware and software.
4.6.2 Start-up is the demonstrated operation of the analyzer systems with actual
process samples.
4.6.3 After successful commissioning, start-up, and a defined period of
uninterrupted on-line operation, turnover (or transfer of ownership) of the
systems to the owner is completed.
4.6.4 Commissioning, start-up, and turnover typically involves resources from the
owner, the E&C contractor, the ASV, and/or the Analyzer OEM.
4.6.5 The tasks outlined in the following sections are completed during this stage
of the project. These tasks may not be presented in a timeline sequence
because the project participants often complete them in parallel.
4.6.6 Owner and/or E&C Contractor Tasks and Deliverables
4.6.6.1 Participate in site start-up and commissioning of all analyzers and
ancillary equipment.
4.6.6.2 If specified, issue requisition to ASV and Analyzer OEM to perform
on-site start-up, commissioning, and training.
4.6.7 ASV Tasks and Deliverables
4.6.7.1 Provide on-site test procedures and test documentation requirements.
4.6.7.2 Provide start-up and commissioning requirements that refer to all
ASV provided equipment analyzers, analyzer shelter, ancillary
equipment, etc.
4.6.7.3 Provide start-up system with process samples.
4.6.7.4 Provide on-site training program for owner personnel on operation
and maintenance of the equipment. ASV should complete training
program documentation before site installation and complete
training classes on site before commissioning. Proposal should
include per diem rate (time, travel, and expenses) and numbers of
days required for training.
4.6.8 Analyzer OEM Tasks and Deliverables
Provide on-site start-up assistance and training as required.

4.7 Project Completion


4.7.1 The installation, commissioning, and start-up of an analyzer system may
require field modifications or changes that can require updates to the project
design drawings and documentation. Updating these documents to reflect the
“as-built” condition of the installed systems is essential for maintenance and
support of these systems.

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COMPLETE REVISION PIP PCEPA002
August 2006 Process Analyzer Project Implementation Guidelines

4.7.2 The E&C contractor, ASV, and/or the Analyzer OEM are typically involved
in ensuring the accuracy of the “as-builts.”

5. Project Scheduling
Table 1 provides notional parameters for consideration in establishing a schedule for an
analyzer systems project.

Table 1 – Analyzer Project Scheduling Elements


Notional Time to Completion:
Conceptual Design 1–5 years.
Production Design 1–2 years.
Implementation 3–6 months.

Analyzer pre-bid meeting(s) Maximum 30 days before bid due date


Issue request for bid Minimum 10 working days before bid due date
Purchase order (PO) placement Minimum 10 working days after receipt of bids
Owner, E&C contractor, and ASV kick- Maximum 10 working days after order
off meeting placement

Detail Design

Preliminary drawing submittals Maximum 30 working days after order


placement
First pass approval drawings Maximum 60 days after order placement
Process analyzer system safety review Minimum 10 working days after receipt of
approval drawings
Final approval drawing submittal Minimum 10 working days after completion of
safety review
Release for fabrication Upon final approval drawing sign-off
Analyzer OEM inspections As bid
ASV Factory Acceptance Tests As bid
Release for shipment After completion of Factory Acceptance Tests
and punch list corrections
Spare parts list 6 weeks before receipt of systems
Final data books Maximum 10 workings days after receipt of
systems

Installation
Field installation – completion date 1–3 months after receipt on site
Commissioning/Start-up/Turnover

On-site commissioning and training Upon installation completion


Plant start-up 3-6 months after receipt on-site
Turnover After plant start-up or 3–6 months after
receipt on-site

Process Industry Practices Page 13 of 13


COMPLETE REVISION
August 2006

Process Industry Practices


Process Control

PIP PCEPA001
Process Analyzer System Engineering Guidelines
PURPOSE AND USE OF PROCESS INDUSTRY PRACTICES

In an effort to minimize the cost of process industry facilities, this Practice has
been prepared from the technical requirements in the existing standards of major
industrial users, contractors, or standards organizations. By harmonizing these
technical requirements into a single set of Practices, administrative, application, and
engineering costs to both the purchaser and the manufacturer should be reduced. While
this Practice is expected to incorporate the majority of requirements of most users,
individual applications may involve requirements that will be appended to and take
precedence over this Practice. Determinations concerning fitness for purpose and
particular matters or application of the Practice to particular project or engineering
situations should not be made solely on information contained in these materials. The
use of trade names from time to time should not be viewed as an expression of
preference but rather recognized as normal usage in the trade. Other brands having the
same specifications are equally correct and may be substituted for those named. All
Practices or guidelines are intended to be consistent with applicable laws and
regulations including OSHA requirements. To the extent these Practices or guidelines
should conflict with OSHA or other applicable laws or regulations, such laws or
regulations must be followed. Consult an appropriate professional before applying or
acting on any material contained in or suggested by the Practice.

