You are on page 1of 16

TÜRK STANDARDI

TS EN 1426
Ocak 2008

TS 118 EN 1426:2002 yerine

ICS 75.140; 91.100.50

Bitüm ve bitümlü bağlayıcılar-İğne batma derinliği tayini

Bitumen and bituminous binders - Determination of needle penetration

Bitumes et liants bitumineux - Détermination Bitumen und bitumenhaltige Bindemittel -


de la Bestimmung der
pénétrabilité à l'aiguille Nadelpenetration

TÜRK STANDARDLARI ENSTİTÜSÜ


Necatibey Caddesi No.112 Bakanlıklar/ANKARA
TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
ICS 75.140; 91.100.50 TS EN 1426 : 2008-01
TÜRK STANDARDI
EN 1426:2007
Milli Önsöz

Bu standard, CEN/TC 336 “Bituminous binders-Bitümlü bağlayıcılar” Teknik Komitesi tarafından


hazırlanmış, CEN tarafından 03.02.2007 tarihinde onaylanmış ve Türk Standardları Enstitüsü Teknik
Kurulu'nun 31.01.2008 tarihli toplantısında Türk Standardı olarak kabul edilerek yayımına karar
verilmiştir.

Bu standardda kullanılan bazı kelimeler ve/veya ifadeler patent haklarına konu olabilir. Böyle bir
patent hakkının belirlenmesi durumunda TSE sorumlu tutulamaz.

Bu standard yayınlandığında TS 118 EN 1426:2002 standardının yerini alır.

CEN üyeleri sırasıyla, Almanya, Avusturya, Belçika, Birleşik Krallık, Bulgaristan, Çek Cumhuriyeti,
Danimarka, Estonya, Finlandiya, Fransa, Hollanda, İrlanda,İspanya, İsveç, İsviçre, İtalya, İzlanda,
Kıbrıs, Letonya, Litvanya, Lüksemburg, Macaristan, Malta, Norveç, Polonya, Portekiz, Romanya,
Slovakya, Slovenya ve Yunanistan'ın millî standard kuruluşlarıdır.

TS EN 1426 : 2008 standardı, EN 1426:2007


standardı ile birebir aynı olup, Avrupa Standardizasyon Komitesi'nin (rue de Stassart, 36 B-1050 Brussels) izniyle basılmıştır.

Avrupa StandardlarınınTÜRK STANDARDLARININ


herhangi bir şekildeTELiF HAKKI TSE'YE
ve herhangi AiTTiR.
bir yolla tümSTANDARDIN BU NÜSHASININ
kullanım hakları KULLANIM iZNiKomitesi
Avrupa Standardizasyon TSE TARAFINDAN
(CEN/CENELEC) ve
üye ülkelerine aittir.KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE kanalıyla CEN/CENELEC'den yazılı izin alınmaksızın çoğaltılamaz.
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01

EUROPEAN STANDARD EN 1426


NORME EUROPÉENNE
EUROPÄISCHE NORM March 2007

ICS 75.140; 91.100.50 Supersedes EN 1426:1999

English Version

Bitumen and bituminous binders - Determination of needle


penetration

Bitumes et liants bitumineux - Détermination de la Bitumen und bitumenhaltige Bindemittel - Bestimmung der
pénétrabilité à l'aiguille Nadelpenetration

This European Standard was approved by CEN on 3 February 2007.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the
official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION


COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: rue de Stassart, 36 B-1050 Brussels

© 2007 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 1426:2007: E
worldwide for CEN national Members.

TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

Contents Page

Foreword..............................................................................................................................................................3
1 Scope ......................................................................................................................................................4
2 Normative references ............................................................................................................................4
3 Terms and definitions ...........................................................................................................................4
4 Principle..................................................................................................................................................4
5 Apparatus ...............................................................................................................................................5
6 Sampling.................................................................................................................................................7
7 Procedure ...............................................................................................................................................7
8 Expression of results ............................................................................................................................9
9 Precision.................................................................................................................................................9
10 Test report ............................................................................................................................................10
Annex A (normative) Characteristics of thermometers ...............................................................................13
Bibliography ......................................................................................................................................................14

2 TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

Foreword
This document (EN 1426:2007) has been prepared by Technical Committee CEN/TC 336 “Bituminous
binders”, the secretariat of which is held by AFNOR.

This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by September 2007, and conflicting national standards shall be
withdrawn at the latest by September 2007.

This document supersedes EN 1426:1999.

According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
Sweden, Switzerland and United Kingdom.

TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN 3
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

1 Scope
This European Standard specifies a method for determining the consistency of bitumen and bituminous
binders. Normal procedure is described for penetrations up to 330 × 0,1 mm, but for penetrations above this
value, up to 500 × 0,1 mm, different operating parameters are necessary.

WARNING — Use of this European Standard may involve hazardous materials, operations and
equipment. This European Standard does not purport to address all of the safety problems associated
with its use. It is the responsibility of the user of this European Standard to establish appropriate
safety and health practices and determine the applicability of regulatory limitations prior to use.

2 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.

EN 58, Bitumen and bituminous binders – Sampling bituminous binders

EN 1425, Bitumen and bituminous binders – Characterization of perceptible properties

EN 1427, Bitumen and bituminous binders – Determination of the softening point – Ring and Ball method

EN 10088-3, Stainless steels – Part 3: Technical delivery conditions for semi-finished products, bars, rods,
wire, sections and bright products of corrosion resisting steels for general purposes

EN 12594, Bitumen and bituminous binders – Preparation of test samples

EN 12597, Bitumen and bituminous binders – Terminology

ISO 6508-1, Metallic materials – Rockwell hardness test – Part 1: Test method (scales A, B, C, D, E, F, G, H,
K, N, T)

3 Terms and definitions


For the purposes of this document, the terms and definitions given in EN 12597 and the following applies.

3.1
penetration
consistency, expressed as the distance in tenths of a millimetre that a standard needle will penetrate vertically
into a sample of the material under specified conditions of temperature, load and loading duration

4 Principle
The penetration of a standard needle into a conditioned test sample shall be measured. For penetrations up to
approximately 330 × 0,1 mm the operating parameters shall be a test temperature of 25 °C, an applied load of
100 g, and a loading duration of 5 s. For penetrations expected above approximately
330 × 0,1 mm, the test temperature shall be reduced to 15 °C but the operating parameters of the applied load
and the loading duration remain unchanged.

4 TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

5 Apparatus
Usual laboratory apparatus and glassware, together with the following:

5.1 Penetrometer; apparatus that permits a needle holder to move vertically without measurable friction
and enables the needle penetration to be determined to the nearest 0,1 mm. The needle holder shall be
readily detachable from the apparatus and shall have a mass of (47,50 ± 0,05) g. A weight of (50,00 ± 0,05) g
suitable for attachment to the needle holder shall be provided if not already fixed to the needle holder. The
stand upon which the specimen container, or transfer dish rests shall be flat and horizontal. The 50 g weight
shall be fixed underneath the support (see Figure 1).

NOTE An example of a suitable penetrometer is shown in Figure 1. To facilitate levelling, the penetrometer should be
provided with level adjustment screws.

Equipment that controls the penetration time automatically may also be used. Such equipment shall be
checked regularly for correct penetration time (see 5.6).

5.2 Penetration needle, (see Figure 2), made from fully hardened, tempered and polished stainless steel
of type X105CrMo17 (1.4125), conforming to EN 10088-3, taking into account that it is not necessary to
comply with the minimum content of molybdenum specified in that standard, and of Rockwell hardness C54 to
C60 determined in accordance with ISO 6508-1. The cylindrical body of the needle shall have a diameter of
1,00 mm to 1,02 mm and one end shall be symmetrically tapered by grinding to a cone with an angle of 9 °
(10 ± 30) ' over the entire cone length. The cone shall be co-axial with the cylindrical body of the needle; the
total axial variation of the intersection between the conical and cylindrical surfaces shall not exceed 0,2 mm.
The conical tip of the needle shall be ground square to the axis of the needle within 2 ° until the diameter at
the tip is between 0,14 mm and 0,16 mm. The edge of the ground tip shall be sharp and free from burrs.

For penetrations up to 330 × 0,1 mm the length of the needle shall be approximately 50 mm. For penetrations
between 330 × 0,1 mm and 500 × 0,1 mm, use needles that shall conform to the requirements given for mass
and dimensions, but which are longer in length so that the ferrule into which the needle is fixed does not
penetrate the material undergoing testing.

The needle shall be rigidly mounted in a brass or stainless steel ferrule with 5 mm to 10 mm of the needle
inside the ferrule. The run-out of the needle tip or any part of the needle relative to the ferrule axis shall not
exceed 1,0 mm. The ferrule shall be (3,20 ± 0,05) mm in diameter and (38 ± 1) mm in length.

The mass of the ferrule and needle assembly shall be (2,50 ± 0,05) g.

NOTE 1 A drill hole at the end of the ferrule or a flat on the side is possible to control the mass.