This Practice is subject to revision at any time.

© Process Industry Practices (PIP), Construction Industry Institute, The


University of Texas at Austin, 3925 West Braker Lane (R4500), Austin,
Texas 78759. PIP member companies and subscribers may copy this Practice
for their internal use. Changes, overlays, addenda, or modifications of any
kind are not permitted within any PIP Practice without the express written
authorization of PIP.

PRINTING HISTORY
August 2000 Issued
August 2006 Complete Revision

Not printed with State funds


COMPLETE REVISION
August 2006

Process Industry Practices


Process Control

PIP PCEPA001
Process Analyzer System Engineering Guidelines
Table of Contents

1. Introduction................................. 2
1.1 Purpose............................................ 2
1.2 Scope ............................................... 2

2. References .................................. 2

3. Guidelines ................................... 2
.

Process Industry Practices Page 1 of 3


PIP PCEPA001 COMPLETE REVISION
Process Analyzer System Engineering Guidelines August 2006

1. Introduction

1.1 Purpose
This Practice supplements the International Electrotechnical Commission (IEC) Technical
Report TR 61831, On-Line Analyzer Systems – Guide to Design and Installation. Together
this Practice and IEC TR61831 provide guidelines for the design and installation of process
analyzer systems.

1.2 Scope
This Practice describes additions, changes, and deletions that have been made to
IEC TR61831.

2. References
Applicable parts of the following Practices, industry codes and standards, and references
shall be considered an integral part of this Practice. The edition in effect on the date of the
contract award shall be used, except as otherwise noted. Short titles will be used herein
where appropriate.

- PIP PCTPA001 - Process Analyzer System Acceptance Testing

- NFPA 70 - National Electrical Code (NEC) 2005 Edition - Chapter 5, Special


Occupancies

- IEC TR61831 - On-Line Analyser Systems – Guide to Design and Installation

3. Guidelines
The numbering of the headings and paragraphs in the Guidelines section corresponds to the
numbering of IEC 61831 which this Practice revises. The type of revision made to a
specified heading or paragraph is described after the heading or paragraph identification. All
provisions of IEC 61831 that are not revised remain in force.

PIP recommends the use of International Electrotechnical Commission (IEC) Technical


Report TR 61831, On-Line Analyser Systems - Guide to Design and Installation as
PIP PCEPA001, Process Analyzer System Engineering Guidelines, with the following
additional comments:

3. “Housings”
3.1 Ventilation requirements - modification. The over pressure should be
limited to a total pressure of 50 Pa instead of 2 to 5 mbar.
3.2 Purged Equipment - modification to final paragraph. The certification EX
“p” should not be specified because it is not recognized in the National
Electric Code (NEC) Division System of Classification.

Page 2 of 3 Process Industry Practices


COMPLETE REVISION PIP PCEPA001
August 2006 Process Analyzer System Engineering Guidelines

4. “Sampling Systems”
4.1 Introduction - modification to final paragraph. PIP PCTPA001, Process
Analyzer System Acceptance Testing, should be used for sample system
physical inspection.
4.2 “Sample Point Location - modification to item (f). The analyzer and
laboratory process sample point may be combined and the sample system
should be designed to prevent low flow when both are in use.
4.3 “Fast Circulating Systems” - modification to paragraph 7. The sample to the
analyzer should normally be filtered. The type of filter chosen is a function
of sample system design.
4.4 Special Considerations - modification to final paragraph. Pressure relief
valves should be included in the system design if required to prevent the
fluid pressure from rising to a value that could cause analyzer system
hardware failure and loss of fluid containment.
4.5 General - modification to paragraph 3 – Following the first process take-off
valve, instrumentation tubing specifications are commonly used for sample
transport including analyzer fast loops and analyzer flows.

Process Industry Practices Page 3 of 3


COMPLETE REVISION
September 2006

Process Industry Practices


Process Control

PIP PCCPA001
Process Analyzer System Design Criteria
PURPOSE AND USE OF PROCESS INDUSTRY PRACTICES

In an effort to minimize the cost of process industry facilities, this Practice has
been prepared from the technical requirements in the existing standards of major
industrial users, contractors, or standards organizations. By harmonizing these
technical requirements into a single set of Practices, administrative, application, and
engineering costs to both the purchaser and the manufacturer should be reduced. While
this Practice is expected to incorporate the majority of requirements of most users,
individual applications may involve requirements that will be appended to and take
precedence over this Practice. Determinations concerning fitness for purpose and
particular matters or application of the Practice to particular project or engineering
situations should not be made solely on information contained in these materials. The
use of trade names from time to time should not be viewed as an expression of
preference but rather recognized as normal usage in the trade. Other brands having the
same specifications are equally correct and may be substituted for those named. All
Practices or guidelines are intended to be consistent with applicable laws and
regulations including OSHA requirements. To the extent these Practices or guidelines
should conflict with OSHA or other applicable laws or regulations, such laws or
regulations must be followed. Consult an appropriate professional before applying or
acting on any material contained in or suggested by the Practice.

This Practice is subject to revision at any time by the responsible Function Team and
will be reviewed every 5 years. This Practice will be revised, reaffirmed, or withdrawn.
Information on whether this Practice has been revised may be found at www.pip.org.

© Process Industry Practices (PIP), Construction Industry Institute, The


University of Texas at Austin, 3925 West Braker Lane (R4500), Austin,
Texas 78759. PIP member companies and subscribers may copy this Practice
for their internal use. Changes, overlays, addenda, or modifications of any
kind are not permitted within any PIP Practice without the express written
authorization of PIP.

PIP will not consider requests for interpretations (inquiries) for this Practice.

Printing History

August 2000 Issued September 2006 Complete Revision

Not printed with State funds


COMPLETE REVISION
September 2006

Process Industry Practices


Process Control

PIP PCCPA001
Process Analyzer System Design Criteria
Table of Contents

1. Introduction................................. 2
1.1 Purpose............................................ 2
1.2 Scope ............................................... 2

2. References .................................. 2
2.1 Process Industry Practices............... 2
2.2 Industry Codes and Standards......... 2

3. Definitions ................................... 2

4. Requirements.............................. 3
4.1 General ............................................ 3
4.2 Safety ............................................... 4
4.3 Process Interface ............................. 4
4.4 Sample Transport ............................ 6
4.5 Sample Conditioning ........................ 7
4.6 Calibration ........................................ 8
4.7 Analyzer Shelters ............................. 8
4.8 Status and Validation Signals .......... 9
4.9 Documentation ................................. 9

Process Industry Practices Page 1 of 9


PIP PCCPA001 COMPLETE REVISION
Process Analyzer System Design Criteria September 2006

1. Introduction

1.1 Purpose
This Practice provides requirements for use by an experienced analyzer systems engineer
for the design and installation of process analyzer systems.

1.2 Scope
This Practice describes the requirements for process analyzer systems which are
engineered, designed, and fabricated for the following:
a. Process measurement monitoring or control.
b. Effluent measurement monitoring or control.
c. Ambient atmospheric measurement monitoring or control.

2. References
Applicable parts of the following Practices, industry codes and standards, and references shall be
considered an integral part of this Practice. The edition in effect on the date of the contract award
shall be used, except as otherwise noted. Short titles will be used herein where appropriate.

2.1 Process Industry Practices (PIP)


– PIP PCEPA001 - Process Analyzer System Engineering Guidelines
– PIP PCSPA001 - Process Analyzer Project Documentation Data Sheet Instructions
– PIP PCSPA01D - Process Analyzer Project Documentation Data Sheet
– PIP PCSPA002 - Process Analyzer System Data Sheet Instructions

2.2 Industry Codes and Standards


– IEC TR61831 - On-Line Analyser Systems – Guide to Design and Installation

3. Definitions
process analyzer system: A system that consists of an analyzer, a sample-conditioning system,
and one or more readout devices. The system is designed and assembled to automatically take a
representative portion of a process stream and to identify and measure specific component
concentrations or physical properties of the sample.

fast loop: A part of the sample transport system that is designed to transport the process sample
close to but not through the analyzer. The purpose is to reduce the time lag in getting sample
from the process tie point, it should be returned to process whenever possible. The term “speed
loop or bypass sample line” is sometimes used to define the same part of the system.

sample: The process take off from the fast loop that is delivered to the analyzer for specific
component analysis or for physical property determination.