Individual identification marking shall be engraved or stamped on the ferrule of each needle; the same
marking shall not be repeated by the manufacturer within a 3 year period.

The needle shall be inspected visually for corrosion and shape and the masses of the needle and spindle
checked sufficiently regularly to assure satisfactory condition.

NOTE 2 The mass of the needle plus needle holder together with the additional mass of the weight provides a moving
load of 100 g.

It is important that initial and continued compliance with the stringent requirements for the needle is
maintained. Certification of compliance can be obtained through the needle supplier or a qualified agency.

NOTE 3 For information concerning tolerances of the needle (Figure 2), see ISO 286-1, ISO 1829, ISO 1101 and ISO
1302.

TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN 5
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

5.3 Test sample container, metal or glass, cylindrical, flat-bottomed. The internal depth of the container
shall be appropriate in order to contain a bituminous sample of which the depth shall be at least 10 mm
greater than the expected penetration, and not less than 35 mm. The internal diameter of the container shall
be at least 55 mm and shall not exceed 70 mm.

NOTE 1 Recommended dimensions of the test sample container are given in Table 1.

Table 1 — Recommended dimensions of the test sample container


Penetration Internal depth Internal diameter

(0,1 mm) (mm) (mm)

penetration < 160 35 55

160 ≤ penetration ≤ 330 45 70

If insufficient binder is available (e.g. if it was obtained by extraction of a bituminous mix core or while
monitoring short- or long-term ageing development) use a small stainless steel container. In order to fulfil the
requirements of 7.4.2, the container shall have an inner diameter of at least 35 mm and a wall thickness
between 1,5 mm and 2,0 mm. For penetrations lower than 100 x 0,1 mm, the inner height of the container
shall be at least 20 mm. For penetrations from 100 x 0,1 mm up to 200 x 0,1 mm, the inner height of the
container shall be at least 30 mm. To ensure a good stable temperature during testing, the container shall be
placed in a brass ring with an inner diameter within 0,5 mm of the outer diameter of the sample container and
a height of (21 ± 1) mm or (31 ± 1) mm.

NOTE 2 The precision of the penetration values determined using the metal ring can be different from those given in
Clause 9.

5.4 Water bath (constant temperature bath), with a capacity of at least 10 l, and able to maintain the
temperature of the test sample within ± 0,15 °C. The bath shall have a perforated shelf supported in a position
not less than 50 mm from the bottom and not less than 100 mm below the liquid level in the bath. If
penetration tests are to be made in the bath itself, an additional shelf, strong enough to support the
penetrometer shall be provided.

NOTE The use of distilled or deionized water is recommended for the bath. Care should be taken to avoid
contamination of the bath water by active surface agents or any other material that can affect the penetration values.

5.5 Transfer dish, for tests outside the water bath. The dish shall have a capacity of at least 350 ml and
shall be deep enough to ensure that the test sample container is completely covered with water.

The bottom of the transfer dish shall be constructed so that the dish cannot be rocked when it is placed on the
stand of the penetrometer. Similarly the surface on which the test sample container rests shall be made so
that the test sample container cannot rock during penetration of the test sample.

For temperatures lower than 25 °C, the capacity of the transfer dish shall be 1,5 l.

5.6 Timing device, accurate to within 0,1 s.

5.7 Thermometers, solid stem, as specified in Annex A.

Other temperature measuring devices may be used instead of mercury stem thermometers, however, the
mercury stem thermometer is the reference device and any alternative device employed shall be calibrated to
provide the same readings as a mercury stem thermometer, recognising and allowing for change of thermal
response compared with Hg thermometer.

6 TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

NOTE 1 When measuring and controlling nominally constant temperatures, as in the method described, alternative
devices can indicate greater cyclic variations than mercury thermometers, to an extent depending on the cycle time of
heating and the power of the controlled heat input.

NOTE 2 In order to obtain the relevant precision (± 0,15 °C), reading of the temperature on thermometer should be
performed with a lens

6 Sampling

6.1 Take the laboratory sample in accordance with EN 58, taking all necessary safety precautions, and
ensuring that the test sample is representative of the laboratory sample from which it is taken. Ensure that the
laboratory sample is homogeneous and is not contaminated (see EN 1425).

6.2 Remove a sufficient amount of the laboratory sample, if necessary using a warmed knife, and transfer it
to a suitable container (see EN 12594).

6.3 Raise the material to the required temperature, i.e. 80 °C to 90 °C above the expected softening point
(see EN 1427) and fill one clean (free of dust, grease, rust, etc...) test sample container (5.3). Fill the container
to a depth so that, when the test sample is cooled to the test temperature, the depth is 10 mm greater than the
depth to which the needle is expected to penetrate.