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COMPLETE REVISION PIP PCCPA001
September 2006 Process Analyzer System Design Criteria

calibration and auto-calibration: The introduction of a standard to the analyzer. The measured
results are compared with the standard, and the response factors of the analyzer are adjusted so
that the measured results match the standard. Auto-calibration is the same activity with no human
intervention and is normally on a fixed time cycle.

validation and auto-validation: The introduction of a standard to the analyzer. The measured
results are compared with historical data and reported, and the response factor is not changed.
Auto-validation is the same activity with no human intervention and is normally on a fixed time
cycle. Other terms commonly used are “bench mark” and “check peak.” When the historical data
trend of a validation sample clearly exceeds the acceptable limit, the instrument should be
calibrated.

Original Equipment Manufacturer (OEM) Tests: The acceptance tests that are performed at the
Analyzer Manufacturer’s facility. These tests must have defined and measurable parameters with
repeatability factors or tolerance factors that are stated in the data sheets or in engineering notes.
Examples of these tests are baseline drift, repeatability, resolution, signal ranges, etc.

Factory Acceptance Tests (FAT): The tests that are performed at an Analyzer System Vendor’s
(ASV) facility after complete fabrication and assembly of the analyzer system(s).

Site Acceptance Test (SAT): The transfer of ownership of an analyzer system following a defined
period of uninterrupted, on-line operation within acceptable performance parameters. These tests,
including the documentation requirements and standards compliance, must be fully defined at the
bidding stage of an analyzer project.

4. Requirements

4.1 General
The process analyzer system design shall consider and integrate the following design
aspects:
a. physical and chemical properties data for each monitored sample stream
b. analytical technologies available
c. safety (e.g., relief vents, analyzer vents, safety monitors, safety equipment)
d. process interface (e.g., sample probes, in-line sensing elements)
e. sample transport
f. sample conditioning
g. calibration
h. analyzer shelter
i. status and validation signals
j. signal conversions and control system interfaces
k. materials of construction

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PIP PCCPA001 COMPLETE REVISION
Process Analyzer System Design Criteria September 2006

l. utilities support
m. maintenance
n. reliability
o. operability

4.2 Safety
4.2.1 Safety shall be the foremost design parameter during all stages of the analyzer
selection and system design.
4.2.2 The system design shall be in accordance with all applicable codes and
standards, and all electrical equipment and instrumentation shall meet the
electrical area classification where installed.
4.2.3 For highly toxic process samples, the following shall be considered:
a. Distance (minimize) of the analyzer to the process sample source point
b. Quantity (minimize) of sample needed for a reliable, safe, and speedy
analysis
c. Distance of the analyzer to the sample disposal or return point for proper
disposal of spent samples
d. Availability of safety support equipment, such as breathing air stations,
safety showers, etc.
e. Emergency escape routes from the analyzer location
f. Location of toxic gas monitors and alarm devices
4.2.4 For highly flammable process samples, the following shall be considered:
a. Lower explosive limit of sample stream constituents
b. Lower explosive limit of chemical reagent components
c. Surface temperature of sample system hardware components (T-Rating)
d. Need and location of combustible area monitoring detectors and the
calibration of the monitors for the sample stream
e. Sources of static electricity such as air conditioner blowers, etc.
f. Safety issues with any of the other process analysis requirements
4.2.5 Transport, conditioning, and disposal of the sample shall not create a hazard to
personnel, the environment, the process, or the facility that is being monitored.
4.2.6 All hazardous materials, that are part of the analyzer system, or are required
reagents for the system, shall be properly identified, labeled, or tagged.

4.3 Process Interface


4.3.1 Sample Probes
4.3.1.1 A sample probe shall be installed in lines 3 inches (75 mm) or greater in
diameter.

Page 4 of 9 Process Industry Practices


COMPLETE REVISION PIP PCCPA001
September 2006 Process Analyzer System Design Criteria