For polymer modified bitumen, the temperature may not exceed 200 °C irrespective of the softening point.

6.4 Immediately after filling, loosely cover the test sample container with a container such as a lipped
beaker of suitable size.

NOTE 1 This assists in eliminating any air bubbles and it is a convenient way of providing protection against dust.

Allow the test sample to cool at an ambient temperature between 15 °C and 30 °C; for test samples less than
or equal to 45 mm deep, cool for 60 min to 90 min and for test samples more than 45 mm to 60 mm deep,
cool for 90 min to 120 min provided the volume of the test sample does not exceed 180 ml; for test samples of
more than 180 ml, cool for 60 min to 90 min for each 100 ml of test sample, then, place the test sample in the
constant temperature bath for a similar period to that used for cooling, and start testing.

NOTE 2 For measurement at temperatures lower than 25 °C, longer cooling times can be required.

6.5 When test conditions are not specified, for penetration values below approximately 330 × 0,1 mm, the
temperature, total applied load (see 5.2 Note 2) and loading duration shall be 25 °C, 100 g and 5 s. For
penetration values above approximately 330 × 0,1 mm, the test shall be carried out at conditions of 15 °C,
100 g and 5 s.

When other conditions are used, the details shall be reported in full.

NOTE In this case, the precision can be different from that stated in Clause 9.

7 Procedure

7.1 Preparation of the needle holder and needles

Examine the needle holder and its guide to check that it is free of water and other extraneous matter. Ensure
that the needle holder moves freely in its guide. Clean a penetration needle with toluene or other suitable
solvent, dry with a clean cloth and insert the needle into the needle holder. Unless otherwise specified, add
the 50 g weight and ensure that the total applied load is (100,00 ± 0,10) g.

Erratic results can be obtained with bitumen’s from certain sources. In such cases the needles shall be pre-treated by
immersing for 5 min in a 1% solution of oleic acid in toluene prior to drying.

TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN 7
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

7.2 Tests in the constant temperature bath

If tests are made with the penetrometer in the bath, place the test sample container directly on the submerged
shelf of the penetrometer. Keep the test sample container completely covered with the water in the bath.

7.3 Tests outside the constant temperature bath

If tests are made with the penetrometer outside the bath, place the sample container in the transfer dish that
has been kept in the bath with the test samples, cover the test sample container completely with water from
the constant temperature bath, and place the transfer dish on the stand of the penetrometer. Make sure that
the transfer remains at the chosen temperature until the measurement is completed.

For reference tests, make penetrations at temperatures other than 25 °C without removing the test samples
from the bath unless the transfer dish is separately controlled to ensure the correct temperature.

7.4 Determination of the penetration

7.4.1 First determinations

With the test sample container in position, slowly lower the needle until its tip just makes contact with its image
reflected by the surface of the test sample. Ensure that the zero position of the needle is noted, then, quickly
release the needle holder for the specified period of time. If the container moves during the determination,
discontinue the test. Adjust the instrument as necessary to determine the penetration of the needle into the
sample in tenths of a millimetre.

NOTE The positioning of the needle can be aided materially by good illumination, e.g. by the use of an illuminated
methyl methacrylate tube or a lens.

7.4.2 Repeat determinations

Carry out at least three valid determinations with three separate needles at points on the surface of the test
sample that are not less than 10 mm from the sides of the container and are not less than 10 mm apart. Use a
clean needle for each determination. If the penetration is greater than 100 × 0,1 mm, leave all the needles in
the test sample until all the determinations have been completed. If the test is carried out outside the bath and
the three determinations are not carried out within 2 min, return the test sample and transfer dish to the bath
and repeat the determination(s).

7.5 Maximum range of valid determinations

For tests carried out under the conditions of a test temperature of 25 °C, a total applied load of 100 g and a
loading duration of 5 s, the three determinations shall be acceptable if the range of the results obtained does
not exceed the relevant value given in Table 2.

Table 2 — Maximum range of the valid determinations


250 and
Penetration in 0,1 mm up to 49 50 to 149 150 to 249
above

Maximum difference between


2 4 6 8
highest and lowest determinations

NOTE These ranges are not necessarily applicable at other conditions and for modified bitumen. For modified
bitumen they should only be used as guidance, until criteria are available.

8 TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

If the appropriate maximum difference is exceeded, discard the results and repeat the test from clause 6 on a
second sample test container.