4.3.1.2 The sample point shall be selected to provide a representative sample,


fast response time and maintainability.
4.3.1.3 The sample probe shall be positioned at 12 o’clock or 3 o’clock on a
horizontal line or at any position on a vertical line. There shall be
sufficient clearance for insertion and removal of the probe. The probe
shall be located in the permanently gas-filled portion of the pipe for gas
sampling and in the permanently liquid-filled portion of the pipe for
liquid sampling.
4.3.1.4 Sample points that can be multi-phase shall be avoided.
4.3.1.5 Space must be considered for the removal of the sample probe.
4.3.1.6 Fixed-flange probes are recommended for any operating pressures.
These probes shall have the following features:
a. An arrow stamped on the flange indicating the direction of flow
in the process line
b. Capable of being rodded out or blown back to process
c. Welded shutoff valve in accordance with line specifications
d. Sized for approximately 30% immersion beyond the inside pipe
wall up to a maximum immersion of 3 inches (75 mm)
Comment: A typical fixed-flange sample probe is shown in
Annexe A of IEC 61831, (PIP PCEPA001).
Approximate calculations are shown in subsequent
annexes.
4.3.1.7 For high-maintenance service, retractable sample probes shall be
permitted if equipped with the following additional safety features and
characteristics:
a. Arrow stamped for flow orientation
b. Marked for insertion depth Comment: scoring tubing reduces
mechanical strength
c. Marked for retraction depth to clear the process root valve
d. Expanded section on end of probe to prevent blowout through
packing gland
e. Safety chain for blowout prevention
4.3.1.8 Special-purpose, high-pressure, retractable probe devices are
commercially available and may be used for pipeline or similar
demanding service.
4.3.1.9 Fixed or retractable sample probes shall be in accordance with the
process pipe specification and shall have the mechanical strength to
avoid failure in high-velocity flow conditions.
4.3.1.10 Harmonic calculations are available and shall be used to predict the
mechanical breakpoint of the sample probe.

Process Industry Practices Page 5 of 9


PIP PCCPA001 COMPLETE REVISION
Process Analyzer System Design Criteria September 2006

4.31.11 The sample probe shall be subjected and marked in accordance with the
Positive Material Identification (PMI) requirements.
4.3.2 In-Line Sensing Elements
4.3.2.1 In-line sensing elements shall be designed to be removed for
replacement or maintenance while the process is in operation.
4.3.2.2 Sensing elements and analyzers that are mounted in process slip streams
shall be designed to be blocked in, depressurized, and flushed while the
process is in operation.
4.3.2.3 All “wet electrolyte” sensing elements must be installed so that the
sensing element is constantly wetted to ensure that the sensor does not
dry out.
4.3.2.4 In-line sensing elements shall be installed so that the sensing element
does not become fouled with debris.

4.4 Sample Transport


4.4.1 The primary objective of fast loop design shall be to minimize the sample
transport time and the mass of sample transported.
4.4.2 One or more of the following techniques may be used to minimize sample
transport time or sample mass:
a. Pressure reduction
b. Phase change
c. Minimum-bore tubing and components
d. Eductors
e. Pumps
f. Heating
4.4.3 The sample return point selected directly influences fast loop design. The sample
return point shall be selected to optimize the sample return flow to process.
4.4.4 Sample Phase
4.4.4.1 Phase shall not be changed if the sample phase matches the phase
required by the analyzer.
4.4.4.2 Phase shall be changed if required for analyzer system operation.
4.4.4.3 To avoid erratic analysis results, if a phase change is designed into the
sample transport system, the phase change shall be maintained once it
has occurred.
4.4.5 Sample transport system components shall be stainless steel unless the process
sample is not compatible with stainless steel.
4.4.6 Sample transport systems shall be designed and fabricated without low spots,
loops, or pockets.

Page 6 of 9 Process Industry Practices


COMPLETE REVISION PIP PCCPA001
September 2006 Process Analyzer System Design Criteria