If the appropriate range is again exceeded, ignore all determinations and repeat the test until three valid
determinations have been obtained on the same test sample.

7.6 After completing the test, clean the penetration needles with a suitable solvent and store so as to
prevent corrosion or damage. Do not use detergent or silicone oil for cleaning the needles.

8 Expression of results
Express the penetration value as the arithmetic mean of the acceptable determinations (see 7.5), in tenths of
a millimetre rounded to the nearest integer.

9 Precision

9.1 Repeatability

The difference between two test results obtained by the same operator with the same apparatus under
constant operating conditions on identical test material would, in the long run, in the normal and correct
operation of the test method, exceed the values given in Table 3 in only one case in twenty.

9.2 Reproducibility

The difference between two single and independent test results obtained by different operators working in
different laboratories on identical test material would, in the long run, in the normal and correct operation of
the test method, exceed the values given in Table 3 in only one case in twenty.

Table 3 — Precision
Operating conditions Penetration in 0,1 mm Repeatability, r Reproducibility, R

25 °C

100 g < 50 2 3

5s ≥ 50 4 % of the mean value 6 % of the mean value

15 °C

100 g ≥ 50 5 % of the mean value 8 % of the mean value

5s

5 °C

200 g < 50 2 4

60 s ≥ 50 9 % of the mean value 13 % of the mean value

NOTE These precision data are not necessarily applicable at other conditions and for modified bitumen. For modified
bitumen they should only be used as a guide until further Round Robin Tests are available. These precision data state the
best available data at the moment.

TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN 9
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

10 Test report
The test report shall contain at least the following information:

a) type and complete identification of the sample under test;


b) reference to this European Standard;
c) type of apparatus (manual, automatic);
d) result of the test (see Clause 8);
e) any deviation, by agreement or otherwise, from the procedure specified;
f) date of the test.

10 TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

Key

1. Spindle 6. Needle and ferule

2. Dial assembly 7. Transfer dish with flat bottom

3. Needle holder 8. Test sample container

4. Release assembly 9. Base plate (stand)

5. 50 g mass 10. Level adjustment screw

Figure 1 — Example of penetrometer

TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN 11
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

All dimensions in millimetres

The radial run out shall not be greater


than 1 mm in any plane of measurement
during one revolution about the datum
axis A-B.

The axis of the cylinder, to which the


tolerance frame is connected, shall be
contained in a cylindrical zone of
diameter 0,2 with the datum axis C-D.

Figure 2 — Needle for penetration test

12 TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

Annex A
(normative)

Characteristics of thermometers

Temperature range °C - 8 to + 32 19 to 27 25 to 55
Scale marks
Subdivision °C 0,1 0,1 0,1
Long lines at each °C 0,5 0,5 0,5
Numbers at each °C 1 1 1
Max. scale error °C 0,1 0,1 0,1
Immersion Total Total Total
Expansion chamber temperature permits °C 80 100 105
heating to
Total length mm 374 to 384 270 to 280 374 to 384
Stem outside diameter mm 7,0 to 8,0 6,0 to 7,0 7,0 to 8,0
Bulb length mm 25 to 35 25 to 35 25 to 35
Bulb outside diameter mm 6,0 to 7,0 6,0 to 7,0 > 5,0 and not
greater than stem
Scale location
between bottom of bulb to line at °C -5 19 25
Distance mm 77 to 98 135 to 150 115 to 135
Length of scale mm 239 to 289 67 to 101 189 to 229

NOTE The thermometers ASTM 63C, 17C and 64C were found suitable for the different temperature ranges.

TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN 13
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.
TS EN 1426 : 2008-01
EN 1426:2007 (E)

Bibliography

[1] ISO 286-1, ISO system of limits and fits – Part 1: Bases of tolerances, deviations and fits

[2] ISO 1101, Geometrical Product Specifications (GPS) – Geometrical tolerancing – Tolerances of form,
orientation, location and run-out

[3] ISO 1302, Geometrical Product Specifications (GPS) – Indication of surface texture in technical
product documentation

[4] ISO 1829, Selection of tolerance zones for general purposes

14 TÜRK STANDARDLARININ TELiF HAKKI TSE'YE AiTTiR. STANDARDIN BU NÜSHASININ KULLANIM iZNi TSE TARAFINDAN
KARAYOLLARI GENEL MÜDÜRLÜGÜ'A VERiLMiSTiR. BASILMA TARiHi: 17.04.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR BÖLÜMÜ/TAMAMI iLTiBAS EDiLEMEZ, ÇOGALTILAMAZ.

You might also like