4.5 Sample Conditioning


4.5.1 The sample-conditioning system shall not alter the concentration of the measured
component.
4.5.2 Response time of the sample-conditioning system shall be consistent with the
requirements of process control or monitoring.
4.5.3 The system shall be maintainable and provide sufficient information to aid in
trouble shooting the analyzer system.
4.5.4 The sample-conditioning system may include auto-calibration and/or auto-
validation.
4.5.5 All materials used in the sample-conditioning system, including elastomers,
metals, and composites, shall be verified for compatibility with the process
sample.
4.5.6 Isolation valves shall be provided at the sample probe and sample return points
and at the sample-conditioning system. Comment: Typically a flush valve is
included to run the fast loop with the sample system isolated.
4.5.7 Dead-volume components contributing to increased lag time shall be minimized.
4.5.8 Double block and bleed, or equivalent, shall be used to prevent an incorrect
analysis caused by cross contamination from valve leaks in multi-stream sample
systems.
4.5.9 Pressure or temperature sensitive components or devices used in the sample-
conditioning system shall be protected from exposure to excessive pressure or
temperature.
4.5.10 Heated sample lines shall enter the sample-conditioning enclosure via heat
shrink entry seals to ensure that the sample temperature is uniformly maintained
and that no cold spots are created.
4.5.11 The sample-conditioning system enclosure shall have windows suitable for
viewing measuring devices (e.g., pressure, flow, etc.) if the enclosure cannot be
opened because of safety requirements or operating conditions.
4.5.12 If high temperatures are maintained within the enclosure, all adjustments for the
sample conditioning system shall be externally accessible.
4.5.13 Sample-conditioning enclosures shall close and seal sufficiently using, at a
minimum, a single-handle, three-point latch mechanism.
4.5.14 All sample-conditioning systems, whether enclosed or plate-mounted, shall be
provided with a means for decontamination before maintenance.
4.5.15 For samples containing toxic or flammable materials, the location of sample-
conditioning systems shall be determined by the following:
a. For an analyzer located inside an analyzer building, the sample-conditioning
system shall be installed on an outside exterior wall and shall include flow-
limiting devices to the analyzer.

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PIP PCCPA001 COMPLETE REVISION
Process Analyzer System Design Criteria September 2006

b. For field-mounted analyzer enclosures, the sample-conditioning system shall


be installed adjacent to the analyzer enclosure.
c. For analyzers mounted in three-sided, free-ventilation shelters, the sample-
conditioning system shall be installed where most convenient for
maintenance.
4.5.16 Components of all sample-conditioning systems, whether enclosed or plate-
mounted, shall be installed in such a way that each can readily be removed for
maintenance without removing any others.
4.5.17 All components and controls of sample-conditioning systems, whether enclosed
or plate-mounted, shall be clearly tagged and labeled for ease of identification
and maintenance. Normal settings such as flow and pressure shall be indicated.

4.6 Calibration
4.6.1 All process analyzer systems shall be provided with a means for calibration.
Comment: The design of a process analyzer system influences its overall
precision. The calibration standard used on the system
determines only the relative accuracy. PIP PCSPA002 defines
and specifies these terms.
4.6.2 Calibration samples shall be introduced to the analyzer in the same phase as the
conditioned process sample.

4.7 Analyzer Shelters


4.7.1 The selection of a shelter for a Process Analyzer System shall be based upon the
following:
a. Analyzer manufacturer’s published specifications for operating conditions
b. Ambient site conditions
c. Criticality of analysis
d. Owner’s requirements
4.7.2 The following four basic types of analyzer shelters may be used:
a. Type I – Field mounted - An analyzer in an integral enclosure mounted on a
free-standing support
b Type II – Freely ventilated - Typically a three-sided shelter
c Type III – Climate controlled - Enclosure interior is temperature controlled
for proper operation of the analyzer system(s)
d. Type IV – Controlled for area classification reduction - Enclosure interior
is pressurized and purged to allow operation of analyzer system(s) that are
not rated for the exterior area classification
4.7.3 For shelter Types III and IV, doors shall open outward and shall be equipped
with panic hardware, automatic door closers, and windows.

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COMPLETE REVISION PIP PCCPA001
September 2006 Process Analyzer System Design Criteria

4.7.4 Closed shelters shall be equipped with appropriate sensors for combustible gas,
toxic gas, oxygen deficiency, and loss of pressurization.
4.7.5 Alarm conditions shall be shown outside each entry door and transmitted to a
continuously monitored location.

4.8 Status and Validation Signals


4.8.1 Valid analytical information shall be conveyed to the owner’s Control System.
4.8.2 If a process analyzer system is on closed loop control and has a fault/status
signal available, this signal shall be transmitted along with the measured
parameter to the owner’s Control System and/or his monitoring computer.
Comment: As the complexity of a process analyzer system increases, other
signals may be required (e.g., calibration, purge fail, no sample
flow, etc.).

4.9 Documentation
4.9.1 Once a process analyzer system is shipped to its final destination, the following
minimum documentation shall be provided:
a. Original Equipment Manufacturer’s documentation for all parts of the
system
b. Analyzer System vendor’s drawings and documentation
c. Original specifications with all agreed-upon changes documented by the
Analyzer System vendor
d Start-up and shut-down procedures
e. Calibration procedures
f. Maintenance procedures
g. All software documented to facilitate changes by the owner
4.9.2 Documentation shall be provided in accordance with PIP PCSPA001.

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